• Title/Summary/Keyword: high Tg

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Reliability Enhancement of Anisotropic Conductive Adhesives Flip Chip on Organic Substrates by Non-Conducting Filler Additions

  • Paik, Kyung-Wook;Yim, Myung-Jin
    • Journal of the Microelectronics and Packaging Society
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    • v.7 no.1
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    • pp.41-49
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    • 2000
  • Flip chip assembly on organic substrates using ACAs have received much attentions due to many advantages such as easier processing, good electrical performance, lower cost, and low temperature processing compatible with organic substrates. ACAs are generally composed of epoxy polymer resin and small amount of conductive fillers (less than 10 wt.%). As a result, ACAs have almost the same CTE values as an epoxy material itself which are higher than conventional underfill materials which contains lots of fillers. Therefore, it is necessary to lower the CTE value of ACAs to obtain more reliable flip chip assembly on organic substrates using ACAs. To modify the ACA composite materials with some amount of conductive fillers, non-conductive fillers were incorporated into ACAs. In this paper, we investigated the effect of fillers on the thermo-mechanical properties of modified ACA composite materials and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACAs composites with different content of non-conducting fillers, dynamic scanning calorimeter (DSC), and thermo-gravimetric analyser (TGA), dynamic mechanical analyzer (DMA), and thermo-mechanical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in the content of filler brought about the increase of $Tg^{DSC}$ and $Tg^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significantly affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.

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The antihyperlipidemic effect of alginate-free residue from sea tangle in hyperlipidemic rats

  • Yim, Mi-Jin;Lee, Jeong Min;Choi, Grace;Cho, Soon-Yeong;Lee, Dae-Sung
    • Fisheries and Aquatic Sciences
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    • v.22 no.11
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    • pp.27.1-27.6
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    • 2019
  • Background: In order to assess the high value-added use of the alginate-free residue of sea tangle, an animal study was performed to evaluate the functional activities and key compounds present. In the animal study, sea tangle and the alginate-free residue demonstrated good anti-hyperlipidemic and anti-arteriosclerotic abilities. Results: The functional compounds in the alginate-free residue of the sea tangle were effectively extracted by supercritical fluid extraction (SFE). The optimum extraction temperature and pressure were 40 ℃ and 6500 psi (M1) in the SFE, a better method in comparison to the conditions of 70 ℃ and 4500 psi (M2), respectively. The anti-atherosclerotic effects of the alginate-free residue of sea tangle (M1, M2) were investigated in Sprague-Dawley rats treated with poloxamer 407, Triton WR 1339, corn oil, and a high-fat diet. The M1 fraction reduced the serum lipid levels with greater efficacy than the M2 fraction. In the hyperlipidemic rats, treatment with M1 decreased the serum triglyceride (TG), total cholesterol (TC), and low-density lipoprotein-cholesterol (LDL-C) levels when compared to the levels in normal rats. Conclusion: Our results demonstrated that the alginate-free residue of sea tangle reduces serum TC, TG, and LDL-C. These results suggest that the alginate-free residue of sea tangle contains physiologically active components, such as fucosterol, that may exert beneficial effects in the prevention of atherosclerosis.

Thermal Denitration of High Concentration Nitrate Salts Waste Water (열분해에 의한 고농도 질산염 폐액의 탈질)

  • ;;;;;C. Latge
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2003.11a
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    • pp.665-670
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    • 2003
  • This study investigated the thermodynamic and the thermal decomposition properties of high concentration nitrate salts waste water for the lagoon sludge treatment. The thermodynamic property was carried out by COACH and GEMINI II based on the composition of nitrate Salts waste water. The thermal decomposition property was carried out by TG-DTA and XRD. Ammonium nitrate and sodium nitrate were decomposed at $250^{\circ}C$$730^{\circ}C$$450^{\circ}C$$Na_2O$ into stable $Na_2O$.$Al_2O_3$. The flow sheet for nitrate salts waste water treatment was proposed based on the these properties data. These will be used by the basic data of the process simulation.

