• 제목/요약/키워드: in-situ processing

검색결과 187건 처리시간 0.025초

Changing PEO coating formation on Mg alloys by particle additions to the treatment electrolyte

  • Blawert, Carsten;Srinivasan, Bala;Liang, Jun;Huang, Yuanding;Hoche, Daniel;Scharnagl, Nico;Heitmann, Volker;Burmester, Ulrich
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2012년도 추계총회 및 학술대회 논문집
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    • pp.7-11
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    • 2012
  • Plasma electrolytic oxidation of magnesium alloys is a well known technique to produce corrosion and wear resistant coatings. The addition of particles to the electrolyte provides a possibility to produce coatings with an increasing range of composition by in-situ incorporation of those particles into the coating. An extensive literature review has revealed that the mode of incorporation depends mainly on the melting point of the used particles and the energy provided by the discharges of the PEO process. The spectrum ranges from inert to partly reactive incorporation, but a complete reactive incorporation and a formation of a new single phase coating was not observed so far. Thus a new approach in PEO processing is introduced using specific particles as a kind of sintering additive, changing not only the composition but lowering the melting temperature and increase the liquid phase fraction during the discharges, resulting in a new amorphous coating.

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$CeO_{2}/BaTiO_{3}$ 이중완충막을 이용한 YBCO 박막 제작 (Fabrication of YBCO superconducting film with $CeO_{2}/BaTiO_{3}$double buffer layer)

  • 김성민;이상렬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.790-793
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    • 2000
  • We have fabricated good quality superconducting YBa$_2$Cu$_3$$O_{7-x}$(YBCO) thin films on Hastelloy(Ni-Cr-Mo alloys) metallic substrates with CeO$_2$and BaTiO$_3$buffer layers in-situ by pulsed laser deposition in a multi-target processing chamber. YBCO film with CeO$_2$ single buffer layer shows T$_{c}$ of 71.64 K and the grain size less than 0.1 ${\mu}{\textrm}{m}$. When BaTiO$_3$is used as a single buffer layer, the grain size of YBCO is observed to be larger than that of YBCO/CeO$_2$by 200 times and the transition temperature of the film is enhanced to be about 84 K. CeO$_2$/BaTiO$_3$double buffer layer has been adopted to enhance the superconducting properties, which results in the enhancement of the critical temperature and the critical current density to be about 85 K and 8.4 $\times$ 10$^4$ A/cm$^2$ at 77 K, respectively mainly due to the enlargement of the grain size of YBCO film.ilm.

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$CeO_2$/$BaTiO_3$이중완충막을 이용한 YBCO 박막 제작 (Fabrication of YBCO Superconducting Film with $CeO_2$/$BaTiO_3$Double Buffer Layer)

  • 김성민;이상렬
    • 한국전기전자재료학회논문지
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    • 제13권11호
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    • pp.959-962
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    • 2000
  • We have fabricated good quality superconducting YBa$_2$Cu$_3$$O_{7-x}$(YBCO) thin films on Hastelloy(Ni-Cr-Mo alloys) metallic substrates with CeO$_2$and BaTiO$_3$buffer layers in-situ by pulsed laser deposition in a multi-target processing chamber. YBCO film with CeO$_2$single buffer layer shows T$_{c}$ of 71.64 K and the grain size less than 0.1${\mu}{\textrm}{m}$. When BaTiO$_3$ is used as a single buffer layer, the grain size of YBCO is observed to be larger than that of YBCO/CeO$_2$by 200 times and the transition temperature of the film is enhanced to be about 84 K. CeO$_2$/BaTiO$_3$double buffer layer has been adopted to enhance the superconducting properties, which results in the enhancement of the critical temperature and the critical current density to be about 85 K and 8.4$\times$10$^4$ A/$\textrm{cm}^2$ at 77 K, respectively mainly due to the enlargement of the grain size of YBCO film.ilm.

