• Title/Summary/Keyword: inorganic powder

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Fabrication and Magnetic Properties of A New Fe-based Amorphous Compound Powder Cores

  • Xiangyue, Wang;Feng, Guo;Caowei, Lu;Zhichao, Lu;Deren, Li;Shaoxiong, Zhou
    • Journal of Magnetics
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    • v.16 no.3
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    • pp.318-321
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    • 2011
  • A new Fe-based amorphous compound powder was prepared from Fe-Si-B amorphous powder by crushing amorphous ribbons as the first magnetic component and Fe-Cr-Mo metallic glassy powder by water atomization as the second magnetic component. Subsequently by adding organic and inorganic binders to the compound powder and cold pressing, the new Fe-based amorphous compound powder cores were fabricated. This new Fe-based amorphous compound powder cores combine the superior DC-Bias properties and the excellent core loss. The core loss of 500 kW/$m^3$ at $B_m$ = 0.1T and f = 100 kHz was obtained When the mass ratio of FeSiB/FeCrMo equals 3:2, and meanwhile the DC-bias properties of the new Fe-based amorphous compound powder cores just decreased by 10% compared with that of the FeSiB powder cores. In addition, with the increasing of the content of the FeCrMo metallic glassy powder, the core loss tends to decrease.

Characterization of Spray-Dried Yttrium Aluminum Garnet Powder

  • Sim, S.M.
    • The Korean Journal of Ceramics
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    • v.1 no.1
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    • pp.35-39
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    • 1995
  • Yttrium aluminum garnet(YAG) powders were synthesized by spray-drying of the hydroxides coprecipitated from a mixture of aqueous solutions of $Al(NO_3)_3.9H_2O \;and\; Y(NO_3)_3.6H_2O$ Phase formation in the powders during heat treatments and their sintering charactristics were investigated. In the powder obtained by washing the hydroxides before spray-drying, a metastable yttrium aluminum hexagonal (YAH) phase was first crystallized and then transformed into YAG as temperature was increased. The formation of YAH was attributed to a deviation in compositions of the particles from the starting composition of YAG. However, the powder prepared without washing step contained a stable yttrium aluminum monoclinic(YAM) phase in addition to YAG due to a large deviation from the starting composition. A powder compact of a single phase YAG was pressureless-sintered for 4 hrs at $1700^{\circ}C$ and the density was 93% of the theoretical density.

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Preparation of Porous Glass by the Sintering (소결법에 의한 다공질유리의 제조)

  • 박용완;이준영
    • Journal of the Korean Ceramic Society
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    • v.31 no.9
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    • pp.957-968
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    • 1994
  • Manufacturing process of porous glass by the filler method was studied. Commercial soda-lime-silicate glass powder was mixed with inorganic salt as the filler such as KCl, K2SO4, Na2SO4. Sintering shrinkages of mixed powders with the variation of sintering temperature were compared, and the effects of the fillers to shrinkages of mixed powder were increased in the order of Na2SO4${\mu}{\textrm}{m}$ of pore diameter were manufactured when the filler sizes 100~200 ${\mu}{\textrm}{m}$. The open pore volume of porous glass is determined by the quantity of filler and porous glasses having open pore volume between 30 and 70 vol% are available. Available sintering temperature range for preparation of porous glass is from the softening temperature of the glass powder to eutectic melting temperature of DTA curve of mixed powder.

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Studies on the Physico-chemical Components of Elephant-foot Produced in Korea (한국산 구약감자의 이화학적 성분조사)

  • Rhee, Seong-Kap
    • Journal of the Korean Society of Food Culture
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    • v.10 no.5
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    • pp.443-448
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    • 1995
  • Korean fresh elephant-foot (Amorphophalus konjak K. Koch) and its powder were analyzed and compared with foreign samples to investigate the physico-chemical characteristics of Korean konjak. The Korean fresh konjak contained 80.6% of moisture content and most of the solid component comprises much of sugar, protein and trace of fat and fibre. The mannan content of Korean konjak powder is far smaller than those of Japanese and Chinese konjak powder. The analysis of the Korean konjak revealed that glutamic acid, aspartic acid and arginine included 45% of total amount, and other amino acid was incresaed with the order of valine, serine, leucine and glycine. The Korean konjak contained a moderate amount of K component and other inorganic component was larger with the order of P, Na and Ca. The yield of refined powder obtained from dried chip of Konjak was 61.0% in Korean one and 57.5% in Chinese one. The degree of lightness of Chinese konjak powder was slightly higher than that of Korean product, but the difference could not be recognized by naked eye.

