• 한국세라믹학회지
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• 제34권1호
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• pp.88-94
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• 1997

플라즈마 용사법(plasma spray method)으로 제작된 상용 가스 터빈 연소기의 finned segment의 열차폐용 코팅계, ZrO2-8wt%Y2O3 top coat/Ni-26Cr-5Al-0.5Y bond coat/Hastelloy X superalloy 기판에서 NiCrAlY bond coat의 산화 거동과 열피로 파괴에 대하여 조사하였다. 생성된 bond coat의 주산화물은 NiO, CrO2, Al2O3였다. ZrO2/bond coat계면에서 생성된 산화물의 분포는 고온에서의 사용 전에 이 계면 아래에 얇은 층의 Al2O3가없는 곳에서는 NiO 산화층 및에 Cr2O3와 Al2O3가 혼합된 형태를 나타내었다. 열피로에 의해 박리된 시편의 파면을 관찰한 결과, 파괴는 주로 ZrO2/산화층 계면보다 세라믹층내로 약간 치우쳐서 일어나지만, 산화층 내에서도 약간 일어남을 알 수 있었다.

• 대한치과보철학회지
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• 제45권1호
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• pp.60-70
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• 2007

Statement of problem: The cement-type abutment would be needed for the reduction of its body in order to correct the axis and to assure occlusal clearance. In the case of intraoral preparation, there is a potential risk that generated heat could be transmitted into the bone-implant interface, where it can cause deterioration of tissues around the implant and failed osseointegration. Purpose: The purpose of this study was to assess the difference of the heat transmitting effect on external and internal connection implant types under various conditions. Material and method: For evaluating the effects of alternating temperature, the thermocoupling wires were attached on 3 areas of the implant fixture surface corresponding to the cervical, middle, and apex. The abutments were removed 1mm in depth horizontally with diamond burs and were polished for 30 seconds at low speed with silicone points using pressure as applied in routine clinical practice. Obtained data were analyzed using Mann-Whitney rank-sum test and Wilcoxon / Kruskal-Wallis Tests. Result: Increased temperature on bone-implant interface was evident without air-water spray coolant both at high speed reduction and low speed polishing (p<.05). But, the difference between connection types was not shown. Conclusion: The reduction procedure of abutment without using proper coolant leads to serious damage of oral tissues around the implant irrespective of external and internal connection type.

• 한국표면공학회지
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• 제29권6호
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• pp.862-868
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• 1996

Cadmium sulfide is commonly used as the window material for thin film solar cells, and can be prepared by several techniques such as sputtering, spray pyrolysis, close spaced sublimation (CSS), thermal evaporation, solution growth methods, etc. In this study, CdS films were deposited by thermal evaporation, close spaced sublimation, and solution growth methods, respectively, and the effects of the methods on physical properties of polycrystalline CdS deposited on ITO/glass were investigated. Also, the effects of variously prepared CdS thin films on the physical properties of CdTe deposited on the CdS were investigated. The thickness of polycrystalline CdS films was maintained at $0.3\mu\textrm{m}$ except for the solution grown CdS when $0.2\mu\textrm{m}$ thick CdS was deposited. After the deposition, all the samples were annealed at $400^{\circ}C$ or $500^{\circ}C$ in H2 atmosphere. To investigate physical properties of the deposited and annealed CdS thin films, UV-VIS spectro-photometry, X-ray diffractometry (XRD), and Auger electron spectroscopy (AES), and cross sectional transmission electron microscopy(XTEM) were used to analyze grain size, crystal structure, preferred orientation, optical properties, etc. The annealed CdS showed the bandedge transition at 510nm and the optical transmittance high than 80% for all of the variously deposited films. XRD results showed that CdS thin films variously deposited and annealed had the same hexagonal structures, however, showed different preferred orientations. CSS grown CdS had [103] preferred orientation, thermally evaporated CdS had [002], and CdS grown by the solution growth had no preferred orientation. The largest grain size was obtained for the CSS grown CdS while the least grain size was obtained for the solution grown CdS. Some of the physical properties of CdTe deposited on the CdS thin film such as grain size at the junction and grain orientation were affected by the physical properties of CdS thin films.

• 한국표면공학회지
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• 제42권1호
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• pp.1-7
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• 2009

Resistive heating sources are widely used to prepare thin films by vapor deposition because they are cheap, and easy to install and handle in vacuum system. Graphite is one of materials used to make the resistive heating source, but until now only limited applications have been possible as it reacts easily with evaporating materials at high temperature. In this study, evaporation characteristics of aluminum have been investigated by using graphite boat thermally treated with BN powder. The employed graphite boat has been prepared by spray-coating BN power onto the cavity surface of the boat and thermal treatment with aluminum in vacuum at the temperature of more than $1400^{\circ}C$. The voltage-current characteristics as well as resistivity changes of the graphite boat have been investigated during aluminum evaporation according to the applied voltage and time. The evaporation aspect has been picturized during flash evaporation for 40 seconds based on the characterization results. The evaporation rate of the graphite boat has been compared with that of BN boat. The graphite boat showed some different characteristics compared with BN boat, in that the evaporation occurred at the last stage of flash evaporation. The film appearance according to the applied voltage has been compared, and also the reflectance of the resulting film has been investigated according to the film thickness. It has been found that the graphite boat thermally treated with BN powder can be used for aluminum evaporation without problem.

