• Title/Summary/Keyword: heating temperature and time

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EFFECT OF ADDED Si ON DENSIFICATION OF Ni-AI INTERMETALLIC COATING ON SPHEROIDAL GRAPHITE CAST IRON SUBSTRATES

  • Kim, Tetsuro ata;Keisuke Uenishi;Akira Ikenaga;Kojiro F. Kobayashi
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.726-731
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    • 2002
  • Reaction synthesis is a process to form ceramics, intermetallics and their composites from elemental powder mixture. Application of this process to a surface modification techniques has a possibilities to enable the process at a lower temperature or for a shorter time, although synthesized materials are likely to include voids and unreacted elements. This paper intend to examine the effect of Si addition to the mixture of Al and Ni on the densification of synthesized Ni-Al intermetallic compounds and to evaluate the surface properties of obtained coatings. By the Si addition, exothermic reaction temperature to form Ni-Al intermetallic was lowered to be below the melting point of Al. Si soluted $Al_3$Ni$_2$, $Al_3$Ni and $Al_{6}$Ni$_3$Si were mainly formed in the coating layer when powder mixture was heated to 973K for 300s. Besides, densification was enhanced by increasing hot press pressure, Si additions and heating rate. When the composition of eutectic Al-Si reaches 78%, void ratio of sintered compact reduced to 0.4%. It is caused by higher flowability of Al-Si liquid phase generated and its infiltration into the void. Since the hardness of NiAl(Si) compound (about 600HV) formed in the coating layer is higher than that of Ni-Al compound (about 400HV), coating layer with high density and superior wear property is obtained by hot press using reaction synthesis from Al-Ni-Si powder mixture.

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Carbon Nanotube Heater Generating High Heat Flux

  • Kang, Yong-Pil;Lee, Hyun-Chang;Kim, Duck-Jong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.530-530
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    • 2012
  • Many practical applications of carbon nanotubes(CNTs) have been proposed and there have been attempts to utilize CNT films as transparent electrodes for solar cells and displays. Our group has considered the use of the CNT film as a thin film heater (TFH) and proposed it for the first time and reported the thermal behavior of the TFH made of single walled CNTs. However, due to the relatively high electrical resistance of the CNT film, using the TFH in application areas requiring high heat flux has been a difficult problem. To overcome this obstacle, we adopted a 'branch electrodes' concept to increase the film conductance dramatically. If two branch electrodes are inserted into a TFH whose original electrical resistance is R, the total resistance will be reduced to R/9. Because of the increased aspect ratio, the resistance of each segmented TFH will be reduced to R/3. Furthermore, since they are connected in parallel, the total resistance reduces to R/9. This could be extended to n branch electrodes, and the total resistance of the film will be reduced to R/(n+1)2, if the resistance of electrodes are negligibly small. We fabricated the heaters with different number of branch electrodes. The number of branch electrodes of the fabricated heaters are 0, 2, 4, 8 and their electrical resistance are 101.4, 39.5, 20.0, $15.4{\Omega}$, respectively. We applied 20V to each heater and monitored the temperature variations. We could achieve high heating temperature even with low voltage supply. This technique could be applied to relevant industrial applications which need high power film heater.

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Measurement of Peltier Heat at the Solid/Liquid Interface and Its Application to Crystal Growth II : Measurement and Application (고/액 계면에서의 Peltier 열 측정 및 결정성장에의 응용 II : 측정과 응용)

  • Kim, Il-Ho;Jang, Kyung-Wook;Lee, Dong-Hi
    • Korean Journal of Materials Research
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    • v.9 no.11
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    • pp.1112-1116
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    • 1999
  • Thermoelectric effects on the temperature changes at the solid- and liquid-phase and its interface were studied by using the unidirectional solidification of $\textrm{Bi}_{2}\textrm{Te}_{3}$. Cooling or heating effects measured with current density. polarity and current passing time were quite different. By separating sole Peltier, Thomson and Joule heat theoretically and experimentally, the Peltier coefficient at the solid/liquid interface of $\textrm{Bi}_{2}\textrm{Te}_{3}$ was -1.10$\times\textrm{10}^{-1}$V, and the Thomson coefficients of solid- and liquid-phase were 7.31\times\textrm{10}^{-4}V/K, 5.77\times\textrm{10}^{-5}V/K, respectively. When D.C. passed from solid-phase to liquid-phase during the crystal growth of $\textrm{Bi}_{2}\textrm{Te}_{3}$ the crystal with more directionality was obtained owing to increase of the temperature gradient in liquid by the Peltier cooling. But in reverse current direction, the crystallinity was not changed significantly.

