• 제목/요약/키워드: homogeneous gel

검색결과 204건 처리시간 0.028초

디스크형 산화구리 촉매담지 세라믹필터의 제조와 물성 (Preparation and Properties of Disc Type CuO Catalyst Impregnated Ceramic Filters)

  • 홍민선;문수호;이재춘;이동섭;임우택
    • 한국대기환경학회지
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    • 제20권2호
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    • pp.185-193
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    • 2004
  • A catalyst with CuO ceramic filter for simultaneous treatment of dust and HAP was prepared and characterized. Catalytic ceramic filter can not only potentially achieve the substantial savings in energy but provide with effective optimization and integration of process for simultaneous removal of SO$_2$, NO$_{x}$ and particulates from flue gases. Catalytic ceramic filters remove simultaneously particulates on exterior surface of filters and reduce NO to $N_2$ and $H_2O$ by SCR (Selective Catalytic Reduction) process. Preparation of catalyst impregnated ceramic filter with disk shape (Ψ 50) follow the processing of alumino-silicate ceramic filter, support impregnation and catalyst impregnation (copper oxide). Preparation routes of alumino-silicate catalyst carrier suitable for production of catalytic filters practically were studied and developed using the sol-gel and colloidal processing, homogeneous precipitation and impregnation method. Characterization of the catalyst, catalyst carrier catalytic filter materials have been performed the using various techniques such as BET, XRD, TGA, SEM. Combination of the sol-gel and colloidal processing and impregnation method is recommended to prepare catalyst carriers economically for catalytic filter applications.s.

Fusarium속에서 PFGE를 이용한 Electrophoretic Karyotyping (Electrophoretic Karyotyping by PFGE in the Genus Fusarium)

  • 민병례;정진숙;최영길
    • 한국균학회지
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    • 제26권2호통권85호
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    • pp.135-143
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    • 1998
  • CHEF (Contour-Clamped homogeneous electric field) gel electrophoresis를 이용하여 Fusarium section Sporotrichiella, Liseola, Gibbosum, Discolor와 Martiella에 속하는 10종의 electrophoretic karyotype을 비교하였다. Intact chromosomal DNA는 균류의 원형질체로부터 추출하였으며, 크기에 따라 다양한 조건을 주어 DNA 분자를 분리시켰다. Fusarium속에 속하는 종의 염색체는 0.78Mb에서 7.20Mb의 크기를 가진 염색체가 종에 따라 $5{\sim}13$개였다. 각 종의 total genome 크기는 18.32Mb에서 48.20Mb였다. Electrophoretic karyotype을 비교한 후 F. oxysporum formae speciales lilii로부터 무작위로 선택하여 만든 genomic DNA를 probe로 하여 Southern hybridization 분석을 수행하였다.

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한국산 느타리버섯(Pleurotus spp.)의 전기영동 Isozyme Band Pattern 비교 -I. Homogeneous Gel- (Comparison of Electrophoretic Isozyme Band Pattern of Pleurotus spp. in Korea -I. Homogeneous Gel-)

  • 박용환;변명옥;등정부
    • 한국균학회지
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    • 제16권2호
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    • pp.87-94
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    • 1988
  • 한국산 느타리버섯 균주의 균사, Primordia, 갓, 줄기의 전피영동 isozyme 패턴을 비교한 결과 자실체중 Primordia, 갓, 줄기의 패턴은 모두 아주 유사하였으나 균사의 패턴은 자실체의 것과 많은 차이가 있었다. 자생지역이 다른 한국산 Pleurotus ostreatus의 전기영동 isozyme 패턴중 Malate Dehydrogenase, Acid phosphatase는 유사하였으나 Esterase, Peroxidase, Leucine amino peptidase, Superoxide Dismutase의 패턴은 차이가 있었다. Pleurotus osteatus, P. cornucopiac, P. florida의 종간 Esterase 밴드 패턴은 많은 차이가 있어 전기영동에 의한 느타리버섯 종의 가능하였다.

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Prepartion and Characterization of the Pt doped $TiO_2$ Membranes

  • Bae, Dong-Sik;Han, Kyong-Sop;Choi, Sang-Hael
    • The Korean Journal of Ceramics
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    • 제3권1호
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    • pp.52-56
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    • 1997
  • The Pt doped $TiO_2$ composite membranes were prepared by the sol-gel process. The Pt doped titania sol was peptized with hydrochloric acid in the pH range of 1.23 to 1.32 at 5$0^{\circ}C$. The average particle size of the Pt doped titania sol was shown to be below 15nm and well dispersed in the solution. XPS show the Pt elements continuous and homogeneous dispersed in the $TiO_2$ membrane. The mean particle size of the Pt doped $TiO_2$ composite membrane has smaller than that of the undoped $TiO_2$ composite membrane. The average pore size of the Pt doped $TiO_2$ composite membrane was increased from 58 to 193 $\AA$ with firing temperature changed from 550 to 85$0^{\circ}C$. It was observed that the Pt doped $TiO_2$ composite membranes showed crack-free and homogeneous microstructue as well as narrow particle size distribution up to above 75$0^{\circ}C$.

