• Title/Summary/Keyword: high temperature mechanical properties

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Effects of SiC Particle Size and Inorganic Binder on Heat Insulation of Fumed Silica-based Heat Insulation Plates

  • Jo, Hye Youn;Oh, Su Jung;Kim, Mi Na;Lim, Hyung Mi;Lee, Seung-Ho
    • Journal of the Korean Ceramic Society
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    • v.53 no.4
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    • pp.386-392
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    • 2016
  • Heat insulation plates of fumed silica were prepared by mixing fumed silica, SiC powder and chopped glass fiber by a high speed mixer followed by pressing of the mixture powder in a stainless steel mold of $100{\times}100mm$. Composition of the plates, particle size of SiC, and type of inorganic binder were varied for observation of their contribution to heat insulation of the plate. The plate was installed on the upper portion of an electric furnace the inside temperature of which was maintained at $400^{\circ}C$ and $600^{\circ}C$, for investigation of heat transfer through the plate from inside of the electric furnace to outside atmosphere. Surface temperatures were measured in real time using a thermographic camera. The particle size of SiC was varied in the range of $1.3{\sim}17.5{\mu}m$ and the insulation was found to be most excellent when SiC of $2.2{\mu}m$ was incorporated. When the size of SiC was smaller or larger than $2.2{\mu}m$, the heat insulation effect was decreased. Inorganic binders of alkali silicate and phosphate were tested and the phosphate was found to maintain the heat insulation property while increasing mechanical properties.

The Characteristics of Ultrasonic Signals for Detecting Micro-Defects in Ti-6Al-4V Alloy (Ti-6Al-4V 합금의 내부 미소결함에 따른 초음파 신호 특성 연구)

  • Choi, Sang-Woo;Lee, Joon-Hyun;Kubota, M.;Murakami, Y.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.6
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    • pp.591-597
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    • 2001
  • Ti alloy is used for essential parts of aircraft for high temperature environment. Although Ti alloy has excellent performance in regard to mechanical properties, it is difficult ot find fatigue cracks by nondestructive ultrasonic inspection due to its two-phase microstructure, which consists of hard alpha and beta phases. Sound energy reflected from microstructural features in the component produces a background inspection noise which is seen even when no defects are present. This noise can inhibit the detection of critical internal defects such as pores cracks or inclusions. To obtain fundamental data on ultrasonic inspection of Ti alloy, ultrasonic testing was performed using a specimen with small drill holes and ultrasonic wave propagation velocites were measured.

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An Experimental Study of Characteristics of Plate Deformation by Heating Process (열간가공에 의한 판의 변형특성에 관한 실험적 연구)

  • Chang-Doo Jang;Dae-Eun Ko;Byeong-Il Kim;Jeong-Ung Park
    • Journal of the Society of Naval Architects of Korea
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    • v.38 no.2
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    • pp.62-70
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    • 2001
  • As the ship hull is a compound-curved structure, plate bending process is indispensible. The process includes press bending process for forming major 1st curvature and heating process for forming the rest curvature. Especially the heating process that is above 50 percents of entire bending work is carried out exclusively by skillful workers. Many researches have been made to automate the heating process but most of these are about line heating process and researches for triangle heating process are rare. This study is a fundamental study to develop a efficient analysis method for triangle heating and focused on clarifying the deformation characteristics of plate by triangle heating. In this paper, we carried out heating experiments and analysed the deformation characteristics of plate to explain the deformation characteristics of plates rationally by showing the phase transformed high temperature region. Also we investigated the heating effect on the hull material properties by mechanical tests.

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Fracture Behaviour of Lubricants in ABS Terpolymer (ABS 중에 첨가된 저분자 화합물의 파단 거동에 미치는 영향)

  • Don, Yoon-Seung;Shim, Mi-Ja;Kim, Sang-Wook
    • Applied Chemistry for Engineering
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    • v.5 no.5
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    • pp.878-888
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    • 1994
  • In order to investigate the fracture behavior of ABS terpolymer under the tension and impact load, varing the content of rubber, molecular weight of SAN, content and kinds of lubricant, tension speed, the mechanical properties were measured and SEM pictures of fracture area were taken. Under the tension, the tensile strength increased as rubber content and lubricant content decreased, while molecular weight and tension speed increased. The deformation of area near fracture site did not occur as rubber content, tension speed and molecular weight decreased and liquid lubricant was used. And in the shape of fracture seemed phase seperation. Under the impact load, the notched izod impact strength increased as rubber content, molecular weight, ambient temperature and lubricant content increased. In the SEM picture, the strength was high white the fracture surface was small.

