• Preventive Nutrition and Food Science
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• 제16권1호
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• pp.45-54
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• 2011

Volatile components in commercial pine needle (Pinus densiflora S. and Z.) powder were extracted using simultaneous steam distillation and a solvent extraction (SDE) apparatus, and were analyzed by gas chromatography-mass spectrometry (GC-MS). A total of 230 compounds divided into 13 groups were identified, which included alcohols (42), ketones (39), aldehydes (32), terpenes (30), alkenes (17), esters (14), furans (14), benzenes (10), alkanes (8), napthalenes (7), acids (6), miscellaneous compounds (6), and phenols (5). Among the 230 compounds identified, 96 compounds were positively confirmed and quantified, and the rest of the compounds were tentatively identified. The major volatile components identified at relatively high levels were dodecanoic acid, hexadecanoic acid, hexanal, benzaldehyde, (Z)-3-hexen-1-ol, 1-penten-3-one, limonene, and $\beta$-caryophyllene oxide. Among the groups, terpenes accounted for 60.18% of the total concentration of all the volatile components. Some volatile components might account for the unique aroma and the biological activity of the sample.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 추계학술대회논문집B
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• pp.859-866
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• 2001

During the Pre-service Inspection for Wolsong Unit 3&4 in 1997/1998 respectively, 17 Distorted Roll Transition indications(over expanded beyond tubesheet secondary face) were identified at the Unit 4 (S/G B, D). Six(6) tubes out of these tubes were plugged in 1998. However the first Periodic Inspection identified additional 110 indications in 1999 and 2000. The additionally identified 110 indication call, not reported at the Pre-service Inspection, are; 2 Not-Finally-Expanded-Tubes and 108 Distorted Roll Transition tubes. Design limit of each Steam Generator tube Plugging is 6.4%. Plugging was performed by the Steam Generator manufacturer under the warranty. When Distorted Roll Transition indications were first identified on the Unit 4 in 1998 the degree of Over-expansion was measured using an inner dial-gage to make the disposition of Nonconformance report. 2 Not-Finally-Expanded-Tubes were plugged and 10 tubes out of 108 Distorted Roll Transition Tubes were also plugged as a preventive measure.

• 한국산업정보학회논문지
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• 제5권4호
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• pp.1-15
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• 2000

Information systems (IS) failures still continue and are prevalent everywhere. When considering an enormous amount of budget currently invested on IS technology in many organizations, these continuing failures can be critical culprits to failures of the organizations themselves. However, the meaning and definition of IS failures are not unified among IS researchers as well as IS practitioners although there have been a lot of conceptual research regarding the concept of IS failures. Previous empirical studies are not enough yet and thus we anticipate further empirical studies to be performed which will validate previous conceptual research. In this regards, by analyzing IS practitioners perception toward IS failures in a more detailed manner, this research extends conceptual and empirical research in the past which previously identified the structure of information systems (IS) failures. Further, this current study identified the interrelationships among the categories. The data was analyzed using a multidimensional scaling program and fourteen categories of problems were identified as to constitute the IS failure structure. It was found that about a half of categories identified were related to technical failures such as network and system infrastructure, costs, data/information, and program errors. The other remaining categories were related with organizational or social problems such as business success, human resources, relationships, communication, and user skills.

• Smart Structures and Systems
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• 제20권2호
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• pp.115-126
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• 2017

The modal identification of large civil structures such as bridges under the ambient vibrational conditions has been widely investigated during the past decade. Many operational modal analysis methods have been proposed and successfully used for identifying the dynamic characteristics of the constructed bridges in service. However, there is very limited research available on reliable criteria for the robustness of these identified modal parameters of the bridge structures. In this study, two time-domain operational modal analysis methods, the data-driven stochastic subspace identification (SSI-DATA) method and the covariance-driven stochastic subspace identification (SSI-COV) method, are employed to identify the modal parameters from field recorded ambient acceleration data. On the basis of the SSI-DATA method, the modal contribution indexes of all identified modes to the measured acceleration data are computed by using the Kalman filter, and their applicability to evaluate the robustness of identified modes is also investigated. Here, the benchmark problem, developed by Hong Kong Polytechnic University with field acceleration measurements under different excitation conditions of a cable-stayed bridge, is adopted to show the effectiveness of the proposed method. The results from the benchmark study show that the robustness of identified modes can be judged by using their modal contributions to the measured vibration data. A critical value of modal contribution index of 2% for a reliable identifiability of modal parameters is roughly suggested for the benchmark problem.

• 대한방사선기술학회지:방사선기술과학
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• 제25권1호
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• pp.77-81
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• 2002

The purpose of this study is to examine quantitatively the relationship between visual image quality and degradation In spatial resolution for a gamma camera by the increase in distance from collimator. The relationship between the portion(p) of images identified the difference of image quality and the difference(${\Delta}FWHM$) in FWHM between paired images was showed in a sigmoid curve. Using Dendy's method, minimum level to be correctly identified the difference of Image duality on three out of four occasion(p=0.75) was corresponded to 0.4 mm in ${\Delta}FWHM$. Using fuzzy theory, the level to be identified the difference of image quality was examined under various conditions. The truth-value of fuzzy sets-degraded or slightly degraded and not-degraded in image quality between palled Images-was gained the peak at 0.5 mm of ${\Delta}FWHM$. It was founded that changes of $0.4{\sim}0.5\;mm$ in FWHM-corresponding about 2 cm distance from collimator could be sufficiently identified in the difference of image quality.

