• Proceedings of the Korean Institute of Resources Recycling Conference
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• 2004.05a
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• pp.98-102
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• 2004

반도체 산업용 실리콘 잉곳의 절단공정에서 발생하는 폐슬러지 중에는 고순도의 실리콘이 함유되어 있으며, 이 슬러지로부터 분리, 회수한 Si로부터 실리콘화합물 합성하였다. 고비점의 potasium alkoxide 촉매 존재하에서 금속 실리콘과 에탄을 혹은 메탄올과 같은 알코올과의 고액반응에 의해 알콕시 실란을 합성할 수가 있었다 알콕시 실란을 합성반응속도는 반응온도에 크게 의존하였고 최적반응 온도는 $180^{\circ}C{\sim}195^{\circ}C$ 정도이었다. 촉매 첨가량에 따라 알콕시 실란의 반응율이 달라졌으며, 알콕시 실란의 반응율은 최고 90%로 높은 값을 나타내었다.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1996.05a
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• pp.99-101
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• 1996

This paper is concerned with the fabrication of (Fe,Co)-Si-B amorphous magneto-strictive wire which attracts strong attention as a new sensor material. First, we put the ingot of (Fe$\sub$1-x/Co$\sub$x/)$\sub$77/Si$\sub$8/B$\sub$15/ composition into quartz tube. Then, under the condition of 400MHz and 8kW, we melt and mix the in-got in the high frequency induction furnance. After that, we obtain the magnetostrictive wire of 100∼150$\mu\textrm{m}$ in diameter by injection and rapid quenching within the high rotating water. Finally, we find that the wire is under the amorphous state.

• Journal of Korea Foundry Society
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• v.13 no.1
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• pp.81-93
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• 1993

It is well-known that the analysis of elasto-plastic thermal stress and deformation are substantially important in optimal design of metal casting mould. The unsteady state thermal stress and deformation generated during the solidification process of ingot and mould have been analyzed by two dimensional thermal elasto-plastic theories. Distributions of temperature, stress and relative displacement of the mould are calculated by the finite element method and compared with experimental results. In the elasto-plastic thermal stress analysis, compressive stress occurred at the inside wall of the mould whereas tensile stress occurred at outside wall. A coincidence between the analytical and experimental results is found to be fairly good, showing that the proposed analytical method is reliable.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.10a
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• pp.333-337
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• 2004

Steam Generator is one of the most important structural part of nuclear power plant. It is manufactured by various steel forgings such as shell, head, torus and tubesheet. These steel forgings have been made by open die forging process. After steel melting and ingot making, open die forging has been carried out to get a good quality which means high soundness and homogeniety of the steel forgings by using high capacity hydraulic press. This paper introduced the open die forging process and manufacturing experience of large tubesheet forgings which will be used for the steam generator of 1,400MW nuclear power plant.

• Proceedings of the KIEE Conference
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• 1990.07a
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• pp.231-235
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• 1990

Soft magnetic silicon steels containing up to 6.5wt% of silicon were prepared by powder metallurgical processing and their magnetic properties were evaluated. The magnetic properties of P/M silicon steels are similarly affected by the silicon addition as those of conventional ingot processed ones but are also significantly affected by density and interstitial impurities particularly oxygen content. Magnetic flux density, $B_{10}$ and coercivity, Hc, tends to decrease with silicon content whereas maximum permeability, ${\mu}m$, decreases first and then increases rapidly above 5 wt% silicon. Increasing density also increases magnetic flux density and maximum permeability but reduces coereivity. The latter two properties are, however, affected more strongly with oxygen content.

• Transactions of Materials Processing
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• v.18 no.6
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• pp.458-464
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• 2009

Thermal energy control is a important factor to control properties of large sized product in ingot-forging. Good control of thermal energy helps to increase characteristics and eliminate defects of large cast-forged part, such as large sized forged shell. We have studied about not only large size ring forging process and after heat treatment process by FEM simulation. Changes of temperature and microstructure for forged shell were predicted according to different heat treatment conditions. Therefore, we can choose the proper heat treatment condition by FEA. The sectional properties confirmed by practical experiment and evaluation have presented possibilities of process design by computational analysis.

• Journal of the Korean Vacuum Society
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• v.3 no.3
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• pp.346-354
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• 1994

삼원화합물 반도체 CuAlSe2 및 CuGaSe2 단결정의 solid solution 인 CuAl1-xGaxSe2 및 cobalt를 2.0 mol% 첨가한 CuAl1-xGaxSe2 : Co2+ 단결정을 iodine을 수송물질로 사용한 화학수송법으로 성장시켰 다. source material로는 CuAl1-xGaxSe2 의 화학조성비에서 Se를 3.0mol% 과잉으로 첨가하여 합성한 ingot를 사용하였으며 불순물이 첨가된 CuAl1-xGaxSe2:Co2+ 단결정성장시에는 source ma-terial 에 cobalt 분말을 2.0mol% 첨가하였다. X-선 회절무늬로부터 성장된 단결정들이 chalcopyrite 결정구조를 하고 있음을 확인하였으며 격자상수를 구하였다. 광흡수 spectra 측정으로부터 성장된 단결정에서 나타 는 cobalt 불순물에 의한 광흡수 peak가 Td 대칭점에위치한 Co2+ 이온의 에너지 준위들간 전자전이에 의해 나타남을 규명하였다.

• Korean Journal of Materials Research
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• v.16 no.2
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• pp.75-79
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• 2006

The effect of ozone and/or ultrasound treatments on the efficiency of slurry removal in post sliced cleaning (PSC) of silicon ingot was studied. Efficiency of slurry removal was evaluated as functions of time, temperature and surfactant with DOE (Design of Experiment) method. Residual slurries were observed on the wafer surface in case of cleaning by ozone or ultrasound separately. However, a clean wafer surface was appeared when cleaned with ozone and ultrasound simultaneously. It has found that cleaning time was the main effect among temperature, time and surfactant. Elevated temperature, addition of surfactant and high ozone concentration helped to accelerate efficient removal of slurry. The improvement of removal efficiency seems to be related to the formation of more active OH radicals. The highly cleaned surface was achieved at 10 wt% ozone, 1 min and 10 vol% surfactant with ultrasound. Application of ozone and ultrasound might be a useful method for PSC process in wafer cleaning.

• Journal of Korea Foundry Society
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• v.21 no.4
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• pp.246-252
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• 2001

Variation in the microstructure of Mg-5%Al semi-solid slurry during isothermal heating was investigated in relation to initial microstructure, holding time, and holding temperature. Specimens with three different initial microstructures were isothermally heated. Dendritic structure in as-cast ingot was decomposed into solid globules in the semi-solid slurry during isothermal holding, while in the recrystallized specimens prepared by extrusion or rolling the size of solid particles was continuously increased during the heating. Effects of mold temperature and liquid fraction of slurry on the mold filling ability were also studied. Very thin section (0.4 mm) could be successfully filled up to 50 mm by 60% liquid slurry when the mold was heated to $600^{\circ}C$.

• Journal of Korea Foundry Society
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• v.22 no.6
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• pp.293-298
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• 2002

The effects of alloying elements added on the microstructure and high temperature oxidation behavior of the electro-slag remelted Fe-22Cr-5Al alloy were investigated. The amount of casting defect was makedly reduced by the electro-slag remelting. The electro-slag remelted ingot had a directionally solidified structure and cleaner surface than that of air-melted one. The high temperature oxidation reststance was greatly improved by the addition of Be and Zr.