• 한국표면공학회지
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• 제37권3호
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• pp.137-145
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• 2004

This study surveys the microscopic wear of CVD TiN coatings in repeated sliding, using the SEM Tribosystem as in-situ system. According to the research, the depth of wear groove and the specific wear amount are changed by the transition of the microscopic wear mode. This investigation leads to the fact that the change of wear characteristics produces the transition of the wear mode. In this survey, four modes are observed for CVD TiN coatings with the thickness of 1.6$\mu\textrm{m}$: ploughing, powder formation, flake formation and coating delimitation. The microscopic wear properties is quantitatively evaluated in terms with the microscopic wear mode and the specific wear amount. These relationships prove that the observation of wear modes with a SEM Tribosystem is useful to evaluate wear properties.

• 대한원격탐사학회지
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• 제25권3호
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• pp.243-253
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• 2009

For the last 14 years, space-borne satellite SAR system such as RADARSAT-1, ERS-2, and ENVISAT ASAR have provided a continuous observation over the ocean. However, the data acquired from those systems were limited to C-band frequency until the advent of the first spacebome German X-band SAR system TerraSAR-X in 2007. Korea is also planning to launch the nation's first X-band SAR satellite (KOMPSAT-5) in 2010. It is timely and necessary to develop X-band models for estimating geophysical parameters from these X-band SAR systems. In this study, X-band wind retrieval model was investigated and developed based on numerical ocean scattering model (radar backscattering model and hydrodynamic interaction model). Although these models have not yet been tested and validated for broad ranges of wind conditions, the estimated wind speeds from TerraSAR-X data show generally good agreement with in-situ measurements.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2017년도 춘계학술대회 논문집
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• pp.151.1-151.1
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• 2017

This work studied the corrosion behavior of AZ31 Mg alloy galvanically coupled with Cu during immersion in 0.1 and 0.5 M NaCl solutions by in-situ observation and galvanic corrosion current measurement using a zero resistance ammeter. The corrosion behavior of AZ31 Mg alloy was also studied by salt spray test. The average galvanic corrosion density during 2 h immersion in 0.1 NaCl solution was found to decrease as an exponential function with increasing the surface area ratios between AZ31:Cu or with increasing the distance between AZ31 and Cu. The corrosion of electrodeposited Cu on AZ31 Mg alloy was concentrated at the area next to Cu (about 5 mm for immersion test and 2 mm for salt spray test) and pitting corrosion was accelerated at the area beyond the severely corroded area by the galvanic coupling effect.

• Bulletin of the Korean Chemical Society
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• 제30권5호
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• pp.1097-1100
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• 2009

New types of conducting polyaniline-polymannuronate (PANI-PM) composites were synthesized by in situ deposition techniques in an aqueous media. By dissolving different weight percentage of polymannuronate (PM) (5, 10, 15, and 25%), the oxidative polymerization of aniline was carried out using ammonium per sulfate as an oxidant. The obtained composites were studied for their thermal stability and electrochemical behavior. The thermal stability of PANI-PM composites is lower than PANI, which supports a strong interaction between PANI and PM. However, the composites show an appreciable electrochemical behavior. Based on these observation the PANI-PM composites can be explored in different fields such as electric devices, sensors, functional coatings, etc.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.469-470
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• 2006

[ $TiO_2$ ] nanoparticle was synthesized by the flame method, which was controlled by varying the ratio and flow rate of gas mixtures consisting of oxygen (oxidizer), methane (fuel) and nitrogen (carrier gas). The crystalline phases of $TiO_2$ nanoparticle depended strongly on the temperature distribution in the flame, whereas the morphology was not sensitive. We proved that the anatase phase formed without the phase transformation in the flame and the rutile phase generated through several phase transformations.

• Applied Microscopy
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• 제18권2호
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• pp.167-176
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• 1988

Extrachromosomal circular DNA complexes from erythrocytes and splenocytes isolated from Carassius carassius were examined by mica-press-absorption method. The method was described that released small polydisperse circular DNA molecules in situ from the erythrocytes and the splenocytes and that allows selective observation of the small circular DNA complexes bound to cellular components. The released polydisperse circular DNA complexes were absorbed preferentially on mica in a divalent cation-free medium then processed for electron microscopy. Small circular DNAs showed a heterogeneous size distribution of $2{\sim}10{\mu}m$ with a mean contour length of $4.3{\mu}m$ for the circulating erythrocytes and that of $0.7{\sim}3.6{\mu}m$ with a mean contour of length $2.04{\mu}m$ for the splencytes. Cells contained $100{\sim}300$ copies and $300{\sim}700$ copies obtained from the erythrocytes and the splenocytes, repectively. Possible biological functional implications for size distribution of extrachromosomal circular DNAs are discussed.