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Evaluation of Fire-induced Damage for Shield Tunnel Linings Subjected to High Temperatures (고온에 노출된 쉴드터널 라이닝의 손상평가)

  • Lee, Chang Soo;Kim, Yong Hyok;Kim, Young Ook
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.4
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    • pp.1-8
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    • 2012
  • The aim of this study is to evaluate fire-induced damage for shield tunnel linings. Full-scale fire test was conducted to evaluate fire-induced damage. Residual compressive strength was measured on the core samples of shield tunnel lining subjected to high temperatures. Heating temperature was predicted by XRD and TG analysis. As a result, Strength degradation of concrete with temperatures can be evaluated by residual compressive strength of core samples. In addition, residual compressive strength can be estimated by previous studies if heating temperature is exactly predicted. It is possible that heating temperature is predicted by XRD and TG analysis at $450^{\circ}C$. For more accurate prediction of heating temperature it should be performed both instrumental analysis and analytical methods with temperatures ranging from $400{\sim}600^{\circ}C$.

Comparison of Serum Insulin, Leptin, Adiponectin and High Sensitivity C-Reactive Protein Levels according to Body Mass Index and their Associations in Adult Women (비만도에 따른 성인 여성의 혈청 인슐린, 렙틴, 아디포넥틴 및 hs-CRP 농도 비교와 상호 관련성)

  • Lee, Mi-Young;Kim, Jung-Hee
    • Korean Journal of Community Nutrition
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    • v.16 no.1
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    • pp.126-135
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    • 2011
  • Obesity is characterized by increased storage of fatty acids in an adipose tissue and closely associated with the development of insulin resistance and cardiovascular diseases (CVD) through secretion of adipokines. This study was done to compare serum insulin, leptin, adiponectin and high sensitivity C-reactive protein (hs-CRP) levels according to body masss index (BMI) in Korean adult women aged 19 to 50. In addition, we examined the association of BMI, serum lipids and Homa-IR with serum adiponectin, leptin and hs-CRP levels. The subjects were divided into 3 groups by their BMI, normal weight (BMI ${\leq}$ 22.9, n = 30), overweight (23.0 ${\leq}$ BMI ${\leq}$ 24.9, n = 71) and obese group (25.0 ${\leq}$ BMI, n = 59). Serum levels of total-cholesterol, TG, and LDL-cholesterol were significantly higher in obese group than in normal weight group. LDL/HDL ratio and AI were significantly higher in obese group than in normal or overweight group. Fasting serum levels of glucose and insulin and Homa-IR as a marker of insulin resistance were significantly higher in obese group than in overweight group. Serum leptin level was significantly higher in obese group while serum adiponectin level was significantly lower in obese group compared to other two groups. hs-CRP was significantly increased in obese group. Correlation data show that serum adiponectin level was positively correlated with serum HDLcholesterol level and was negatively correlated with BMI, WC, TG, LDL-cholesterol, Homa-IR, hs-CRP and leptin. In addition, serum leptin level was positively correlated with BMI, WC, glucose, insulin, Homa-IR and hs-CRP. These results might imply that the regulation of key adipokines such as adiponectin might be a strategy for the prevention or treatment of obesity-associated diseases such as diabetes and CVD.