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Physico-mechanical Properties and Optimum Manufacturing Conditions of Bi-Sn Metal Alloy Impregnated Wood Composites (Bi-Sn 용융합금주입 목재복합체의 최적제조조건 및 물리·기계적 특성)

  • Park, Kye-Shin;Lee, Hwa-Hyoung;Kang, Seog Goo
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.6
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    • pp.691-699
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    • 2014
  • In order to improve the dimensional stability and durability of wood, this study attempted to impregnate bismuth (Bi) - tin (Sn) alloy metal with low melting temperature into solid woods of three species such as radiata pine, red oak and white oak, and investigated to determine an optimum condition of manufacturing the metal alloy-wood composites with natural wood grains. These Bi-Sn alloys were chosen for this study because they were harmless to human and melting at low temperatures. The composites resulted in high dimensional stability and low thickness swelling, and also showed much improved performance such as high bending strength, high hardness, high electric conductivity, and high thermal conductivity as floor materials. A proper impregnating condition of all specimens was determined as 10 minutes of the preliminary vacuum time, and $185^{\circ}C$ of the heating temperature. The proper processing condition for radiata pine wood was 2.5 minutes of the pressuring time at the pressure of $10kgf/cm^2$. For red oak wood, 10 minutes of the pressuring time at the pressure of $30kgf/cm^2$ were the proper condition. The proper manufacture conditions for white oak wood was determined as 10 minutes of the pressuring time at the pressure of $50kgf/cm^2$.

Study on Press-drying of Italian Poplar Board and its Effect on Improvement of Wood Property (이태리포푸라재(材)의 건조성(乾燥性) 및 성질개선(性質改善)에 관(關)한 연구(硏究))

  • Jung, Hee Suk
    • Journal of Korean Society of Forest Science
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    • v.37 no.1
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    • pp.17-30
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    • 1978
  • Press drying was used on italian poplar (Populus euamericana) to find the profitable means of drying. This study was designed to investigate the process of platen drying considering core temperature, drying time, current moisture content, drying rate, shrinkage and recovery, and green volume specific gravity, equilibrium moisture content and dimensional stability of press dried material and air dried material, The drying tests were conducted using 1.5 centimeter thick material at platen temperature of $175^{\circ}C$. The results were summarized as follows. 1. Core temperature was divided into three stages of drying characterized by period initial heating, plateau temperature and rising core temperature. Plateau temperature was 114 to $119^{\circ}C$. 2. The following predicting equations of drying time(y) in different core temperatures were developed for initial thickness($x_1$), initial moisture content ($x_2$) and final moisture content ($x_3$) 3. The predicting equaltion of current moisture content(u) was log u=4.658-0.060t as funtion of drying time(t) and that of drying rate(r) was log r=-2.797-0.049t. Current moisture content and drying rate of air drying were shown in figure 2. 4. The predicting equation of shrinkage in thickness direction(y) was log y=1.933+0.038t as function of drying time(t), and that of expansion in width direction was $y=-0.692+0.043t-0.001t^2$. 5. Thickness shrinkage was increased more than proportional at to pressure increase. Width shrinkage and thickness recovery was greatest at 35psi. 6. Green volume specific gravity of press dried material was 25% greater than that of air dried material. But equilibrium moisture content of press dried material was less 24% than that of air dried material. Antishrinkage efficiency of press dried material were obtained 27.7%.

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The Development of Infant Smart Incubator for Home use (가정용 영유아 스마트 인큐베이터 개발)

  • Eum, Sang-Hee
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.24 no.10
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    • pp.1325-1330
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    • 2020
  • New-born babies who require special attention medically are admitted often to incubator. Incubators are well equipped to fulfill take care of infants, but they have to hospital and so expensive. This paper proposes a smart incubator that can solve the problem of convenience and cost aspect of these incubators. Developed incubator enables near-field monitoring using Arduino Uno as the main control device and Bluetooth communication. The environment in the incubator measures temperature and humidity using a DHT22 sensor and the sound using a P5510 microphone. If the temperature and humidity data set by the user are lower or higher than the reference value, it is designed to operate the heating pad using the controller or turn on the fan to allow air circulation. The measured values in the incubator are displayed in real time on the user's smartphone monitoring screen and are programmed using app inventor. Developed incubators can help take care of infants at low cost in the home.

Formation and Thermal Properties of Amorphous Ti40Cu40Ni10Al10 Alloy by Mechanical Alloying (Mechanical Alloying에 의한 비정질 Ti40Cu40Ni10Al10 합금의 형성 및 열적특성)

  • Kim, Hyun-Goo
    • Journal of Powder Materials
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    • v.16 no.5
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    • pp.363-369
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    • 2009
  • The amorphization process and the thermal properties of amorphous Ti$_{40}$Cu$_{40}$Ni$_{10}$Al$_{10}$ powder during milling by mechanical alloying were examined by X-ray diffractometry (XRD), differential scanning calorimetry (DSC), and transmission electron microscopy (TEM). The chemical composition of the samples was examined by an energy dispersive X-ray spectrometry (EDX) facility attached to the scanning electron microscope (SEM). The as-milled powders showed a broad peak (2$\theta$ = 42.4$^{\circ}$) with crystalline size of about 5.0 nm in the XRD patterns. The entire milling process could be divided into three different stages: agglomeration (0 < t$_m$ $\leq$ 3 h), disintegration (3 h < t$_m$ $\leq$ 20 h), and homogenization (20 h < t$_m$ $\leq$ 40 h) (t$_m$: milling time). In the DSC experiment, the peak temperature T$_p$ and crystallization temperature T$_x$ were 466.9$^{\circ}C$ and 444.3$^{\circ}C$, respectively, and the values of T$_p$, and T$_x$ increased with a heating rate (HR). The activation energies of crystallization for the as-milled powder was 291.5 kJ/mol for T$_p$.

