• Title/Summary/Keyword: high curing temperature

검색결과 504건 처리시간 0.028초

Curing Reaction and Physical Properties of High-Solid Acrylic/Isocyanate Coatings (하이솔리드 아크릴/이소시아네이트 도료의 경화반응과 도막물성)

  • Park, Hong-Soo;Shim, Il-Woo;Jo, Hye-Jin;Kim, Seong-Kil;Kim, Myung-Soo
    • Journal of the Korean Applied Science and Technology
    • /
    • 제22권4호
    • /
    • pp.371-378
    • /
    • 2005
  • In the previous study, three kinds of monomers and the functional monomer, acetoacetoxyethyl methacrylate (AAEM), which could improve the film property and cross-linkage, were polymerzied into acrylic resin copolymers (HSA-98-20, HSA-98-0, HSA-98+20) containing 80% solid content. In this study, the high-solid coatings(HSA-98-20C, HSA-98-0C, HSA-98+20C) were prepared by the curing reaction between acrylic resins containing 80% solid content and isocyanate at room temperature. Various properties were examined for the film coated with the prepared high-solid coatings. The introduction of AAEM in the coatings enhanced the abrasion resistance and solvent resistance of coatings, which indicated the possible use of high-solid coatings for top-coating materials of automobile. The curing times measured by viscoelastic measurement were 350, 264, and 212 min for HSA-98-20C, HSA-98-0C, and HSA-98+20C, respectively. This shows that the curing times become shorter with increasing $T_g$ values.

A Study on the Plate for Deep Discharge in Lead Acid Battery (납축전지의 심방전용 극판에 관한 연구)

  • Jeong, Soon-Wook;Ku, Bon-Keun
    • Journal of the Korean Applied Science and Technology
    • /
    • 제31권2호
    • /
    • pp.197-202
    • /
    • 2014
  • Positive plate was composed of lead hydroxide via reaction between lead oxide and $H_2O$ and lead sulfate was formed of the reaction of lead hydroxide with sulfuric acid. And its density is $3.8g/cm^3$, $4.0g/cm^3$, $4.2g/cm^3$ and $4.4g/cm^3$ by controlling volume of refined water. Curing of positive plate is done for low ($45^{\circ}C$, 40hr, over 95% of relative humidity) & high ($80^{\circ}C$, 40hr, over 95% of relative humidity) temperature, which created 3BS & 4BS active materials. Experimental result of DOD with 100% life cycle test shows that it was not related to the density of active materials but to the low & high temperature aging of active materials. The test makes us to understand that the crystallization which is made by curing of active materials is a more of a main factor than density of active materials under the deep cycle using circumstances. The active materials which were from the high temperature curing are better for deep cycle performance.

Flexural Behavior of High-strength Concrete Beams of 90 MPa According to Curing Temperature (양생온도에 따른 90 MPa 수준의 고강도 철근 콘크리트 보의 휨거동)

  • Hwang, Chul-Sung
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • 제21권5호
    • /
    • pp.134-140
    • /
    • 2017
  • In this study, the flexural behavior of high strength concrete members with different curing condition of 90 MPa of compressive strength was investigated. Experimental parameters included normal and low temperature curing conditions, tensile steel amount and concrete compressive strength. 8 beam members were fabricated and flexural tests were carried out. Crack spacing, load-deflection relation, load-strain relation and ductility index were determined. Experimental results show that as the amount of rebar increases, the number of cracks increases and the crack spacing decreases. The higher the concrete strength, the smaller the number of cracks, but the effect is significantly smaller than the amount of rebar. As a result of comparison with the proposed average crack spacing in the design criteria, the experimental results are slightly larger than the results of the proposed formula, but the proposed formula does not reflect the concrete strength and curing conditions. The ductility index of normal temperature cured members was 3.36~6.74 and the ductility index of low temperature cured members was 1.51~2.82. The behavior of low temperature cured members was found to be lower than that of normal temperature cured members. As a result of comparing the ductility index with the existing studies similar to the experimental members, the ductility index of the high strength concrete member was larger than the ductility index of the ordinary strength concrete of the previous study. Further research is needed to understand more specific results.

Effect of Compressive Strength and Curing Condition on the Direct Tensile Strength Properties of Ultra High Performance Concrete (압축강도 및 양생조건에 따른 초고성능 콘크리트의 직접인장강도 특성)

  • Park, Ji Woong;Lee, Gun Cheol
    • Journal of the Korea Institute of Building Construction
    • /
    • 제17권2호
    • /
    • pp.175-181
    • /
    • 2017
  • The purpose of this study is evaluating the characteristics of tensile strength of UHPC and examining tensile performance of notched specimens by direct tensile test. For test variables, 120, 150, and 180MPa of target design standard strength were aimed at. With general water curing and $90^{\circ}C$ high temperature steam as curing conditions, the properties were reviewed. Overall, it was represented that the specimens of notch-type direct tensile strength concrete was effective in inducing central cracks compared with existing direct tension specimens. Through this, it was judged that data construction with high reliability was possible. Above all, in a graph of direct tensile strength and strain, in the case of steam curing at high temperature, there was great difference of initial tensile strength compared with water curing. As passing of ages, an aspect that the difference gradually decreased was shown. Maximum tensile strength was found to increase steadily with increasing age for all target design strengths in water curing, in the case of steam curing, the tendency to increase significantly due to the initial strength development effect at 7 days of age. The initial crack strength increases with age in case of underwater curing, in the case of steam curing, it was higher than that of water curing in 7 days, while the strength of 28 days was lowered. In this part, it is considered necessary to examine the arrangement condition of the steel fiber.