Production of Methyl Ester from Coconut Oil using Microwave: Kinetic of Transesterification Reaction using Heterogeneous CaO Catalyst

  • Mahfud, Mahfud;Suryanto, Andi;Qadariyah, Lailatul;Suprapto, Suprapto;Kusuma, Heri Septya
    • Korean Chemical Engineering Research
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    • v.56 no.2
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    • pp.275-280
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    • 2018
  • Methyl ester derived from coconut oil is very interesting to study since it contains free-fatty acid with chemical structure of medium carbon chain ($C_{12}-C_{14}$), so the methyl ester obtained from its part can be a biodiesel and another partially into biokerosene. The use of heterogeneous catalysts in the production of methyl ester requires severe conditions (high pressure and high temperature), while at low temperature and atmospheric conditions, yield of methyl ester is relatively very low. By using microwave irradiation trans-esterification reaction with heterogeneous catalysts, it is expected to be much faster and can give higher yields. Therefore, we studied the production of methyl ester from coconut oil using CaO catalyst assisted by microwave. Our aim was to find a kinetic model of methyl ester production through a transesterification process from coconut oil assisted by microwave using heterogeneous CaO catalyst. The experimental apparatus consisted of a batch reactor placed in a microwave oven equipped with a condenser, stirrer and temperature controllers. Batch process was conducted at atmospheric pressure with a variation of CaO catalyst concentration (0.5; 1.0; 1.5; 2.0, 2.5%) and microwave power (100, 264 and 400 W). In general, the production process of methyl esters by heterogeneous catalyst will obtain three layers, wherein the first layer is the product of methyl ester, the second layer is glycerol and the third layer is the catalyst. The experimental results show that the yield of methyl ester increases along with the increase of microwave power, catalyst concentration and reaction time. Kinetic model of methyl ester production can be represented by the following equation: $-r_{TG}=1.7{\cdot}10^6{_e}{\frac{-43.86}{RT}}C_{TG}$.

Effects of Wolbitang on Obese Rats Induced by High Cholesterol Diet (고(高)콜레스테롤 식이(食餌)로 유도된 비만 흰쥐에 대한 월비탕(越婢湯)의 효과)

  • Park, Woong-Duck;Lee, Young-Jong
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.19 no.2
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    • pp.466-474
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    • 2005
  • Four kinds of decoctions (Wolbi-tang, Wolbigachul-tang, Wolbigabanha-tang and Wolbi-tang with Psyllium Husk diet)was prescribed to examined the therapeutic effects on hyperlipidemia. Four decoctions prepared from the prescriptions were respectively administrated to the corpulent rats induced by a high cholesterol diet. Wolbi-tang mollified the increasing rate of the body weight, and decreased the amount of food eaten. It slightly increased the concentrations of blood Tc, blood TG, blood FFA, and lipids in feces, and decreased the contents of blood HDL-c. Wolbigachul-tang mollified the increasing rate of the body weight, and decreased the amount of food eaten. It decreased the amount of FFA and HDL-c lipids in the blood. Wolbigabanha-tang mollified the increasing rate of the body weight, and decreased the amount of food eaten. Also, it decreased the concentrations of blood glucose. However, it increased the content of blood HDL-c. Wolbi-tang with Psyllium Husk diet mollified the increasing rate of body weight, and decreased the amount of food eaten. Also, it slightly decreased the concentrations of blood TG and blood FFA, but increased the concentrations of blood Tc. Considering the above results, four kinds of decoctions(Wolbi-tang, Wolbigachul-tang, Wolbigabanha-tang and Wolbi-tang with Psyllium Husk diet) could be applied for the treatment of obesity, and Wolbigabanha-tang would be the most recommendable among them.

A Cross-sectional Study on the Risk Factors Related to Fatty Liver (지방간의 위험요인에 관한 단면적 연구)

