• Title/Summary/Keyword: heating and grinding

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Effect of Heating Treatment of Silica Powder on Stirred Ball Milling Efficiency (규석 분말의 교반형 볼 밀 분쇄효율에 미치는 열처리의 영향)

  • 김병곤;박종력;최상근;이재장
    • Journal of the Korean Ceramic Society
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    • v.40 no.7
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    • pp.696-701
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    • 2003
  • The grinding efficiencies of silica powder in a small scale stirred ball mill were investigated by energy consumption estimate. Comparing with a non-treated silica powder and a heating treated silica powder, it was found that a silica powder cooled in room temperature after heating treatment at 600∼900$^{\circ}C$ consumed lower grinding energy than non-treated silica powder, and a silica powder quenched after heating treatment consumed lower grinding energies about 52∼62%, in case of dry grinding. Additionally, if heating treated silica powder grind in wet method, energy consumption will be decreased about 40% than in dry grinding, and the dependency of the particle size to the grinding efficiency, quenching significantly improved it.

Extraction and Mixing Effects of Grape (Campbell) Seed Oil

  • Kang, Han-Chul;Min, Young-Kyoo;Hwang, Jong-Taek;Kim, Si-Dong;Kim, Tae-Su
    • Journal of Applied Biological Chemistry
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    • v.42 no.4
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    • pp.175-179
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    • 1999
  • Grape seed oil was extracted using different preparatory treatments as follows: (1) grinding, (2) grinding and roasting, (3) grinding and wet- roasting, (4) grinding, roasting, and wet-roasting, and (5) grinding, wet-roasting, and wet-roasting. The highest antioxidant activity was obtained from the sample with the method (2). Initial states of oxidation were similar except method (1) that showed more oxidized state, being P.O.V.8. Acid values were observed in the range from 1.42 to 1.89. The lowest acid value was found as 1.42 in method (1) and those of others were somewhat higher, indicating that heating process of roasting produced some free fatty acids. From the results of sensory evaluation, the best odor and taste were obtained from the methods (2) and (3). Repetitive procedure of wet-roasting, like method 5, caused some loss of flavor components and decrease in the sensory evaluation score. Addition of grape seed oil (method 2) to soybean and perilla oil at the level of 20% retained considerable antioxidant activities as much as 4.3 and 5 times, respectively, than 100% soybean or perilla oil stored for 12 weeks. When soybean or perilla oil was mixed with 20% grape seed oils, P.O.V. decreased to half of that of unmixed oils.

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Synthesis of lanthanum oxyfluoride by grinding lanthanum oxide with poly (tetrafluoroethylene)

  • Lee Jaeryeong;Ahn Jonggwan;Kim Dongjin;Shin Heeyoung;Chung Hunsaeng;Saito Fumio
    • 한국지구물리탐사학회:학술대회논문집
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    • 2003.11a
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    • pp.624-628
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    • 2003
  • Lanthanum oxyfluoride can be synthesized by mechanochemical (MC) reaction between lanthanum oxide ($La_2O_3$) and polytetrafluoroethylene (PTFE, ($({CF_2CF_2}_n)$) in air using a planetary mill. MC reaction between the two materials induced from intensive grinding operation. The MC reaction is almost finished by 240min, and the products ground for 240min or more are composed of LaOF, amorphous $La(CO_3)F$ and amorphous carbon (C). Heating this MC reaction products at $600^{\circ}C$ enables us to eliminate amorphous C and decompose $La(CO_3)F$ into LaOF, so that pure LaOF material can be obtained as the final product. The average particle size of the final product (purified LaOF) is around few ten nanometers.

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Variation of Water Content and Thermal Behavior of Talc Upon Grinding: Effect of Repeated Slip on Fault Weakening (활석 분쇄에 따른 함수율 및 열적거동 변화: 단층의 반복되는 미끌림이 단층 약화에 미치는 영향)

  • Kim, Min Sik;Kim, Jin Woo;Kang, Chang Du;So, Byung Dal;Kim, Hyun Na
    • Journal of the Mineralogical Society of Korea
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    • v.32 no.3
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    • pp.201-211
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    • 2019
  • The particle size and crystallinity of fault gouge generally decreases with slip. Phyllosilicates including talc are known to be present in fault gouge and play an important role in fault weakening. In particular, the coefficient of friction varies depending on the presence of a water molecule on the surface of mineral. The purpose of this study is to investigate the effect of talc on fault weakening by changing the water content and dehydration behavior of talc before and after grinding, which systematically varied particle size and crystallinity using high energy ball mill. Infrared spectroscopy and thermal analysis show that the as-received talc is hydrophobic before grinding and the water molecule is rarely present. After grinding up to 720 minutes, the particle size decreased to around 100 ~300 nm, and in talc, where amorphization proceeded, the water content increased by about 8 wt.% and water molecule would be attached on the surface of talc. As a result, the amount of vaporized water by heating increased after grinding. The dihydroxylation temperature also decreased by ${\sim}750^{\circ}C$ after 720 minutes of grinding at ${\sim}950^{\circ}C$ before grinding due to the decrease of particle size and crystallinity. These results indicate that the hydrophobicity of talc is changed to hydrophilic by grinding, and water molecules attached on the surface, which is thought to lower the coefficient of friction of phyllosilicates. The repeated slip throughout the seismic cycle would consistently lower the coefficient of friction of talc present in fault gouge, which could provide the clue to the weakening of matured fault.

