• Title/Summary/Keyword: inter mode

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200 MeV Ag15+ ion beam irradiation induced modifications in spray deposited MoO3 thin films by fluence variation

  • Rathika, R.;Kovendhan, M.;Joseph, D. Paul;Vijayarangamuthu, K.;Kumar, A. Sendil;Venkateswaran, C.;Asokan, K.;Jeyakumar, S. Johnson
    • Nuclear Engineering and Technology
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    • v.51 no.8
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    • pp.1983-1990
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    • 2019
  • Spray deposited Molybdenum trioxide (MoO3) thin film of thickness nearly 379 nm were irradiated with 200 MeV Ag15+ ion beam at different fluences (Ø) of 5 ×1011, 1 × 1012, 5 × 1012 and 1 × 1013 ions/㎠. The X-ray diffraction (XRD) pattern of the pristine film confirms orthorhombic structure and the crystallinity decreased after irradiation with the fluence of 5 × 1011 ions/㎠ due to irradiation induced defects and became amorphous at higher fluence. In pristine film, Raman modes at 665, 820, 996 cm-1 belong to Mo-O stretching, 286 cm-1 belong to Mo-O bending mode and those below 200 cm-1 are associated with lattice modes. Raman peak intensities decreased upon irradiation and vanished completely for the ion fluence of 5 ×1012 ions/㎠. The percentage of optical transmittance of pristine film was nearly 40%, while for irradiated films it decreased significantly. Red shift was observed for both the direct and indirect band gaps. The pristine film surface had densely packed rod like structures with relatively less porosity. Surface roughness decreased significantly after irradiation. The electrical transport properties were also studied for both the pristine and irradiated films by Hall effect. The results are discussed.

Simultaneous Determination of Baicalein, Baicalin, Wogonin, and Wogonoside in Rat Plasma by LC-MS/MS for Studying the Pharmacokinetics of the Standardized Extract of Scutellariae Radix

  • Chung, Hye-Jin;Lim, Sun-Young;Kim, In-Sook;Bu, Young-Min;Kim, Ho-Cheol;Kim, Dong-Hyun;Yoo, Hye-Hyun
    • Bulletin of the Korean Chemical Society
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    • v.33 no.1
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    • pp.177-182
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    • 2012
  • A new composition of standardized Scutellariae Radix extract (HPO12) was developed for treatment of Alzheimer's disease. For the preclinical pharmacokinetic study of HPO12, a rapid, sensitive, and selective LCMS/MS method was developed and validated for the simultaneous determination of 4 bioactive compounds, baicalein, baicalin, wogonin, and wogonoside. After extraction with ethylacetate, chromatographic analysis was performed on a Thermo $C_{18}$ column ($150mm{\times}2.1mm$, $3{\mu}m$) with a mobile phase consisting of 0.1% formic acid (A) and 0.1% formic acid in 95% acetonitrile (B) by using gradient elution at a flow rate of $250{\mu}L/min$. Analytes introduced to a mass spectrometer were monitored by multiple reaction monitoring (MRM) in positive ion mode. Using $25{\mu}L$ of plasma sample, the method was validated over the following concentration ranges: 25-5000 ng/mL for baicalein, 20-40000 ng/mL for baicalin, 1-1000 ng/mL for wogonin, and 5-10000 ng/mL for wogonoside. The intra- and inter-day precision and accuracy of the quality control samples at the 4 concentrations showed $\leq$ 13.7% relative standard deviation (RSD) and 86.6-105.5% accuracy. The method was successfully applied to determine the concentrations of baicalein, baicalin, wogonin, and wogonoside in rat plasma after intraperitoneal and oral administrations of HPO12.

A Fault Diagnosis Technique of an Inverter-fed PMSM under Winding Shorted Turn and Inverter Switch Open Fault (권선 단락 및 스위치 개방 고장 시의 인버터 구동 영구자석 동기전동기의 고장 진단 기법)

  • Kim, Kyeong-Hwa
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.24 no.5
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    • pp.94-105
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    • 2010
  • To detect faults in an inverter-fed permanent magnet synchronous motor (PMSM) drive under the circumstance having faults in a stator winding and inverter switch, an on-line basis fault detecting scheme during operation is presented. The proposed scheme is achieved by monitoring the second-order harmonic component in q-axis current and the fault is detected by comparing these components with those in normal conditions. The linear interpolation method is employed to determine the harmonic data in normal operating conditions. As soon as the fault is detected, the operating mode is changed to identify a fault type using the phase current waveform. To verify the effectiveness of the proposed fault detecting scheme, a test motor to allow inter-turn short in the stator winding has been built. The entire control algorithm is implemented using DSP TMS320F28335. Without requiring an additional hardware, the fault can be effectively detected by the proposed scheme during operation so long as the steady-state condition is satisfied.