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Effects of Organic Binder and Film Thickness on Optoelectrical Properties of AC Powder EL Devices Prepared by Screen Printing Method for LCD Backlight Applications (LCD 백라이트를 위해 스크린 프린팅법으로 제조된 AC Powder EL 소자의 유기결합제와 막두께가 광전기적 성질에 미치는 영향)

  • Lee, Kang-Ryeol;Park, Sung
    • Journal of the Korean Ceramic Society
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    • v.38 no.12
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    • pp.1085-1092
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    • 2001
  • The high efficient AC powder EL devices classified by low cost and low power consumption type fabricated using screen printing method with film thickness and organic binder. Brightness and current density were measured at frequency range of 400Hz∼1kHz and voltage range of 50∼300V$\_$rms/ to estimate optoelectrical properties of AC powder EL devices, respectively. Frequency generator was used as system producing frequency and voltage of a sine wave. Also brightness and current density were measured by luminometer and multimeter. In the case of low cost type AC powder EL device, brightness and current density were about 43 cd/m$^2$and 20$\mu$A/cm$^2$when the thickness of phosphor and dielectric layer was 45∼50$\mu$m under no addition of plasticizer respectively. In the case of low power consumption type AC powder EL device, brightness and current density were about 74 cd/m$^2$and 30∼40$\mu$A/cm$^2$when the thickness of phosphor and dielectric layer was 45∼50$\mu$m and 15∼20$\mu$m under addition of 15wt% plasticizer respectively. Also, AC powder EL device fabricated in this study showed absolutely excellent characteristics as the lifetime was longer than products of other company.

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Effects of SiC Particle Size and Inorganic Binder on Heat Insulation of Fumed Silica-based Heat Insulation Plates

  • Jo, Hye Youn;Oh, Su Jung;Kim, Mi Na;Lim, Hyung Mi;Lee, Seung-Ho
    • Journal of the Korean Ceramic Society
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    • v.53 no.4
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    • pp.386-392
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    • 2016
  • Heat insulation plates of fumed silica were prepared by mixing fumed silica, SiC powder and chopped glass fiber by a high speed mixer followed by pressing of the mixture powder in a stainless steel mold of $100{\times}100mm$. Composition of the plates, particle size of SiC, and type of inorganic binder were varied for observation of their contribution to heat insulation of the plate. The plate was installed on the upper portion of an electric furnace the inside temperature of which was maintained at $400^{\circ}C$ and $600^{\circ}C$, for investigation of heat transfer through the plate from inside of the electric furnace to outside atmosphere. Surface temperatures were measured in real time using a thermographic camera. The particle size of SiC was varied in the range of $1.3{\sim}17.5{\mu}m$ and the insulation was found to be most excellent when SiC of $2.2{\mu}m$ was incorporated. When the size of SiC was smaller or larger than $2.2{\mu}m$, the heat insulation effect was decreased. Inorganic binders of alkali silicate and phosphate were tested and the phosphate was found to maintain the heat insulation property while increasing mechanical properties.

Development of an Oraganic-Inorganic Hybrid Coating Solution for Improvement in Flame Retardant Properties of Wallpapers (벽지의 방염특성을 개선하기 위한 유-무기 하이브리드 코팅 용액 개발)

  • Jeong, Gyu Jin;Kang, Tae Wook;Kim, Jin Ho;Kim, Bong Man;Seo, Eun Kyung;Bae, Byungseo;Kim, Sun Woog
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.2
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    • pp.178-183
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    • 2022
  • For enhancing the flame-retardant properties of wallpapers, we developed an organic-inorganic hybrid solution with ZrSiO4 as a functional ceramic powder, coated on non-woven fabric using dip coating, spray coating, and slot-die coating methods. Their flame retardant properties were characterized by a 45° combustion tester, which is manufactured according to the flame-retardant performance standard (KOFEIS 1001 and KS F 2819). In organic-inorganic hybrid solution, with increasing the concentration of acid-catalyst (acetic acid), the precipitation of ZrSiO4 powders increased, and the flame retardant properties decreased. The highest flame retardant result was obtained for the solution adding 5 wt% acetic acid. The optimization of the coating method and coating number resulted in the most excellent flame-retardant properties being obtained for the non-woven fabric coated for 5 or 7 times by dip coating method, and their flame-retardant properties corresponded to class 2 flame-retardant performance of wallpapers.