• 한국항공우주학회지
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• 제31권10호
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• pp.60-65
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• 2003

회전분무시스템을 적용한 가스터빈연소기의 점화특성을 연구하기 위한 실험적 연구를 수행하였다. 연료분사는 연료를 회전연료노즐의 내측에 공급한 후, 고속모터로 회전하는 연료노즐에서 발생하는 원심력을 이용하여 분사되는 방식을 이용하였다. 실물크기의 연소기 및 시험리그를 제작하여 한국항공우주연구원의 연소시험설비를 이용하여 대기압 조건에서 연소시험을 수행하였다. 시험결과 이 연소기의 점화성능은 연료노즐의 회전속도를 증가하거나 감속할 경우 연소가스의 온도가 급격하게 변화되는 특성이 있음을 알 수 있었다.

• Journal of Biosystems Engineering
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• 제31권3호
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• pp.153-160
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• 2006

This study was performed to evaluate some geometrical characteristics of disc type swirl nozzles and to develop nozzles having improved spraying performance for knapsack sprayers. Considered geometrical characteristics of the nozzles were disc thickness, orifice diameter, swirl chamber diameter and shape of the swirl chamber (nozzle chamber). 3 types of nozzle cores were compared. Main results of this study were as follows. 1. Spraying angle (A) was increased with decreasing disc thickness (x), and with increasing orifice diameter (y) or spraying pressure (z). The equation was as a follow. $$A=3.95\frac{1}{x}+73.50\sqrt{y}+18.97\sqrt{z}-60.16$$ 2. Spraying flow rate (F) was increased with decreasing disc thickness (x), and with increasing orifice diameter (y) or spraying pressure (z). The equation was as a follow. $$F=-89.95x+611.09y+620.49\sqrt{z}-868.20$$ 3. Mean spraying droplet size (V) was decreased with decreasing disc thickness (x), with increasing orifice diameter (y) in low spraying pressure, with decreasing orifice diameter (y) in high spraying pressure, and with increasing spraying pressure (z). $$V=148.77x^4-746.85x^3+1311.76x^2-917.31x$$ 4. The spray pattern was compared using CV values. The CV value of the nozzle core type 1 was 26.7% in spraying pressure $3\;kgf/cm^2$, the CV value of the core type 2 was 23.6% in spraying pressure $2\;kgf/cm^2$, the CV value of the core type 3 was 20.6% in spraying pressure $1\;kgf/cm^2$. 5. Minimum spraying pressure was improved from $1.5\;kgf/cm^2\;to\;1.0\;kgf/cm^2$ by changes of nozzle core shape.

• 한국유기농업학회지
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• 제21권3호
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• pp.363-372
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• 2013

가지 담배가루이 친환경 방제기술을 개발하고자, 난황유 등 8종의 천연물질을 가지 정식 후 7일 간격으로 살포하면서 생육을 조사한 결과 님제처리에서 가장 양호한 경향이었다. 담배가루이 성충과 약충의 발생은 디노테퓨란약제처리에서 가장 적었고, 친환경자재 중에서는 님제 처리에서 가장 적었다. 수량은 디노테퓨란 약제처리에서 가장 많았고, 친환경 자재에서는 님제, 고추씨유 등이 많았으며, 고삼제 은행과육 등에서 적었다. 님제 처리의 경우 무처리에 비하여 69% 많았고, 디노테퓨란약제에 비해 52% 낮은 수량을 나타내었다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제40회 동계학술대회 초록집
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• pp.423-423
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• 2011