Packetizing Scheme for Reliable Transmission of Wavelet Video Stream (신뢰성있는 웨이블릿 비디오 전송을 위한 패킷화 기법)

  • Lee, Joo-Kyong;Kang, Jin-Mi;Kim, Chung-Kil;Chung, Ki-Dong
    • The KIPS Transactions:PartB
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    • v.10B no.5
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    • pp.553-560
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    • 2003
  • Since Wavelet Transform decomposes a video frame into subbands with various frequencies and resolutions, the reconstructed video qualify at a receiver fluctuates according to the location of transmission errors within frames. This deteriorates the whole visual duality of the video. Specifically, for a wavelet based video which exploits the motion estimation prediction scheme, the transmission errors of a subband not only have a bad effect on other subbands within a same frame but also propagates to the subsequent frames. In this paper, we propose BDP(Block Based Dispersive Packetization) scheme, for a wavelet based video stream, which maintains constant video quality despite packet location that a transmission error occurs. To evaluate the performance of the proposed scheme, we use MRME(Multi-Resolution Motion Estimation) scheme to compress a video in Inter coding mode and Gilbert´s error model to generate the error patterns in wireless network environment. The simulation results show that BDP is more efficient than BP (Block based Packetization) or DP (Dispersive Packetization) in both PSNR and visual quality.

A Experimental Study on the Translation from Korean Digital Topographic Maps to Distributed Objects (수치지형도의 객체화 변환에 관한 연구)

  • 황철수
    • Spatial Information Research
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    • v.7 no.2
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    • pp.255-269
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    • 1999
  • This is an experimental study to translate the Korean digital topographic maps into distributable information-hide objects, which are designed with object-oriented development's key features ; encapsulation, polymorphism, inheritance, In order to achieve this goal , the characteristics of the data mode and inter-relationships of digital topographic maps are investigated . As a result, it is revealed that the current Korean digital topographic maps, which is organized into so many individual layers of mixed spatial and attributed data, have to explicit and concrete hierarchies in spatial data model and data definition . Due to this limitation , data layer stage and object class stage are integrated. And ISCO(the is-computer -of relationships) mechanism is mainly used to develop the objects of digital topogrpahic maps, which is implemented with spatial primitive classes. the designed objects are coded with JAVA and then testified in web interface.

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Development of a Simultaneous Detection and Quantification Method of Anorectics in Human Urine Using GC-MS and its Application to Legal Cases (GC-MS를 이용한 사람 뇨시료 중 비만치료제 분석 및 비만치료제 남용 현황의 법과학적 고찰)

  • Choi, Hyeyoung;Lee, Jaesin;Jang, Moonhee;Yang, Wonkyung;Kim, Eunmi;Choi, Hwakyung
    • YAKHAK HOEJI
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    • v.57 no.6
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    • pp.420-425
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    • 2013
  • Phentermine (PT) and phenmetrazine (PM) have been widely used as anti-obesity drugs. These drugs should be used with caution due to its close relation to amphetamine in its structure and toxicity. PT and PM, amphetamine-type anorectics, have recently been considered as alternatives for methamphetamine abuse in Korea. In addition, the misuse and abuse of PT and PM obtained by illegal sources such as the internet become a serious social problem. In the present study, a simultaneous detection and quantification method for determining PT and PM in human urine was developed and validated according to the international guidelines. The urine samples were screened using a fluorescence polarization immunooassay and analyzed by gas chromatography mass spectrometry (GC-MS) after extraction using automatic solid phase extraction (SPE) with a mixed-mode cation exchange cartridge and derivatization with pentafluoropropionic anhydride (PFPA). The validation results for selectivity, linearity, limits of detection (LOD) and quantification (LOQ), intra- and inter-assay precision and accuracy and recovery were satisfactory. The validated method was successfully applied to authentic urine samples collected from 38 drug abuse suspects. PT and/or PM were identified with or without methamphetamine in urine samples. Abuse of PT and PM have increased continuously in Korea, therefore, closer supervision of the inappropriate use of anoretics is necessary.