• Wind and Structures
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• 제17권6호
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• pp.609-627
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• 2013

The Yingxian wooden tower in China is currently the tallest wooden tower in the world. It was built in 1056 AD and is 65.86 m high. Field measurements of wind speed and wind-induced response of this tower are conducted. The wind characteristics, including the average wind speed, wind direction, turbulence intensity, gust factor, turbulence integral length scale and velocity spectrum are investigated. The power spectral density and the root-mean-square wind-induced acceleration are analyzed. The structural modal parameters of this tower are identified with two different methods, including the Empirical Mode Decomposition (EMD) combined with the Random Decrement Technique (RDT) and Hilbert transform technique, and the stochastic subspace identification (SSI) method. Results show that strong wind is coming predominantly from the West-South of the tower which is in the same direction as the inclination of the structure. The Von Karman spectrum can describe the spectrum of wind speed well. Wind-induced torsional vibration obviously occurs in this tower. The natural frequencies identified by EMD, RDT and Hilbert Transform are close to those identified by SSI method, but there is obvious difference between the identified damping ratios for the first two modes.

• Smart Structures and Systems
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• 제19권5호
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• pp.523-538
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• 2017

A series of field vibration tests are conducted on the Runyang Suspension Bridge during both the construction and operational stages. The purpose of this study is devoted to the analysis of the dynamic characteristics of the suspension tower. After the tower was erected, an array of accelerometers was deployed to study the evolution of its modal parameters during the construction process. Dynamic tests were first performed under the freestanding tower condition and then under the tower-cable condition after the superstructure was installed. Based on the identified modal parameters, the effect of the pile-soil-structure interaction on dynamic characteristics of the suspension tower is investigated. Moreover, the stiffness of the pile foundation is successfully identified using a probabilistic finite model updating method. Furthermore, challenges of identifying the dynamic properties of the tower from the coupled responses of the tower-cable system are discussed in detail. It's found that compared with the identified results from the freestanding tower, the longitudinal and torsional natural frequencies of the tower in the tower-cable system have changed significantly, while the lateral mode frequencies change slightly. The identified modal results from measurements by the structural health monitoring system further confirmed that the vibrations of the bridge subsystems (i.e., the tower, the suspended deck and the main cable) are strongly coupled with one another.

• 한국수산과학회지
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• 제53권4호
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• pp.566-571
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• 2020

To classify a presumed hybrid of imported grouper species acquired from the National Fishery Products Quality Management Service, maternal and paternal lines were identified based on partial sequencing of mitochondrial cytochrome c oxidase 1 (co1) and nuclear recombination activation gene 1 (rag1) genes. The matrilineal species was identified as Epinephleus moara by a partial (760 bp) co1 sequence. Ambiguous sequences with base pairs belonging to E. moara or E. lanceolatus were found in a total of 15 different base pairs in the partial 1,159 bp of the rag1 gene, and the patrilineal species was found to be E. lanceolatus. Therefore, all of the groupers examined in the study were identified to be hybrids of E. moara and E. lanceolatus. In addition, a fast and convenient method using random amplification of polymorphic DNA (RAPD) was established for hybrid discrimination. Hybrids between E. moara ♀ and E. lanceolatus ♂ were identified through specific bands of 387 bp and 433 bp in PRIMER 6.

• 한국식품영양과학회지
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• 제32권3호
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• pp.315-319
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• 2003

브로콜리 중의 bioactive organosulfur phytochemicals를 분석하기 위해 브로콜리를 용매추출하여 GC/MSD에 의해 분리동정하였다. 브로콜리에 함유된 phytochemicals 중에서 isothiocyanate류가 40.42%로 대부분을 차지하였으며, glucosinolate분해산물인 nitrile류는 5.12%로 isothiocyanate류에 비해 적었고, sulfide류는 0.84%로 매우 적었다. 분리 동정된 isothiocyanate류의 종류로는 3-butenyl 4-methtlthiobutyl, 4-methrlthio -3- butenyl, 5- methylthiopentyl, 2- phenylethyl, 3-methylsulfinyl propyl 및 4-methylsulfinylbutyl isothiocyanate의 7종이었다. Isothiocyanate류 중에서 3-butenyl isothiocynate는 22.05%로 가장 많았으며, 그 다음으로 sulforaphane 16.50%로 2종의 isothiocyanate가 대부분을 차지하였다. Nitrile의 종류는 4-methylthiobutyl, 5-methylthiopentyl, 2-phenylethyl 및 4-methylsulfinylbutyl nitrile의 6종류가 확인되었다. 한편, 동정된 sulfide종류로는 dimethyl disulfide, dimethyl trisulfide 및 dimethyl tetrasulfide이었다.

• 분석과학
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• 제9권4호
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• pp.399-405
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• 1996

참기름 중의 향기성분을 연속수증기증류법(SDE)과 동적헤드스페이스법(DHS)으로 포집하여 GC와 GC-MSD로 동정하였다. SDE로 분석하였을 때 alcohol 6종, aldehyde 6종, ketone 및 acid류 5종, furan 및 phenol류 4종, pyrazine 화합물 12종, pyridine 및 thiazole류 4종, 기타 9종으로 총 46종이 확인되었다. DHS로 분석한 경우 alcohol 3종, aldehyde 6종, ketone, furan 및 phenol류 6종, pyrazine류 12종, pyridine 및 thiazole 4종, 기타 5종으로 모두 36종이 확인되었다. 대부분의 화합물이 SDE법에서 분리된 것이었으나 1-hexanol, pentanal, dimethylsulfide등은 DHS법에 의해서만 분리되었다.