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복사전달모델을 이용한 KOMPSAT-3A 중적외선 데이터의 복사보정계수 산출: 탐구적 사례 (Derivation of Radiometric Calibration Coefficients for KOMPSAT-3A Mid-wave Infrared Data Using a Radiative Transfer Model: An Exploratory Example)

  • 김용승
    • 대한원격탐사학회지
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    • 제36권6_2호
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    • pp.1629-1634
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    • 2020
  • 위성데이터 처리과정에서 지표온도와 같은 지구물리변수를 산출하려면 위성에서 관측한 수치 값(Digital Number, DN)을 물리적 변수인 복사량(Radiance)으로 변환시키는 과정이 필수적이다. 본 연구의 목적은 위성발사 전에 실험실 측정치로 수립된 DN·Radiance 관계식을 KOMPSAT-3A 중적외선 데이터와 MODTRAN 복사전달모델을 이용하여 개선하는데 있다. 연구결과는 개선된 DN Radiance 관계식이 현실적인 복사량 값을 제공할 수 있음을 보였다. 후속연구에서는 이들 복사량에 대해 지상관측과 복사전달모델을 이용해 보다 정량적인 검증이 이루어지기를 기대한다.

Wet Foam Stability from Colloidal Suspension to Porous Ceramics: A Review

  • Kim, Ik Jin;Park, Jung Gyu;Han, Young Han;Kim, Suk Young;Shackelford, James F.
    • 한국세라믹학회지
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    • 제56권3호
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    • pp.211-232
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    • 2019
  • Porous ceramics are promising materials for a number of functional and structural applications that include thermal insulation, filters, bio-scaffolds for tissue engineering, and preforms for composite fabrication. These applications take advantage of the special characteristics of porous ceramics, such as low thermal mass, low thermal conductivity, high surface area, controlled permeability, and low density. In this review, we emphasize the direct foaming method, a simple and versatile approach that allows the fabrication of porous ceramics with tailored microstructure, along with distinctive properties. The wet foam stability is achieved under the controlled addition of amphiphiles to the colloidal suspension, which induce in situ hydrophobization, allowing the wet foam to resist coarsening and Ostwald ripening upon drying and sintering. Different components, like contact angle, adsorption free energy, air content, bubble size, and Laplace pressure, play vital roles in the stabilization of the particle stabilized wet foam to the porous ceramics. The mechanical behavior of the load-displacements curves of sintered samples was investigated using Herzian indentations testes. From the collected results, we found that microporous structures with pore sizes from 30 ㎛ to 570 ㎛ and the porosity within the range from 70% to 85%.

Enzymatic Extraction of Lemon Pectin by Endo-Polygalacturonase from Aspergillus niger

  • Contreras-Esquivel, Juan C.;Voget, Claudio E.;Vita, Carolina E.;Espinoza-Perez, J.D.;Renard, Catherine M.G.C.
    • Food Science and Biotechnology
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    • 제15권2호
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    • pp.163-167
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    • 2006
  • Pectin was enzymatically extracted from industrial lemon pomace by using an endo-polygalacturonase from Aspergillus niger as a processing aid and compared to pectin extraction by hot hydrochloric acid. The yield of pectin was 17.6 and 20.2% with enzymatic and acidic treatments, respectively. The molecular weight distribution did not vary greatly between the samples extracted with enzyme or acid. Large differences in charge density were observed, however, when the samples were analyzed by anionic-exchange chromatography. Pectin extracted by the enzymatic treatment indicated higher charge density than that obtained by hydrochloric acid. The higher charge density could due to the presence of endogenous lemon pectinesterase, which was activated at low pH 4.5 in situ conditions during the process of enzymatic extraction, leading to low methoxylated pectin with a higher charge density.

네트워크에 기반한 MT자료의 처리기술 개발 연구 (Development of Network Based MT Data Processing System)

  • 이희순;권병두;정호준;오석훈
    • 지구물리와물리탐사
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    • 제3권2호
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    • pp.53-60
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    • 2000
  • 본 연구에서는 급격히 증가하는 인터넷망 및 분산(distribution) 컴퓨팅 환경을 이용한 서버/클라이언트(server/client) MT자료 처리 시스템의 구축을 위한 여러 가지 기술적 사항에 대해 논의하였다. 이러한 시스템은 표준적인 처리 방식의 도입과 인증된 자료 처리 서버에서의 해석 수행을 통해 일관성과 안정성을 동시에 제공할 수 있을 것이다. 또한 인터넷망을 이용하여 현장에서의 자료해석이 가능해지므로 탐사 시간, 경비의 감소 및 추가 탐사 계획 수립에도 도움을 줄 것이다. 각종 자바 기술(pure java와 enterprised java)은 네트워크 프로그램을 손쉽게 개발할 수 있는 많은 방법들을 제공한다. 본 연구에서는 이를 이용하여 웹(web)에 의한 서버/클라이언트 모델과, 소켓(Socket) 및 원격 함수 호출(RMI: Remote Method Invocation) 에 의한 처리 기법을 MT자료의 해석에 적용하기 위한 방법에 대해 논하였다. 또한 MT자료의 특성상, 그 해석은 고성능의 컴퓨터를 이용하였을 때에도 상당한 시간을 필요로 하므로 이를 극복하기 위해 서버 프로그램에 MPI(Message Passing Interface) 병렬처리 기술을 적용하고자 한다. 이는 고가의 병렬 처리 컴퓨터를 대체할 수 있으며, 표준적인 코딩이 제시되었으므로 관리 및 유지, 보수에 있어 효율성을 제공할 것이다.