A Study on RAMS Parameters in the Procurement Requirement for Rolling Stock (철도차량의 구매 요구사항에 포함되는 RAMS 특성값에 관한 연구)

  • Chung, In-Soo;Lee, Kang-Won;Kim, Jong-Woon
    • Journal of the Korean Society for Railway
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    • v.11 no.4
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    • pp.371-377
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    • 2008
  • As a railway is receiving attention as an environment-friendly transportation mode, many high speed, inter-city and urban railway are constructed and remodeled in the world. With this trend, railway RAMS was included in the international standard IEC 62278 in 2002. RAMS activity in domestic market is also increased with this international trend. However, IEC 62278 does not describe the methodology of substantial contents like how reliability target is set although it can be used as an overall guideline when RAMS requirements are included in the purchase specification. That is because RAMS requirements should be set with the specific railway condition. It is required to fully understand the meaning of railway RAMS parameters and apply those correspond to the specific railway system and environment condition especially when a quantitative RAMS requirement is set. In this study, the meaning and characteristics of RAMS parameters applicable to the development of quantitative RAMS requirement of rolling stock is described. And the basic concept of RAMS and the definition of failure that IEC 62278 describes is modified and suggested in order to make more suitable to the development of quantitative RAMS requirement.

A Novel Channel Compensation and Equalization scheme for an OFDM Based Modem (OFDM 전송시스템의 새로운 채널 보상 및 등화 기법)

  • Seo, Jung-Hyun;Lee, Hyun;Cheong, Cha-Keon;Cho, Kyoung-Rok
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.28 no.12A
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    • pp.1009-1018
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    • 2003
  • A new fading channel estimation technique is proposed for an OFDM based modem In the ITS system. The algorithm is based on the transfer function extraction of the channel using the pilot signals and compensated the channel preceding the equalization. The newly derived algorithm is division-free arithmetic operations allows the faster circuit operation and the smaller circuit size. Proposed techniques compensate firstly the distortion which is generated at fading channels and secondly eliminate inter-symbol interference. All algorithms are suitability estimated and improved for a system implementation using digital circuits. As the results, the circuit size is reduced by 20% of the conventional design and achieved about 10% performance improvement at low SNR under 10dB in case of ITS system adapted 16-QAM mode.

A Study of Shorted-Turn Detection in the Cylindrical Synchronous Generator Rotor Windings via Discrete Wavelet Transform (이산 웨이브렛 변환을 이용한 동기발전기 회전자 층간단락 진단에 관한 연구)

  • Kim, Jang-Mok;Kim, Young-Jun;Ahan, Jin-Woo;Kim, Heung-Geun;Jung, Tae-Uk
    • The Transactions of the Korean Institute of Power Electronics
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    • v.11 no.6
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    • pp.570-576
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    • 2006
  • This paper describes a method for the detection of shorted-turn in the cylindrical synchronous generator rotor windings based on the discrete wavelet transform. Multi-resolution analysis(MRA) based on discrete wavelet transform provides a set of decomposed signals in independent frequency bands, which contain independent dynamic information due to the orthogonality of wavelet function. In the proposed method, shorted-turn detection in rotor windings is based on the decomposition of the rotor currents, where wavelet coefficients of these signals have been extracted. Comparing these extracted coefficients is used for diagnosing the healthy machine from faulty machine. Experimental results are presented for healthy, and machines with 25%, 42%, 67%, 83%, 99% inter-turn short circuits in a rotor slot. Deviation of wavelet coefficients in healthy mode from faulty modes depicts the inverse proportion of shorted-turns. Experimental results show the effectiveness of the proposed method for shorted-turn detection in the cylindrical synchronous generator rotor windings.

An Efficient Data Dissemination Protocol for Cluster-based Wireless Sensor Networks (클러스터 기반의 무선 센서네트워크에서 통신량을 줄인 데이터 보급방법)

  • Cho, Ji-Eun;Choe, Jong-Won
    • Journal of KIISE:Information Networking
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    • v.36 no.3
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    • pp.222-230
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    • 2009
  • A sensor network is an important element of the ubiquitous and it consists of sensor fields that contain sensor nodes and sink nodes that collect data from sensor nodes. Since each sensor node has limited resources, one of the important issues covered in the past sensor network studies has been maximizing the usage of limited energy to extend network lifetime. However, most studies have only considered fixed sink nodes, which created various problems for cases with multiple mobile sink nodes. Accordingly, while maintaining routes to mobile sink nodes, this study aims to deploy the hybrid communication mode that combines single and multi-hop modes for intra-cluster and inter-cluster transmission to resolve the problem of failed data transmission to mobile sink nodes caused by disconnected routes. Furthermore, a 2-level hierarchical routing protocol was used to reduce the number of sensor nodes participating in data transmission, and cross-shape trajectory forwarding was employed in packet transmission to provide an efficient data dissemination method.