• 대한금속재료학회지
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• 제46권8호
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• pp.477-481
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• 2008

The secondary hardening and fracture behavior in P/M high speed steels bearing V content of 9 to 10 wt% have been investigated in terms of austenitizing temperature and precipitation behavior. Austenitizing was conducted at 1,100 and $1,175^{\circ}C$ of relatively low and high temperatures. Coarse primary carbides retained after austenitization were mainly V-rich MC type. They give a significant influence on hardeness and toughness, as well as wear resistance. Tempering was performed in the range of $500{\sim}600^{\circ}C$. The peak hardness resulting from the precipitation of the fine MC secondary carbides was observed near 520, irrespective of austenitizing temperature. Aging acceleration(or deceleration) did not occur with increasing austenitizing temperature because it mainly influences contents of V and C of matrix through the dissloution of coarse primary MC containing lots of V and C. The precipitation of secondary MC carbides, which also contain V and C, did not change the aging kinetics itself. In the 10V alloy containing much higher C content, the impact toughness was lower than 9V alloy, because of the larger amount of primary carbide and high hardness.

• 공업화학
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• 제10권5호
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• pp.711-717
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• 1999

다층구조 고분자 재료의 비결정성 영역에서의 파괴 역학 변형과정을 통하여 ductile 및 brittle층을 동시에 함유하는 다층 구조 가공물을 이용하여 단층 구조물과의 물성을 비교, 조사하였다. 그 결과 거의 유사한 유리 전이온도($T_g$) 및 동일한 dimension에서 다층 구조물의 충격강도가 단일층 구조물보다 현격히 높게 나타났으며, toughness는 약 2배 이상 향상됨을 알 수 있었다. 이것은 ductile층과 brittle층의 두께 비에는 임계값이 있으며, 그 이하에서는 brittle한 재료이더라도 ductile하게 나타날 수 있다는 toughening 원리가 본 실험의 측정 속도 영역 및 온도 범위에서 적용되고 있음을 의미한다. 또한 고속 균열이 진행하는 경우의 운동 응력(kinetic stress wave) 효과를 해석하기 위하여 충격파동 중첩의 원리(superposition principle of impact pulse)를 도입하였다. 그 결과 다층 구조물의 최종 toughness 향상은 ductile/brittle 비율의 최적설계에 있음을 알 수 있었다.

• 한국압력기기공학회 논문집
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• 제10권1호
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• pp.100-106
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• 2014

There is a growing need to introduce advanced pressure vessel steels with higher strength and toughness for the optimizatiooCn of the design and construction of longer life and larger capacity nuclear power plants. SA508 Gr.4N Ni-Cr-Mo low alloy steels have superior strength and fracture toughness, compared to SA508 Gr.3 Mn-Mo-Ni low alloy steel. Therefore, the application of SA508 Gr.4N low alloy steel could be considered to satisfy the strength and toughness required in advanced nuclear power plants. The purpose of this study is to characterize the microstructure and mechanical properties of SA508 Gr.4N low alloy steels. 1 ton ingot of SA508 Gr.4N model alloy was fabricated by vacuum induction melting followed by forging, quenching, and tempering. The predominant microstructure of the SA508 Gr.4N model alloy is tempered martensite having small packet and fine Cr-rich carbides. The yield strength at room temperature was 540MPa, and it was decreased with an increase of test temperature while DSA phenomenon occurred at around $288^{\circ}C$. Overall transition property of SA508 Gr.4N model alloy was much better than SA508 Gr.3 low alloy steel. The index temperature, $T_{41J}$, of SA508 Gr.4N model alloy was $-132^{\circ}C$ in Charpy impact tests, and reference nil-ductility transition temperature, $RT_{NDT}$ of $-105^{\circ}C$ was obtained from drop weight tests. From the fracture toughness tests performed in accordance with the ASTM standard E1921 Master curve method, the reference temperature, $T_0$ was $-147^{\circ}C$, which was improved more than $60^{\circ}C$ compared to SA508 Gr.3 low alloy steels.

• Journal of Welding and Joining
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• 제34권2호
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• pp.16-21
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• 2016

Recent keywords of the heavy industries are large-scale structure and productivity. Especially, the sizes of the commercial vessels and the offshore structures have been gradually increased to deliver goods and explore or produce oil and natural gas in the Arctic. High heat input welding processes such as electro gas welding (EGW) have been widely used for welding thick steel plates with flux-cored arc welding (FCAW), especially in the shipbuilding industries. Because high heat input welding may cause the detrimental effects on the fracture toughness of the welded joint and the heat affected zone, it is essential to obtain the sufficient toughness of welded joint. There are well known that the fracture toughness like CTOD, CVN, and KIC were very important factors in order to secure the safety of the structures. Furthermore, the welding residual stress should be considered to estimate the unstable fracture in both EGW and FCAW. However, there are no references on the welding residual stress distribution of EGW and FCAW with thick steel plates. Therefore the welding residual stresses were very important elements to evaluate the safety of the welded structure. Based on the measurement results, the characteristics of residual stress distribution through thickness were compared between one-pass electron gas welding and multi-pass flux-cored arc welding. The longitudinal residual stress in the multi-pass flux-cored arc welding is tensile through all thicknesses in the welding fusion zone. Meanwhile, longitudinal residual stress of EGW is tensile on both surfaces and compressive at the inside of the plate. The magnitude of residual stresses by electron gas welding is lower than that by flux-cored arc welding.