• 한국세라믹학회지
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• 제34권12호
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• pp.1235-1239
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• 1997

Sodium niobate single crystals were grown by high temperature solution growth with Na2O/B2O3 flux. The phase transitions and domain structures of sodium niobate were observed using transmission polarizing microscope from room temperature to $650^{\circ}C$. There was imperfect extinction region within as-grown crystals and this area could be removed by heat treatment. The area existed within crystal till 3$65^{\circ}C$, in which temperature the space group of sodium niobate is changed from Pbma to Pmnm. The phase transition from Pbma to Pmnm happened abruptly with changing domain structure. At 48$0^{\circ}C$, 52$0^{\circ}C$ and 572$^{\circ}C$, the colors and walls of domains were changed. All domains disappeared and the space group of sodium niobate was changed from P4/mbm to Pm3m at 64$0^{\circ}C$. When sodium niobate changed from high temperature phase to low temperature phase, the memory effect of domain structure was not observed.

• 한국재료학회지
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• 제17권7호
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• pp.371-375
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• 2007

In-situ observation of electromigration behavior of eutectic SnPb solder was performed as a function of line length at $100^{\circ}C$, $6{\times}10^4A/cm$ condition in a scanning electron microscope chamber. The incubation time for edge drift and the edge drift velocity increase as line length increases, which are discussed with the void nucleation stage of solder bump and the electromigration back flux force, respectively. Finally, the existence of electromigration product (jL) and its line length dependency are also discussed.

• 한국측량학회지
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• 제26권6호
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• pp.625-631
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• 2008

대규모의 토목공사에서 토공량의 확인은 공사비 산정의 적정성 여부와 직결되는 매우 중요한 검토항목 중 하나이다. 이러한 토공량을 정확히 산정하기 위해서는 정밀한 측량이 요구되고 있으나, 대규모 토공공사가 수행되는 시공현장에서는 토털스테이션과 같은 광학식 장비를 사용하여 토공량 확인측량을 실시하므로 관측시간이 과다하게 소요되고 이로 인하여 작업일수가 부족해져 정밀한 측량을 수행하지 못하는 사례가 빈번히 발생하게 되는 것이 현실이다. 이러한 사안은 후일 토공사 시공시 토사 반출입량의 정산문제로 발주자와 시공자간의 분쟁을 야기하는 등 현장에서 많은 문제점을 발생시키게 된다. 본 연구에서는 토털스테이션 등의 기존의 측량방법에 의해 토공량 확인측량을 실시하는 것과는 달리 VRS-RTK 측량기법에 의한 새로운 기법을 채택하여 신속하고 정확한 측량이 가능하도록 하는 기법을 고찰하였다. 본 연구에서 제시한 VRS-RTK 시스템은 소수의 인원으로 원지반의 3차원 좌표를 높은 밀도로 신속하게 관측하는 것이 가능하며, 이 기법은 제한된 시간 내에 정확한 토공량을 산출할 수 있는 가장 경제적인 측량기법 중 하나라는 것을 확인할 수 있었다.

• 한국생물공학회:학술대회논문집
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• 한국생물공학회 2005년도 생물공학의 동향(XVII)
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• pp.860-863
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• 2005

The microcapsules containing fragrant oil as functional material were prepared by in-situ polymerization with prepolymer that was made from melamine-formaldehyde (MF) as wall material of microcapsules. The effects of polymerization variables, such as the nature and concentration of surfactants, stirring rate, and stirring time, on the size and distribution of the particles were investigated. Fourier transform-infrared spectroscopy (FT-IR), thermal analysis, particle size analysis, scanning electron microscopy (SEM) observation were used to investigate the characteristics of microcapsules. Through the FT-IR and SEM analysis, we found that the prepared microcapsules were containing fragrant oil and the shape of particle was spherical. The nature and concentration of surfactants, stirring rate, and stirring time had profound effects on the particle size and particle size distribution.