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Characteristics of the AlON-Al2O3 Ceramic Coatings on the Al2021 Alloy by Electrolytic Plasma Processing

  • Wang, Kai;Byeon, Sang-Sik;Kim, Geun-Woo;Park, Keun-Young;Ahmed, Faheem;Koo, Bon-Heun
    • Korean Journal of Materials Research
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    • v.22 no.3
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    • pp.155-158
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    • 2012
  • In this work, AlON-$Al_2O_3$ coatings were prepared on Al2021 alloy by the electrolytic plasma processing (EPP) method. The experimental electrolytes include: 2 g/l NaOH as the electrolytic conductive agent, 10 g/l $Na_2AlO_2$ as the alumina formative agent, and 0.5 g/l $NaNO_2$, $NaNO_3$, and $NH_4NO_3$ as the nitride inducing agents. The effects of different nitrogen inducing agents were studied by a combined compositional and structural analyses of the ceramic coatings carried out by Xray diffractometry (XRD) and scanning electron microscopy (SEM) for the specimens EPP-treated at room temperature for 15 min under a hybrid voltage of 260 DC along with an AC 50 Hz power supply (200 V). Microhardness tests and wear tests were carried out to correlate the evolution of the microstructure and the resulting mechanical properties. Potentiodynamic polarizations and immersion corrosion tests were carried out in 3.5wt% NaCl water solutions under static conditions in order to evaluate the corrosion behavior of the coated samples. The results demonstrate that $NaNO_2$ is proven to be a good nitrogen inducing agent to produce high quality AlON-$Al_2O_3$ ceramic coatings.

Growth and Optical Properties for $CdGa_2Se_4$ epilayer by Hot Wall Epitaxy (Hot Wall Epitaxy (HWE)에 의한 $CdGa_2Se_4$ 박막 성장과 광학적 특성)

  • Hong, Myoung-Seok;Hong, Kwamg-Joon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.11a
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    • pp.125-126
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    • 2006
  • The stochiometric mix of evaporating materials for the $CdGa_2Se_4$ single crystal thin films was prepared from horizontal furnace. To obtain the single crystal thin films. $CdGa_2Se_4$ mixed crystal was deposited on thoroughly etched semi-insulating GaAs(100) substrate by the Hot Wall Epitaxy (HWE) system. The source and substrate temperature were $630^{\circ}C$ and $420^{\circ}C$, respectively. The crystalline structure of single crystal thin films was investigated by the photoluminescence and double crystal X-ray diffraction (DCXD). The carrier density and mobility of $CdGa_2Se_4$ single crystal thin films measured from Hall effect by van der Pauw method are $8.27{\times}10^{17}cm^{-3}$. $345cm^2/V{\cdot}s$ at 293 K, respectively. From the photoluminescence measurement on $CdGa_2Se_4$ single crystal thin film, we observed free excition ($E_x$) existing only high quality crystal and neutral bound exiciton ($D^{\circ},X$) having very strong peak intensity. Then. the full-width-at -half-maximum(FWHM) and binding energy of neutral donor bound excition were 8 meV and 13.7 meV, respectivity. By Haynes rule. an activation energy of impurity was 137 meV.

