• 센서학회지
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• 제17권4호
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• pp.261-266
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• 2008

In this paper, we present thermal characteristics of high-temperature measurement sensor using fiber Bragg grating(FBG), including peak reflectivity, FWHM bandwidth and various normalized refractive index change along temperature variation. The temperature stability of FBG temperature sensor can be changed by varying the refractive index change and grating length. The proposed FBG temperature sensor can measure up to about $600^{\circ}C$ and 1000 hours of heating time.

• 한국식품과학회지
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• 제29권4호
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• pp.730-736
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• 1997

저염 동치미 쥬스의 향미특성을 유지하는 가열살균 조건을 찾고자 가열온도와 시간이 총균수와 품질특성에 미치는 영향을 검토하였다. 저염 동치미 쥬스의 제조는 무를 0.5%의 소금용액에 담그어 $20^{\circ}C$에서 발효시켰다. 적당히 발효된 pH 3.8의 동치미 쥬스를 $60{\sim}100^{\circ}C$의 범위에서 $5{\sim}30$분간 가열한 결과 pH와 총산도는 거의 변화가 없었으나 쥬스의 밝기(L값)는 감소하였으며 탁도와 a, b값들은 가열온도와 시간이 증가할수록 약간씩 높아졌다. 총균수는 가열 후 현저히 감소하여 60, $70^{\circ}C$에서 30분씩 가열한 동치미 쥬스는 각각 18, 6 CFU/mL로 감소하였으며 90, $100^{\circ}C$에서 10분간 가열한 후에는 균이 검출되지 않았다. 가열한 동치미 쥬스의 관능적 특성은 $70^{\circ}C$에서 20분간 가열할때까지 크게 변하지 않았으나 그 이상의 조건에서는 익은맛 등의 이취미가 현저히 증가하였다. 가열살균한 동치미 쥬스를 $30^{\circ}C$에서 10일간 저장한 결과 pH, 총산도, 색은 거의 변화가 없었지만 가열하지 않은 동치미는 현저히 변화하였다. 살균한 동치미 쥬스의 저장 중 총균수는 초기 총균수와 거의 같은 수준이었다. 그리하여 동치미 쥬스의 가열살균 조건으로는 쥬스의 특성에 영향을 최소한으로 하고 저장성이 높았던 $60^{\circ}C$에서 30분 또는 $70^{\circ}C$에서 20분간이 적절하였다.

• Bulletin of the Korean Chemical Society
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• 제32권6호
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• pp.1957-1964
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• 2011

Various reaction conditions uding temperature, time and type and concentration of templates have been changed in order to facilely synthesize, especially with microwave (MW) heating, SAPO-34 molecular sieves. SAPO-34 molecular sieve can be synthesized rapidly with microwave irradiation from a gel containing tetraethylammonium hydroxide (TEAOH) as a template. However, other several templating molecules lead to SAPO-5 molecular sieve under microwave irradiation even though SAPO-34 is obtained by conventional electric synthesis from the same reactant gels. Moreover, SAPO-34 can be obtained more easily by increasing the TEAOH or silica concentration or by increasing the reaction temperature. SAPO-34 can be obtained within 5 min in a selected condition (high temperature of 210 $^{\circ}C$) with microwave heating, which may lead to a continuous production of the important material. SAPO-34 synthesized by microwave irradiation is homogeneous and small in size and shows acidity and a stable performance in the dehydration of methanol and 2-butanol to olefins, suggesting potential applications in acid catalysis.

• 한국응용과학기술학회지
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• 제33권1호
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• pp.58-66
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• 2016

저온진공건조 조건에 따른 곶감의 건조특성 및 품질적 변화를 분석하였다. 곶감의 건조 특성은 전형적인 항율건조기간과 감율건조기간이 존재함을 확인 할 수 있었다. 진공압력이 높을수록 가열온도가 높을수록 곶감의 당도, 당 함량, 경도 값은 높게 나타났으며 이에 비해 명도 값은 낮게 나타남을 알 수 있었다. 기존 천일 및 열풍건조를 대처할 수 있는 진공건조의 최적 조건은 진공압력이 40~50kPa abs., 가열온도 $30^{\circ}C$, 건조시간은 3~4일 이었다.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2003년도 춘계학술대회논문집
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• pp.483-488
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• 2003

Frictional heating in brakes causes thermoelastic distortion of the contacting bodies and hence affects the contact pressure distribution. The resulting thermo-mechanical coupling can cause thermoelastic instability (TEI) if the sliding speed is sufficiently high, leading to non-uniform heating called hot spots and low frequency vibration known as hot judder. The vibration of brakes to the known phenomenon of frictionally-excited thermoelastic instability is estimated studying the interface temperature and pressure evolution with time. A simple model has been considered where a layer with half-thickness ${\alpha}$ slides with speed V between two half-planes which are rigid and non-conducting. The advantage of this properly simple model permits us to deduce analytically the critical conditions for the onset of instability, which is the relation between the critical speed and the growth rate of the interface temperature and pressure. Symmetrical component of pressure and temperature distribution at the layer interfaces can be more unstable than antisymmetrical component. As the thickness ${\alpha}$ reduces, the system becomes more apt to thermoelastic instability. Moreover, the evolution of the system beyond the critical conditions has shown that even if low frequency perturbations are associated with low critical speed, it might be less critical than high frequency perturbations if the working sliding speed is much larger than the actual critical speed of the system.