Smart Emotional Lighting Control System based on Mobile (모바일 기반의 스마트 감성조명 제어 시스템)

  • Hong, Sung-Il;Lin, Chi-Ho
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.6
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    • pp.3858-3864
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    • 2014
  • This paper proposes the smart emotion lighting control system of a mobile-based. The proposed smart emotional lighting control system to reduce the emotional lighting device, internal heat and the power consumption was configured to the android platform mobile device and zigbee module, emotional lighting device, lighting control module, power supply, and general-purpose transistor. The mobile device was to transmit the real-time control information to the emotional lighting device when connected to the system, and it was designed to control the emotion lighting device based on the control messages and status monitoring. In this paper, the efficiency verification results of the proposed smart emotional lighting control system showed that it was possible to control by emotion lighting control and the color temperature variable. The heating value and the power consumption could be reduced by21% and up to 48%, because of the controlled lighting using emotion language.

Hemicellulose Recovery from Lignocellulosic Material Hydrolyzed by Water (물로 가수분해된 섬유성 기질로부터 hemicellulose 회수)

  • Kim, Sung-Bae;Kim, Chang, Joon
    • KSBB Journal
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    • v.20 no.4
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    • pp.317-322
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    • 2005
  • Various recovery methods were investigated to maximize hemicellulose recovery from lignocellulosic material hydrolyzed by pure water. The pretreatment conditions of water hydrolysis were $170\~180^{\circ}C$ and 1 hour of reaction time. The percentage of hemicellulose solubilized increased as the temperature increased from 170 to $180^{\circ}C$. However, significant decomposition of sugar was observed at temperature of $180^{\circ}C$. From the results of water hydrolysis, the total amount of glucan in solid residue and liquid hydrolyzate was close to the total glucan in the original biomass. For hemicellulose, however, there was a significant difference between both contents. To prove this difference, various recovery methods were proposed. From the total sugar accountability (sugar in liquid + sugar in solid), it was confirmed that hemicellulose recovery in the hydrolyzate was increased if the product including both hydrolyzate and solid residue was physically stimulated by such as heating and ultrasound irradiation. This indicated that, in commercial scale processes that much bigger substrate sizes are used and a sufficient amount of leaching solvent can not be used after pretreatment, a significant amount of oligomers could be trapped in the solid matrix.

A New process for the Solid phase Crystallization of a-Si by the thin film heaters (박막히터를 사용한 비정질 실리콘의 고상결정화)

  • 김병동;정인영;송남규;주승기
    • Journal of the Korean Vacuum Society
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    • v.12 no.3
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    • pp.168-173
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    • 2003
  • Recently, according to the rapid progress in Flat-panel-display industry, there has been a growing interest in the poly-Si process. Compared with a-Si, poly-Si offers significantly high carrier mobility, so it has many advantages to high response rate in Thin Film Transistors (TFT's). We have investigated a new process for the high temperature Solid Phase Crystallization (SPC) of a-Si films without any damages on glass substrates using thin film heater. because the thin film heater annealing method is a very rapid thermal process, it has very low thermal budget compared to the conventional furnace annealing. therefore it has some characteristics such as selective area crystallization, high temperature annealing using glass substrates. A 500 $\AA$-thick a-Si film was crystallized by the heat transferred from the resistively heated thin film heaters through $SiO_2$ intermediate layer. a 1000 $\AA$-thick $TiSi_2$ thin film confined to have 15 $\textrm{mm}^{-1}$ length and various line width from 200 to 400 $\mu\textrm{m}$ was used as the thin film heater. By this method, we successfully crystallized 500 $\AA$-thick a-Si thin films at a high temperature estimated above $850^{\circ}C$ in a few seconds without any thermal deformation of g1ass substrates. These surprising results were due to the very small thermal budget of the thin film heaters and rapid thermal behavior such as fast heating and cooling. Moreover, we investigated the time dependency of the SPC of a-Si films by observing the crystallization phenomena at every 20 seconds during annealing process. We suggests the individual managements of nucleation and grain growth steps of poly-Si in SPC of a-Si with the precise control of annealing temperature. In conclusion, we show the SPC of a-Si by the thin film heaters and many advantages of the thin film heater annealing over other processes