• 콘크리트학회지
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• 제6권4호
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• pp.141-152
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• 1994

산업부산물의 플라이애쉬와 실리카흄 및 국내 부존자원이 풍부한 규사분말, 생석회 및 발포용 알루미늄 분말과 취성개선을 위한 보강용 섬유를 사용한 경량 고강도의 시멘트복합체의 개발을 위하여 오토클래브 양생에 의한 열수 알카리분위기에서의 섬유 자체의 열화현상을 조사함과 아울러 배합요인별로 건재용 경량섬유보강 규산칼슘계 시멘트복합에를 제조하여 그 역학적 특성에 관한 연구를 수행하였다. 시험결과, 탄소섬유 및 내알카리성 유리섬유는 보강용 섬유로서 적합함이 확인되었으며, 경량 섬유보강 규산칼슘계 시멘트복합체의 압축, 인장, 휨강도는 플라이애쉬와 실리카흄 혼입율 및 섬유혼입율이 증가함을 따라 증가하는 경향을 나타내었고 또한 섬유혼입율 증가에 따라 현저히 휨인성이 증가하였으며, 탄소섬유보강의 경유가 유리섬유보강의 경우에 비하여 압축, 인장, 휨강도 및 휨인성은 다소 높은 경향을 나타내었다.

• 한국재료학회지
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• 제28권11호
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• pp.653-658
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• 2018

$ZrO_2$ is a candidate material for hip and knee joint replacements because of its excellent combination of biocompatibility, corrosion resistance and low density. However, the drawback of pure $ZrO_2$ is a low fracture toughness at room temperature. One of the most obvious tactics to cope with this problem is to fabricate a nanostructured composite material. Nanomaterials can be produced with improved mechanical properties(hardness and fracture toughness). The high-frequency induction heated sintering method takes advantage of simultaneously applying induced current and mechanical pressure during sintering. As a result, nanostructured materials can be achieved within very short time. In this study, W and $ZrO_2$ nanopowders are mechanochemically synthesized from $WO_3$ and Zr powders according to the reaction($WO_3+3/2Zr{\rightarrow}W+3/2ZrO_2$). The milled powders are then sintered using high-frequency induction heating within two minutes under the uniaxial pressure of 80MPa. The average fracture toughness and hardness of the nanostructured W-3/2 $ZrO_2$ composite sintered at $1300^{\circ}C$ are $540kg/mm^2$ and $5MPa{\cdot}m^{1/2}$, respectively. The fracture toughness of the composite is higher than that of monolithic $ZrO_2$. The phase and microstructure of the composite is also investigated by XRD and FE-SEM.

• Restorative Dentistry and Endodontics
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• 제35권6호
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• pp.461-472
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• 2010

연구목적: 본 연구는 미세인장결합강도와 파괴인성을 통해 복합 레진 수복물의 수리 시기와 표면 처리 방법에 따른 파괴 거동을 알아보고자 시행되었다. 연구 재료 및 방법: Short rod 시편과 composite resin specimen block을 준비하여 표면 처리 방법에 따라 none-treated, sand blasting, bur roughening 군으로 나누고 이를 다시 즉시군과 2주 지연군으로 나누어 수리했다. 결과: 미세인장결합강도와 파괴인성을 측정한 결과, 두 실험 모두에서 즉시군이 지연군보다 높은 값을 보였다. 기계적 표면 처리군이 none-treated군보다 높은 값을 보였고, sand blasting과 bur roughening 사이에 유의한 차이는 없었다. 파괴인성과 미세인장결합강도는 상관 관계가 없었다. FE-SEM을 보아 수복물의 탈락은 균열 전도와 관계가 있는 것으로 보인다. 결론: 수리된 복합 레진의 파괴 거동 평가에는 파괴인성 실험이 적합하다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2002년도 제7회 단조 심포지엄
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• pp.93-104
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• 2002

• 열처리공학회지
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• 제27권3호
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• pp.121-126
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• 2014

High-nitrogen Fe-18Mn-18Cr-N austenitic steels with higher yield strength have been recently developed and used for generator retaining rings because they have non-magnetic, high strength, high ductility, and good corrosion resistance. In the present study, a high-nitrogen Fe-18Mn-18Cr-0.61N austenitic steel was fabricated and then tensile and Charpy impact tests were conducted on them in order to investigate the effect of cold working on the mechanical properties. Although the yield and tensile strengths usually increased with cold working, the ductility and impact toughness significantly decreased after cold working. On the other hand, the high-nitrogen austenitic steel exhibited a ductile-brittle transition due to unusual brittle fracture at low temperatures despite having a face-centered cubic structure. The ductile-brittle transition temperature obtained from Charpy impact tests could be remarkably increased by $60^{\circ}C$ after 20% cold working because of the enhanced cleavage-like brittle fracture.

• 공업화학
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• 제10권5호
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• pp.789-795
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• 1999

본 연구에서는 비원형의 단-탄소섬유를 이용하여 시멘트 복합재를 제조하고 이 복합재의 특성(건조 수축, 동결 융해저항성, 파괴 인성)을 원형 탄소섬유보강 복합재와 비교하여 연구하였다. 그 결과 섬유의 형상과 길이에 크게 의존하였다. C형 탄소섬유보강 시멘트 복합재의 건조수축저감 효과가 다른 형상의 섬유보강 복합재에 비해 우수하였다. 이 효과는 섬유의 종횡비가 클수록 증가하였다. 또한, 동결융해 저항성은 섬유형상의 영향은 두드러지지 않았으나 섬유길이와 섬유함유율에 따라 증가하였다. 특히, C형 보강 시멘트 복합재의 파괴 인성 및 균열 저항성은 다른 것에 비해 크게 개선되었다. 이는 더 큰 계면으로 파괴에너지를 더 많이 흡수하였기 때문으로 생각된다.