• 한국식품영양과학회지
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• 제35권7호
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• pp.881-885
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• 2006

Glucose-glutamine 모델반응에서 생성물의 종류와 갈변에 의한 색의 변화를 조사하기 위하여, 가열조건을 125, 150 및 $175^{\circ}C$에서 각각 10, 20 및 30분간 가열하고 반응물의 색을 Hunter colorimeter로 측정한 후, ethyl acetate로 추출하여 GC/MS로 생성물을 분석하였다. GC/MS 분석에서 acetic acid, butanoic acid, 2-butenoic acid, di-(2-ethylhexyl) phthalate, 2,3-dihydro-3.5-dihydroxy-6-methyl-4H-pyran-4-one 및 5-hydroxymethylfurfural의 6종의 다량 생성물과 1,3-dimethylbenzene, 2-ethylhexanol, fufural, 5-methylfurfural, 2-pyrrolidinone 그리고 2,6-di(t-butly)-4-hydroxy-4-methyl-2,5-cyclohexadien-1-one 6종의 미량 생성물이 확인되었다. 최대 생성물인 acetic acid와 미량 생성물인 2-ethylhexanol 및 2-pyrrolidinone은 온도 및 가열시간의 경과에 따라 전반적으로 증가하였으나, 그 외 9종의 화합물을은 $125^{\circ}C$부터 생성량이 증가하지만 $150^{\circ}C$ 또는 $175^{\circ}C$를 정점으로 그 이상 온도, 또는 가열시간을 증가할수록 생성량은 감소하였다. 반응생성물이 Hunter $L^*$값은 온도 및 시간의 증가에 따라 지속적으로 감소하여 암색이 반응의 최종산물에 의한 색으로 나타났으며, $a^*$ 및 $b^*$은 $125^{\circ}C$에서 낮고 $150^{\circ}C$ 또는 $175^{\circ}C$, 10분에서 최고점을 나타낸 후 온도 및 시간의 증가에 따라 감소하여 적색과 황색은 반응 중간생성물에 의한 발현이며 반응후기에는 고분자의 화합물에 고착되어 암색을 발현하는 것으로 추정되었으며, 가열조건의 변화에 따른 $a^*$ 및 $b^*$값의 변화는 앞서 언급한 9종 화합물들의 생성 변화와 유사하였다.

• 대한기계학회논문집A
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• 제26권11호
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• pp.2450-2456
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• 2002

Microlenses and microlens arrays are fabricated using a novel fabrication technology based on the exposure of a resist (usually PMMA) to deep X-rays and subsequent thermal treatment. The fabrication technology is very simple and produces microlenses and microlens arrays with good surface roughness (less than 1 nm). The molecular weight and glass transition temperature of PMMA is reduced when it is irradiated with deep X-rays. The microlenses is produced through the effects of volume change, surface tension, and reflow during thermal treatment of irradiated PMMA. The geometry of the microlens is determined by parameters such as the X-ray dose applied to the PMMA, the diameter of the microlens, along with the heating temperature, heating time, and cooling rate in the thermal treatment. Microlenses are produced with diameters ranging from 30 to 1500 ${\mu}{\textrm}{m}$. The modified LIGA process is used not only to construct hemispherical microlenses but also structures that are rectangular-shaped, star-shaped, etc.

• Macromolecular Research
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• 제10권6호
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• pp.345-358
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• 2002

The electrical conductivity during vulcanization process was measured as a function of time for the system of TiC loaded styrene-butadiene rubber (SBR) composites. The phenomenon of negative and positive temperature coefficients of conductivity and its conduction mechanism were also studied for the SBR polymeric composites. The current-voltage characteristics of the polymeric composites were non-linear in high voltage and showed a switching effect. The effects of temperature on the thermal conductivity and effective dielectric constant were measured. The measured parameters were found to be dependent on TiC concentration. The electromagnetic wave shielding (EMS) of the SBR-TiC polymeric composite was also examined. The SBR filled with TiC could be expected to be promising novel smart polymeric composites for self-electrical heating, temperature sensor, time delay switching, and electro-magnetic wave shielding effectiveness.

• 한국세라믹학회지
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• 제49권6호
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• pp.601-607
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• 2012

The alkali-activation reaction of two types of typical kaolin calcined at various lower temperatures was investigated at room temperature and at elevated temperatures. For the assessment of the reactivity, the temperature increase and the setting time of pastes prepared with calcined kaolin and sodium/potassium hydroxide solution were measured. Unlike raw kaolin, calcined kaolin samples prepared at various temperature showed an alkali-activation reaction according to the different aspects of the changes in the mineral phases. The reactivity with alkaline solutions was exceedingly activated in the samples calcined at $600-650^{\circ}C$, but the reactivity gradually decreased as the temperature increased in a higher temperature range, most likely due to the changes in the crystal structure of the dehydrated kaolin. The activation effect of the calcination treatment was achieved at reaction temperatures that exceeded $60^{\circ}C$ and was enhanced as the temperature increased. The reactivity of the calcined kaolin with an alkaline solution was more enhanced with the solution of a higher concentration and with a solution prepared from sodium hydroxide rather than potassium hydroxide.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 추계학술대회논문집
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• pp.103-106
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• 2004

The new rheology fabrication process has been developed to rheo die casting and rheo forming process. Thixoforming process has disadvantages in terms of induction reheating process, scrap recycling, loss of raw material and cycle time. Therefore, to reduce the number of process, new rheology fabrication process with specially designed the rotational barrel type equipment has been proposed to apply in various part productions. The barrel type equipment, which could continuously fabricate the rheology materil, was specially designed to have a function to control cooling rate, shear rate and temperature. During the continuous rotation of barrel with a constant temperature, the shear rate is controlled with the rotation speed. The barrel surface has both the induction heating system and the cooling system to control the temperature of molten metal. By using this system, the effect of the rotation speed and the rotation time on the microstructure was widely examined. The possibility for the rheoforming process was investigated with microstructural characteristic.