  • Ohm, S.H.;Yoo, B.C.;Kim, S.J.;Lee, C.U.;Pai, K.T.;Kim, S.C.;Shin, H.R.
    • Journal of Preventive Medicine and Public Health
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    • v.26 no.2 s.42
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    • pp.179-191
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    • 1993
  • Generally fatty liver is attributed either to chronic alcoholism, diabetes mellitus, or obesity. Based upon this commonly held clinical brief, this study was conducted to investigate the contributing factors of fatty liver and odds ratio (OR) of known contributing factors. A sample of 310 male participants, who visited at Seoul Paik Automated Multiphasic Health Testing System from November 1991 to December 1991, was separated into 112 cases and 198 controls by ultrasonographic fin ding. There were statistically significant difference between fatty liver and normal in triglyceride (TG), body mass index (BMI), alanine aminotransferase (ALT), high density lipoprotein cholesterol (HDL-C), fasting blood sugar (FBS), alcohol consumption, low density lipoprotein cholesterol (LDL-C), total cholesterol, gamma-glutamyl transferase ($\gamma$-GT), duration of alcohol intake and alkaline phosphatase (Alk.P)(P<0.01, P<0.05). The statistically significant elevated odds ratio were noted for TG (4.48, confidence interval (CI) 2.66-7.55, P=0.000), alcohol consumption(3.24, CI 1.56-6.23, P=0.002), BMI(3.05, CI 1.87-4.97, P=0.000), and FBS (2.59, CI 1.53-4.40, P=0,000). In summary, it is suggested that the fatty liver could be preventive by avoiding such deleterious factors as high fat diet, alcohol and obesity.

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Effects of Dietary Prosomillet on cholesterol and Fatty Acid Metabolism in Rats Fed High Cholesterol Diets

  • Cho, Sung-Hee;Jung, Seung-Eun;Lee, Hye-Kyung;Ha, Tae-Youl
    • Nutritional Sciences
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    • v.3 no.1
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    • pp.25-30
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    • 2000
  • To study the effect of prosomillet (Panicum milaceum) on lipid metabolism, male Sprague-Dawley rats weighing 190$\pm$8g were fed six experimental diets for four weeks. The six diets based on AIN-76 composition consisted of one cholesterol-free(normal) and five 1%(w/w) cholesterol diets, i.e. control, two diets containing additional 0.3 and 0.6%(w/w) methanol extracts of prosomillet and another two diets containing 15 and 30% (w/w) prosomillet powder. There was no difference in weight gains between the groups but relative liver weights increased under the cholestrol diets. Plasma levels of total cholesterol and triglyceride(TG) decreased by 23-27% and by 37-52%, respectively, in the four prosomillet diet groups compared to those of the normal and control groups. Whereas in the liver, only TG levels decreased in the prosomillet diet groups. Fecal excretions of bile acid and cholesterol significantly with methanol extracts of prosomillet. There was a significant increase in the activity of hepatic microsomal cholesterol 7$\alpha$-hydroxylase when feeding 1% cholesterol but prosomillet in the diet, either as in the form of powder or methanol extract, appeared to have only slight additional effects, namely increases in enzyme activity. The activity of liver cytosolic glucose-6-phophate dehydrogenase (G6PDH) tended to be reduced with high cholesterol diets and dropped markedly by 15% using additional prosomillet powder. Those of the liver cytoxolic malic enzyme had a similar tendency to those of G6PDH. The results indicate that certain active components in prosmillet other than fiber have the potential to exert hypolipidemic effects via regulating cholesterol excretions and lipogenesis.

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Meta-analysis of the Effects of Obese Management Program for Obese Young Adults (성인 초기 비만인을 대상으로 적용된 중재프로그램의 효과에 대한 메타분석)

  • Lee, Kowoon
    • Journal of the Korea Convergence Society
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    • v.12 no.8
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    • pp.345-356
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    • 2021
  • The aims of this study is to analysis the effects of obese management program for obese young adults. Nineteen studies were included for meta-analysis and SIGN was used for quality assessment. Effect size was analyzed by CMA 3.0 and Revman 5.4. Overall effect size on obese program was big (d=-0.91) and high heterogeneity (I2=81%). BMI (d=-0.83) and body fat (d=-0.93) shown the big effect size and TG (d=-0.76) and LDL (d=-0.59) were medium effect size among the studies that used dependent variables. Intervention with aerobic and combination exercise, middle and high exercise intensity, over 1 hour exercise were effective. Based on current findings, obesity management programs have significant effects for young adults.