Strength Properties of Recycled Concrete Containing Water-redispersible Copolymer Powder (재유화형분말수지를 혼입한 재생콘크리트의 강도 특성)

  • Kim, In-Su;Sung, Chan-Yong
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2005.10a
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    • pp.128-134
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    • 2005
  • This study was performed to evaluate the strength and durability properties of recycled concrete containing water - redispersible copolymer powder(WRP) and blast furnace slag powder(BSP) [RCWS]. Material used were cemente, recycled coarse aggregare, natural fine aggregate, water-redispersible copolymer powder, blast-furnace slag powder. Especially, Water-redispersible powder was used for blending with Inorganic binders such as cemente, gypsum and hydrated lime etc. First of all, Mixed ratio method of RCWS made Two Type. One was called type-1 which used to BSP content 5% and WRP(Water-redispersible powder) content 0%, 1%, 2%, 3%, 4%, 5%, 6%. respectively. Another was called Type-2 which used to BSP(blast furnace slag powder)content 10% and WRP(Water-redispersible powder) content 0%, 1%, 2%, 3%, 4%, 5%, 6%. respectively. According to the experimental results of (RCWS), Incase Type-2 at curing age 28days, Compressive strength, pulse velocity and dynamic modulous of elasticity were shown higher than Type-1 and The more WRP content increasing($0%{\sim}6%$) was the lower Compressive strength, Pulse velocity and Dynamic modulous of elasticity. Water absorption ratio was in the range of $3.85%\;{\sim}\;3.23%$, it was almost equal to Type-1, 2 but Increasing the WRP content($0%{\sim}6%$), The water absorption ratio is decreased.

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The Synthesis of High-purity Zirconia Powders and Its Properties (Compaction and Sintering Behaviro as a Function of Granulation Methods) (고순도 지르코니아 분말의 합성 및 그 특성 (조립방법에 따른 성형 및 소결 특성))

  • Kim, Hwan;Lee, Jong-Kook;Kim, Ju-Young;Hwang, Kyu-Hong
    • Journal of the Korean Ceramic Society
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    • v.25 no.4
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    • pp.357-363
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    • 1988
  • Ccompaction and sintering behavior of highly pure PSZ powders were investigated by laying the stress on the granulation processes. The particle size of coprecipitated PSZ powder was so fine that the agglomeration was severely formed during drying and calcing step and by this agglomeration differential sinering was occurred. The methanol dispersion of precipitates was the good method of avoiding severe agglomeration formed during drying process because of small surface tension than water. But perfect deagglomeraton was not possible due to high surface area of powders. So homogenization by granulation was needed, and among the method spray granulation was the most desirable to obtain homogeneous compacts and subsequent flaw-free ceramics.

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Fabrication of Duplex Ceramic Composites by Organic-Inorganic Solution Process

  • Lee, Sang-Jin;Kim, Youn-Cheol
    • Journal of the Korean Ceramic Society
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    • v.40 no.9
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    • pp.837-841
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    • 2003
  • Duplex microstructure of zirconia and alumina has been achieved via an organic-inorganic solution technique. Zirconium 2,4-pentanedionate, aluminum nitrate and polyethylene glycol were dissolved in ethyl alcohol without any precipitation. The organicinorganic precursor gels were turned to porous powders having volume expansion through explosive, exothermic reaction during drying process. The volume expansion was caused by abrupt decomposition of the organic groups in the gels during the vigorous exothermic reaction. The volume expanded, porous powders were crystallized and densified at 1500$^{\circ}C$ for 1 h. At the optimum amount of the PEG polymer, the metal cations were well dispersed in the solution and a homogeneous polymeric network was formed. The polymer content also affected on the specific surface area of the synthesized powder and the grain size of the sintered composite.