Variation according to Curing Time in Epoxy Composites Using TSC Method (TSC방법을 이용한 에폭시 복합체의 경화 시간에 따른 변화)

  • 장인범;김성렬;박건호;이성일;김영천;이준웅
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 한국전기전자재료학회 1996년도 춘계학술대회 논문집
    • /
    • pp.260-263
    • /
    • 1996
  • The thermally stimulated currents(TSC) are measured to know the behaviour of charging particles of epoxy composites at the temperature range of -160∼200[$^{\circ}C$] and to prove the variation according to curing time in this study. It is confirmed that the peak amplitude is inversely proportional to the curing time, and TSC are reduced is and T$\sub$m/ is moved to high temperature side according to the curing time because carboxyl radical is formed by thermal oxidation and motility becomes lack.

  • PDF

Effect of curing temperature on microstructure of blast furnace slag concrete (양생온도가 고로슬래그 콘크리트의 미세구조에 미치는 영향)

  • Lee, Kyu-Dong;Lee, Chang-Soo;Seol, Jin-Seong;Jun, Myeong-Il
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 한국콘크리트학회 2006년도 추계 학술발표회 논문집
    • /
    • pp.817-820
    • /
    • 2006
  • This study investigated on the differentiation of microstructure of blast furnace slag concrete(BBSC) using Mercury Intrusion Porosimetry(MIP). From the test result, it was found that the BBSC did not show shortcomings of high temperature curing. The BBSC gives more fineness microstructure than that of plain concrete when it is cured same curing condition. The curing age making stable structure to poor surroundings was 28, 14, 7 days for blast furnace concrete cured at 5, 20, $30^{\circ}C$, respectively.

  • PDF

Surface Curing Method of Hot weather Concreting with the Combination of Surface Curing sheets (표면 양생시트 조합에 의한 서중콘크리트용 표면 양생공법)

  • Lee, Ju-Suck;Kim, Jong-Back;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 한국콘크리트학회 2006년도 추계 학술발표회 논문집
    • /
    • pp.785-788
    • /
    • 2006
  • This paper investigates the temperature history of slab mock-up specimens with various surface curing sheets, in order to determine a favorable surface curing method in hot weather condition. Test showed that insulating double bubble sheets+aluminum foil simultaneously on the upper section of a specimen prevented an increase of sudden temperature and a decrease of vaporization when placed during the hot weather condition. It also secured the high strength in early age. Therefore it is found that using the double bubble sheets+aluminum foil on concrete surface declined the plastic and drying shrinkage and inclined the early strength, thus improving the concrete quality.

  • PDF

A Preliminary Study on Mortar Strength Development by Low-Pressure Steam Curing Method (상압증기양생에 의한 모르터의 강도발현성에 관한 기초연구)

  • 곽영근;정상진
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 한국콘크리트학회 1994년도 가을 학술발표회 논문집
    • /
    • pp.194-199
    • /
    • 1994
  • Frefab Construction known for durable construction skill prompting high productivity in developed country is not yet settled in Korea. This situation of prefab construction results from lack of skill, specialists and quality control. In introducing skill, all equipments are thoughtlessly imported without inside eudeavor for development. Regardless of production of goods, basic study for production of goods, construction and structure is not abailable. The object of this study is curing method in the production process of PC concrete product. From change of curing temperature and curing period which would be factors of product quality in PC concrete production, and research of optimized steam curing condition from relations between curing condition and strength development, basic data of concrete steam curing method will be presented.

  • PDF

Effects of Formaldehyde to Urea Mole Ratio on Thermomechanical Curing of Urea-Formaldehyde Resin Adhesives

  • Park, Byung-Dae;Kim, Jae-Woo
    • Journal of the Korean Wood Science and Technology
    • /
    • 제35권5호
    • /
    • pp.76-86
    • /
    • 2007
  • This study was conducted to investigate the effects of formaldehyde to urea (F/U) mole ratio on thermomechanical curing of UF resin adhesives with different F/U mole ratios. Thermomechanical curing of these UF resin adhesives was characterized using parameters of dynamic mechanical analysis (DMA) such as the gel temperature, maximum storage modulus, and peak temperatures of storage and loss modulus. As the F/U mole ratio decreased, the gel temperature of UF resin adhesives increased. The maximum storage modulus as an indicator of the rigidity of UF resin adhesives decreased with decreasing F/U mole ratio. The peak temperature of tan $\delta$ increased with decreasing F/U mole ratio, indicating that the vitrification occurred faster for high F/U mole ratio of UF resin adhesives than for the one of lower F/U mole ratio. These results partially explained the reason why UF resin adhesives with lower F/U mole ratio resulted in relatively poor adhesion performance when they were applied.

Effects of Post Cure Conditions on Thermal Characteristics of A1$_2$O$_3$ Filled Epoxy Resin Composite System (A1$_2$O$_3$ 충전된 에폭시 수지 복합재료계의 후기 경화조건에 따른 열적특성)

  • Cho, Young-Shin;Shim, Mi-Ja;Kim, Sang-Wook
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
    • /
    • pp.227-230
    • /
    • 1998
  • The effects of post curing conditions on thermal properties of alumina filled epoxy resin system DGEBA/MDA/SN were investigated. As the post curing time increased at 15$0^{\circ}C$, the glass transition temperature increased from 121 to 124, slightly. As the heating rate increased, high thermal decomposing temperature (T$_{d}$) and most decomposing temperature (T$_{p}$) increased. For the case of post-cured system at 15$0^{\circ}C$ for 4 days showed lower values than virgin system. At the post curing condition the system must have been thermally degraded.ded.

  • PDF