• Food Science of Animal Resources
• /
• v.22 no.1
• /
• pp.50-54
• /
• 2002

The aim of this work to determine the formation of lactulose during heat treatment process as a contribution to the estabilishment of limits of chemical indicators for different types of heat processed milk and analyze of lactulose for the reconstituted milk added samples. The HTST(75$\^{C}$/15s) and UHT(130$\^{C}$/2∼3s) treatment realized with a pilot plant and heat-treated samples were stroed at 4, 10, 30$\^{C}$ for 4 weeks. Changes in lactulose was evaluated at 7 days intervals. The other heat treatment was sealed in glass tube and heated at 75$\^{C}$ for 10 to 120s and heated at 130$\^{C}$ for 2 to 60s in a thermostatically controlled constant temperature bath of glycerol. The reconstituted milk was made with full fat dry milk that reconstituted with deionized water to 10% total solid, and was added to milk at 10, 20, 30% respectively. The samples processed with a HTST pilot plant showed that lactulose was contained at 1.47∼1.52mg/10()ml and 8.19 ∼8.32mg/100ml for UHT-treated samples. Changes in the lactulose content of heat-treated samples during storage at 4 and 10$\^{C}$ for 4 weeks caused a slight increase, however a noticeable increase was observed at 30$\^{C}$ for 4 week. The glass tube samples showed that high correlations between relative increase in content of lactulose and increasing processing times(75$\^{C}$ : r = 0.986, 130$\^{C}$ : r = 0.987, respectively). Added with reconstituted milk would cause a increase of the lactulose content linear with increasing addition amount(r = 0.982). This results observed for lactulose in commercial milk samples would applied to the detection of chemical changes during heat treatment and illegal use of reconstituted milk.

• Resources Recycling
• /
• v.21 no.1
• /
• pp.17-29
• /
• 2012

potential assessment of converting closed non sanitary landfills into sustainable landfill through the reclamation works(= landfill mining project) of illegal landfill discovered in land development site using Sustainable Landfill Reclamation system(SLR-system) was investigated. The SLR system had treatment capacity of 91.4 $m^3/hr$ (130.61 ton/hr) in condition of 28.0% of water content. Recovery ratio and purity of sorted soil were 98.9% and 99.66%, respectively. Sorted combustibles were 91.8% and 92.0%, respectively. Especially, high heating value (HHV) and low heating value(LHV) of combustibles were 4,282kcal/kg and 3,636 kcal/kg, respectively, in considering the energy content and recovery ratio of combustibles. Therefore, combustibles separated from landfill site have higher value than Fluff RDF standard value(3,500kcal/kg) of MOE. RDF can be produced with combustibles by 84.43%. Averaged size and organic foreign matter content of the sorted soil were less than 035mm and 0.31 %(VN), respectively. In addition, concentration of all contents of hazardous matters containing soils met safety standards. Therefore, it is possible to be recycled as refilling and cover materials to rebuild Sustainable landfills by 98.42%.

• Korean Journal of Food Science and Technology
• /
• v.44 no.2
• /
• pp.148-154
• /
• 2012

It was carried out to detect anti-impotence drug-like compounds, sibutramine and their analogues in dietary supplements, which are doubtful whether they include illegal compounds. A total of 51 food products were bought online and have been investigated. The separation was achieved on a C18 column, with the mobile phase made up of water (5 mM sodium hexanesulfonate and 0.1% phosphoric acid) and 95% acetonitrile, at a flow rate of 1.2 mL/min with gradient elution using by HPLC-DAD. The UV signals were monitored at 220 nm and 291 nm. LC-ESI-tandom MS was utilized to confirm that detected compounds in samples are the same as the reference materials. Two nutrient supplement foods and ginseng products were found to contain 1.3-82.1 mg of sildenafil, dimethylthiolsildenafil and pseudovardenafil per serving size. In addition, two other processed products were detected to contain 1.7 and 2.2 mg of didesmethylsibutramine, derived from sibutramine per serving size.