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액정 폴리에스테르와 Poly(butylene terephthalate)의 에스테르 교환반응 (Transesterification Reaction between Liquid Crystalline Polyester and Poly(butylene terephthalate))

  • 한도수;김두화;조성동;조병욱
    • 대한화학회지
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    • 제41권3호
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    • pp.157-165
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    • 1997
  • 에스테르 교환반응은 고분자 블랜드의 가공시 자체 상용화제를 만들 수 있어 폴리에스테르의 공업적제조에 이용되어질 수 있다. 따라서 에스테르 교환반응에 대한 연구의 일환으로서 열방성 액정고분자인 TR-4,6(poly(tetramethylene-4,4'-terephthaloyldioxydibenzoate-co-hexametylene-4,4'-terephthaloyldioxydibenzoate)를 합성하게 되었으며 이것을 엔지니어링 플라스틱인 폴리부틸렌테레프탈레이트(PBT)와 블랜딩을 하였다. 이 두 구성고분자 사이의 에스테르 교환반응은 IR, DSC, 및 $^{13}C-NMR$에 의한 통계적 처리방법에 의하여 분석하였으며, 교환반응 진행속도와 모노머의 반복단위 서열분포도 조사 연구하였다.

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Ru/$RuO_2$ 금속/산화물 이중전극 위에 증착한 PZT 박막의 전기적 특성 (Electrical Properties of PZT Thin Films Deposited on the Ru/$RuO_2$ Metal/Oxide Hybrid Electrodes)

  • 정규원;박영;송준태
    • 한국전기전자재료학회논문지
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    • 제14권4호
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    • pp.281-288
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    • 2001
  • PZT thin films (3500$\AA$) have been prepard on the Ru/Ru $O_2$ and Ru $O_2$ bottom electrodes with a RF magnetron sputtering system using P $b_{1.05}$(Z $r_{0.52}$, $Ti_{0.48}$) $O_3$ ceramic target. Ru/Ru $O_2$ bottom electrode was fabricated by in-situ processing controlled the $O_2$ partial pressure. The PZT thin films deposited on the Ru/Ru $O_2$ bottom electrode were preferred oriented (101) plane. The PZT thin films deposited on the Ru/Ru $O_2$ bottom electrodes showed better electrical properties than those with Ru $O_2$ bottom electrodes because Ru $O_2$ prevented oxygen vacancies and impurities from existing withing the interface and substrate.e.

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Bio-Optical Modeling of Laguna de Bay Waters and Applications to Lake Monitoring Using ASTER Data

  • Paringit, EC.;Nadaoka, K.;Rubio, MCD;Tamura, H.;Blanco, Ariel C.
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2003년도 Proceedings of ACRS 2003 ISRS
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    • pp.667-669
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    • 2003
  • A bio-optical model was developed specific for turbid and shallow waters. Special studies were carried out to estimate absorption and scattering properties as well as backscattering probability of suspended matter. The inversion of bio-optical model allows for direct retrieval of turbidity and chlorophyll- a from the visible-near infrared (VNIR) range sensor. Time-series satellite imagery from ASTER AM-1 sensor, were used to monitor the Laguna de Bay water quality condition. Spatial distribution of temperature for the lake was extracted from the thermal infrared (TIR) sensor. Corresponding field surveys were conducted to parameterize the bio -optical model. In-situ measurements include suspended particle and chlorophyll-a concentrations profiles from nephelometric devices and processing of water samples. Hyperspectral measurements were used to validate results of the bio -optical model and satellite- based estimation. This study provides a theoretical basis and a practical illustration of applying space- based measurements on an operational basis.

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