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Overexpression of Escherichia coli Thiol Peroxidase in the Periplasmic Space

  • Kim, Sung-Jin;Cha, Mee-Kyung;Kim, Il-Han;Kim, Ha-Kun
    • Journal of Microbiology and Biotechnology
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    • 제8권1호
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    • pp.92-95
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    • 1998
  • Overproduction of Escherichia coli thiol peroxidase in the periplasmic space was achieved by locating the appropriate gene on a downstream region of the strong T7 promoter. E. coli strain BL21 carrying the recombinant plasmid pSK-TPX was induced by IPTG, lysed, and analyzed by SDS-polyacrylamide gel electrophoresis. A large amount of the overexpressed thiol peroxidase was located in the periplasmic space. A homogeneous thiol peroxidase was obtained from E. coli osmotic shock fluid by simple one-step gel permeation chromatography.

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Rhizopus japonicus가 생산하는 인삼 Saponin 전환효소의 정제 (Purification of the Convertible Enzyme of Ginseng Saponin from Rhizopus japonicus)

  • 김상달;서정훈
    • 한국미생물·생명공학회지
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    • 제16권6호
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    • pp.438-442
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    • 1988
  • The enzyme produced by Rhizopus japonicus was able to convert selectively ginsenoside-Rb$_1$which is the most abundant ginseng saponin, into ginsenoside-Rd which was known to be superior to ginsenoside-Rb$_1$pharmaceutically. The convertible enzyme was purified homogeneous from wheat bran culture of Rhizopus japonicus by ammonium sulfate fractionation and column chromatography of TEAE-cellulose, DEAE-Sephadex A-50, Sephadex G-150, Sepharose 2B. Specific activity of the purified enzyme was increased to a bent 96 folds and yield was appeared to be 11% of culture extract. Evidence for homogenity was obtained from polyacrylamide and SDS-polyacrylamide gel electrophoresis. Molecular weight of the enzyme was estimated about 88, 000 daltons by Sephadex G-l50 gel filtration and SDS-polyacrylamide gel electrophoresis, and it did not consist of any subunit.

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고구마 $\beta$-아밀라제의 subunit (Subunits of Sweet Potato $\beta$-Amylase)

  • 안용근
    • 한국식품영양학회지
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    • 제1권2호
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    • pp.50-55
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    • 1988
  • B-Amylase was obtained from sweet potato extract in a crystalline state by dialysis against water after precipitated with acetone according to the method reported previously followed by DEAE Sephadex A-50 ion exchange chromatography plus gel chromatography of Sephadex G-200. The purified enzyme was homogeneous by SDS PAGE. The efforts had done to remove the miner bands in SDS PAGE by Sephadex G-200 gel chromatography, DATE Sephadex A-50 ion exchange chromatography. isoelectrophocusing, affinity chromatography, hydroxyapatite chromatography, recrystallizstion and HPLC on a column of TSK gel SW 3000 but have given any result. But, N -terminal amino acid of the enzyme was revealed mainly alanine and trace of glycine and glutamic acid. Therefore, it seems that the miner bands in SDS PAGE have a role of subunit.

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졸-겔법에 의한 지르콘$(ZrSiO_4)$ 분말 합성 -재분쇄(Milling)에 대한 효과- (Synthesis of $(ZrSiO_4)$ Powders by the Sol-Gel Process -Effect of the Milling-)

  • 신용철;신대용;한상목;남인탁
    • 한국세라믹학회지
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    • 제32권7호
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    • pp.853-857
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    • 1995
  • ZrSiO4 powders were prepared from partially hydrolyzed solution of Si(OC2H5)4 and ZrOCl2.8H2O solution by the sol-gel method and formation rate of ZrSiO4 on the reaction parameter was investigated. In order to prepare homogeneous ZrSiO4 precursor gels, the H2O/Si(OC2H5)4 molar ratio of about 2, the pH of the ZrOCl2.8H2O solution fo about 4 and stirring time of the mixed solutions of about 2 hrs were appropriate. Formation of temperature of ZrSiO4 reduced about 15$0^{\circ}C$ by milling and formation of ZrSiO4 at 1300~135$0^{\circ}C$ showed an accelerative increase through the hedvall effect by silica.

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Sol-Gel법에 의한 강유전체 PZT 박막의 제작 (Preparation of Ferroelectric PZT thin films by Sol-Gel processing)

  • 이병수;유도현;신태현;조기선;육재호;김용혁;김형권;지승한;이덕출
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2000년도 하계학술대회 논문집 C
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    • pp.1685-1686
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    • 2000
  • Crack-free and homogeneous com ceramic and epitaxial lead zirconate titanat ferroelectric thin films with perovskite structure been prepared by sol-gel processing. Ti-isoprop and lead acetate trihydrate and zirconium-pro are used raw materials. EAcAc is used as a cat 2-Methoky ethanol is used as a solvent annealing temperatures of the thin films are 0$^{\circ}C$.

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묵의 구조와 텍스쳐 (Structure and Textural Property of Mook)

  • 배광순;손경희;문수재
    • 한국식품과학회지
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    • 제16권2호
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    • pp.185-191
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    • 1984
  • 전분 젤의 특성을 정토하기 위하여 녹두, 감자, 고구마로 제조한 전분 겔 및 감자, 고구마 전분에 녹두 전분을 혼합하여 제조한 전분 겔의 구조 및 텍스쳐를 측정하고. 관능검사에 의해 전분 겔의 수응력을 평가하였다. 균일하고 porous한 구조를 보인 녹두 겔이 텍스쳐 측정치가 높은 값을 나타냈으며 관능검사에서도수응력이 높게 평가되었다.

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