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The Evaluations of Thermal Stability and Stress Crack Resistance of Geomembranes with Surface Defects in the Landfill (폐기물매립지에서 표면결함이 있는 지오멤브레인의 열적 안정성 및 응력균열저항성 평가)

  • 전한용;이광열;이재영
    • Journal of Soil and Groundwater Environment
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    • v.6 no.1
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    • pp.53-62
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    • 2001
  • Effects of surface defect on thermal stability and stress crack resistance of high density polyethylene geomembranes in environmental conditions were examined by comparing the mechanical properties, chemical resistance and failure times of geomembranes between defective cases under different temperatures. Artificial surface defects were added to the surface of geomembranes by scratch apparatus designed specially. The number of surface defects was increased with the smaller size of scratch induced particles, and the more scratch addition numbers at the shear rate of scratch induced mechanism, 100mm/min. The tensile strength were decreased but the tensile strain was increased with the above conditions. In chemical resistance of defective geomembranes, the tensile strength were decreased but the tensile strain was increased with the longer immersion period and the higher temperature under the same scratch induced conditions. Finally, failure times of defective geomembranes by ESCR test were shifted to the shorter time ranges by increasing temperatures.

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Investigating the effects of confining pressure on graphite material failure modes and strength criteria

  • Yi, Yanan;Liu, Guangyan;Xing, Tongzhen;Lin, Guang;Sun, Libin;Shi, Li;Ma, Shaopeng
    • Nuclear Engineering and Technology
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    • v.52 no.7
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    • pp.1571-1578
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    • 2020
  • As a critical material in very/high-temperature gas-cooled reactors, graphite material directly affects the safety of the reactor core structures. Owing to the complex structures of graphite material in reactors, the material typically undergoes complex stress states. It is, therefore, necessary to study its mechanical properties, failure modes, and strength criteria under complex stress states so as to provide guidance for the core structure design. In this study, compressive failure tests were performed for graphite material under the condition of different confining pressures, and the effects of confining pressure on the triaxial compressive strength and Young's modulus of graphite material were studied. More specifically, graphite material based on the fracture surfaces and fracture angles, the graphite specimens were found to exhibit four types of failure modes, i.e., tension failure, shear-tension failure, tension-shear failure and shear failure, with increasing confining pressure. In addition, the Mohr strength envelope of the graphite material was obtained, and different strength criteria were compared. It showed that the parabolic Mohr-Coulomb criterion is more suitable for the strength evaluation for the graphite material.

Experimental Study on the Material Characteristics of Slag Cement with Various Phosphogypsum Materials (인산부산석고의 각 형태조건에 따른 슬래그 시멘트의 품질특성에 관한 실험적 연구)

  • Park, Jong-Tak;Oh, Hong-Seob
    • Journal of the Korea Concrete Institute
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    • v.21 no.6
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    • pp.729-735
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    • 2009
  • In this study, it is experimentally verified a feasibility of the wasted phosphogypsum ($CaSO_4/H_2O$) that is a byproduct from the phosphoric acid process of manufacturing fertilizers can be applied as an admixture in slag cement. For the test, phosphogypsum is modified as dihydrate, hemihydrate, type III anhydrite, and type II anhydrite, and then chemical characteristics and mechanical properties of various slag cements containing above mentioned gypsum materials were analyzed. The test results show that the gypsum made at high temperature has better quality with decrease of water-soluble phosphoric acid ($S-P_2O_5$) which has an effect on the quality of cement. And type II anhydrite shows superior quality in terms of drying shrinkage and the compressive strength of cement paste with hemihydrate at 56 days is higher than other gypsum material.

Half-dome Thermo-forming Tests of Thermoplastic Glass Fiber/PP Composites and FEM Simulations Based on Non-orthogonal Constitutive Models (열가소성 유리섬유/PP 복합재의 반구돔 열성형 평가 및 비직교 구성방정식을 이용한 FEM 수치해석)

  • Lee, Wonoh
    • Composites Research
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    • v.29 no.5
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    • pp.236-242
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    • 2016
  • In this work, tensile and in-plane shear tests for thermoplastic glass fiber/polypropylene composites were performed at a thermo-forming temperature and their properties were characterized and mathematically expressed by using the non-orthogonal constitutive model. As for the thermo-forming test, half-dome experiments were carried out by varying the usage of a releasing agent and the weight of holders. As results, the optimum final shape having well-aligned symmetry and no wrinkle formation was obtained when the releasing agent was used, and it was found that the careful control of a holding force is crucial to manufacture the healthy product. Furthermore, FEM simulations based on the non-orthogonal model showed similar final shapes and tendency of wrinkle formation with experimental results, and confirmed that wrinkles increase with less holding force and higher punch force is required under high frictional condition.