Zinc oxide is metal oxide semiconductor with the 3.37 eV bandgap energy. Zinc oxide is very attractive materials for many application fields. Zinc Oxide has many advantages such as high conductivity and good transmittance in visible region. Also it is cheaper than other semiconductor materials such as indium tin oxide (ITO). Therefore, ZnO is alternative material for ITO. ZnO is attracting attention for its application to transparent conductive oxide (TCO) films, surface acoustic wave (SAW), films bulk acoustic resonator (FBAR), piezoelectric materials, gas-sensing, solar cells and photocatalyst. In this study, we synthesized ZnO nanoparticles and defined their physical and chemical properties. Also we studied about the application of ZnO nanoparticles as a photocatalyst and try to find a enhancement photocatalytic activity of ZnO nanorticles.. We synthesized ZnO nanoparticles using spray-pyrolysis method and defined the physical and optical properties of ZnO nanoparticles in experiment I. When the ZnO are exposed to UV light, reduction and oxidation (REDOX) reaction will occur on the ZnO surface and generate O2- and OH radicals. These powerful oxidizing agents are proven to be effective in decomposition of the harmful organic materials and convert them into CO2 and H2O. Therefore, we investigated that the photocatalytic activity was increased through the surface modification of synthesized ZnO nanoparticles. In experiment II, we studied on the stability of ZnO nanoparticles in water. It is well known that ZnO is unstable in water in comparison with TiO2. Zn(OH)2 was formed at the ZnO surface and ZnO become inactive as a photocatalyst when ZnO is present in the solution. Therefore, we prepared synthesized ZnO nanoparticles that were immersed in the water and dried in the oven. After that, we measured photocatalytic activities of prepared samples and find the cause of their photocatalytic activity changes.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제40회 동계학술대회 초록집
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• pp.45-45
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• 2011

알루미늄과 그 합금은 내부식성(corrosion resistance)이 좋고, 밀도가 낮아 높은 연료소비 효율을 필요로 하는 항공기와 자동차 같은 운송수단의 내-외장 소재로 사용되고 있다. 또한 알루미늄의 높은 내부식성을 이용하여 철강소재의 부식을 방지하는 보호막으로도 폭 넓게 사용된다. 물리기상증착(physical vapor deposition)으로 알루미늄을 코팅하면 박막 성장 초기단계에서 핵(nucleus)을 형성하고, 형성된 핵을 중심으로 주상 구조(columnar structure)로 박막이 성장하는 것이 일반적으로 알려진 방식이다. 주상 구조의 알루미늄 박막은 주상정과 주상정 사이에 필연적으로 공극(pore)이 존재하게 되어 부식을 일으키는 물질이 박막으로 침투하게 되고, 부식 물질과 모재가 반응하여 공식(pitting corrosion)이 발생한다. 본 연구에서는 스퍼터링(magnetron sputtering)을 이용하여 치밀한 조직을 갖는 알루미늄 박막을 코팅할 수 있는 공정을 개발하고, 치밀한 알루미늄 조직이 내부식성에 어떠한 영향을 미치는지 평가하였다. 기판은 냉연강판(cold rolled steel sheet)이 사용되었으며, 알루미늄 타겟의 순도는 99.999%, 크기는 직경 4"이었다. 냉연강판은 진공용기(vacuum chamber)에 장착하기 전에 계면활성제를 이용하여 표면에 존재하는 기름성분을 제거하였으며, 진공용기에 장착한 후에는 아르곤 가스를 이용하여 발생시킨 글로우 방전으로 표면에 존재하는 산화물을 제거하였다. 알루미늄 박막의 조직에 영향을 미치는 공정변수를 확인하기 위해서 스퍼터링 파워, 공정 온도, 공정 압력, 외부 자기장 세기 등의 공정 조건을 변화시켜 코팅을 실시하였다. 실험을 통해서 얻어진 최적 조건으로 알루미늄을 코팅할 경우, 알루미늄 bulk의 밀도와 비교하여 약 94.7%의 밀도를 갖는 알루미늄 박막을 코팅할 수 있었다. 알루미늄 박막이 약 3 ${\mu}$m의 두께로 코팅된 냉연강판의 내부식성 평가(salt spray test, 5% NaCl) 결과, 평가를 시작한 후 72시간 후에도 적청이 발생하지 않았다.

• 한국농림기상학회지
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• 제8권3호
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• pp.169-173
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• 2006

황사가 과수의 착과와 과실품질에 미치는 영향을 분석하기 위하여 황사 발원지에서 채취한 황토(losses)를 이용하였다. 우리나라에서 포집된 황사와 황사발원지에서 채취한 황토의 화학적 특성을 분석한 결과, 우리나라 평균 밭토양보다 알칼리성이 강하고, 유기물 함량이 높았으며 다량의 치환성 양이온 중 Ca의 함량이 높은 수준이었다. 사과, 배, 복숭아 3 과종의 개화기에 황토를 처리한 결과, 과총 착과율과 과실 당 종자수에서 무처리와 차이가 없었으며, 적숙기에 수확한 과실의 과중, 당도, 과형에서도 처리 간에 차이를 나타내지 않았다. 그러나 본 연구에서는 황사 대신 황토를 처리하였고, 개화기에 인위적으로 살포한 것으로서 매우 제한적인 결과이며, 실제 황사의 발생빈도, 지속시간, 밀도 그리고 황사 발생기간의 기상조건에 따라 과수의 결실과 과실특성에 줄 수 있는 영향이 달라질 수 도 있을 것으로 생각된다. 또한 황사 내에 포함된 각종 세균, 곰팡이, 미생물의 영향은 본 실험에서 고려하지 못하였다.