An Experimental Study on Heating Manufacture of Recycled Aggregate by Design of Experiment (실험계획법을 이용한 가열방식의 순환굵은골재 제조를 위한 실험적 연구)

  • Nam, Eun-Yong;Hwang, Sun-Bok
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.8 no.1
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    • pp.11-17
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    • 2013
  • The use of wasted concrete can settle the environmental pollution and shortage of natural aggregate. However, recycled aggregate includes substantial amount of cement paste, so that these aggregates are more porous, and less resistant to mechanical actions than natural aggregates. Recently, the new manufacturing processes of high quality recycled aggregates were suggested such as heating. In this paper, for the purpose of manufacture of high quality recycled aggregates, the heating processes was considered to the existing process of recycled aggregates. To find the optimum process, the experiment was performed through the statistical design of experiment. The heating temperatures of 4 levels (300, 450, 600 and $750^{\circ}C$) and heating duration time (5, 20, 40, 60minute) were main experimental variables. Through the test results, it was found that the optimum manufacturing condition of coarse recycled aggregate was evaluated to be $600^{\circ}C$ and 40minute.

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Quality Improvement of Recycled Aggregates from Waste Concrete by the heating and grinding

  • Kim, Hyung-Seok;Han, Gi-Chun;Ahn, Ji-Whan;Park, Jae-Seok;Kim, Hwan;Kim, Kyung-Soo
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.571-575
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    • 2001
  • To examine the grinding effect through preheating of waste concrete as a way of retrieving coarse aggregates from waste concrete, the removal rates of cement mortar and paste of both recycled aggregates and heated and grinded ones were investigated. As the preheating temperature increased, the removal rate of cement mortar from waste concrete was raised, and this kind of removal hardly affected the abrasion rate and specific gravity of aggregates. On the other hand, when it was treated over 40$0^{\circ}C$ of preheating temperature, the absorptance was reduced to less than 2.17, and cement mortar was effectively separated from waste concrete. It could meet the Korean Standards on recycled aggregates for concrete, and it is expected to expand the scope of utilization by making it possible to retrieve the aggregates which have the properties close to natural aggregates.

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A parameter study on the pre-heat treatment for the fabrication of a large grain YBCO bulk superconductor without intermediate grinding step

  • Hong, Yi-Seul;Kim, Chan-Joong;Lee, Hee-Gyoun
    • Progress in Superconductivity and Cryogenics
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    • v.22 no.1
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    • pp.1-6
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    • 2020
  • This is a parameter study for the direct fabrication of a large grain YBCO bulk superconductors using Y2O3, BaCO3 and CuO powders without any grinding step. The cracks, which have been formed due to volume contraction during calcination step, have been prevented by controlling the heating rate at 930~950 ℃. It has been observed that multi-grain growth has occurred due to the dissolution of Sm123 seed due to the retention of carbon in Ba-Cu-O melt. In order to accelerate the carbon release in prior calcination heat treatment, the reduction of pellet thickness and the drilling of artificial holes have been applied. Single-grain YBCO bulk superconductor has been successfully fabricated by stacking multiple thin slab. However, the crack formation has been rather prominent for the compact with artificial holes. The use of buffer pellet, which is supposed to act as diffusion barrier, has prevented the dissolution of Sm123 seed crystal and has led to the growth of single grain of high content of carbon containing specimen.

Processing of Sausage Using Duck Mechanically Deboned Meat (오리 기계발골육을 이용한 Sausage 제조)

  • 강동수;최옥수;박욱민
    • Journal of Life Science
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    • v.12 no.1
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    • pp.8-15
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    • 2002
  • In this paper we dealt with processing of sausage using duck mechanically deboned meat(duck-MDM). The results may be summarized as follows : 1) after semi-thawing of freezing duck-MDM at $25^{\circ}C$ for 3 hours and cutting as thin, 2) alkali washing at low temperature for 4 hours by 0.2% NaHCO$_3$and 0.15% NaCl, 3) curing at low temperature for 4 hours, 4) after washing and dehydrating(moisture 80%), 5) grinding at low temperature for 55 minutes by silent cutter such as 1st grinding for 10 minutes added only dehydrated meat, 2rd grinding for 30 minutes added salt in 1st grinded meat and 3rd grinding for 15 minutes added other additives, 6) after quick casing in PVDC film and heating at 9$0^{\circ}C$ for 80 minutes, 7) cooling to below room temperature. The additives added at 3rd grinding process were Polymix-CA(0.3%), Polymix-CS(0.3%), polyphosphate(0.3%), sugar(4.2%), potato starch(8.0%), pyre-phosphates(0.3%), isolated soy protein(7.0%), MSG(0.2%), onion powder(0.5%), garlic powder(0.1%), nutmeg (1.5%), potassium sorbate(<0.1%), food red no.40(0.0075%), egg albumin(7.0%) and gluten(3.0%).

Separation of Radionuclide from Dismantled Concrete Waste (해체 콘크리트 폐기물로부터 방사성핵종 분리)

  • Min, Byung-Youn;Park, Jung-Woo;Choi, Wang-Kyu;Lee, Kune-Woo
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.7 no.2
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    • pp.79-86
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    • 2009
  • Concrete materials in nuclear facilities may become contaminated or activated by various radionuclides through different mechanism. Decommissioning and dismantling of these facilities produce considerable quantities such as concrete structure, rubble. In this paper, the characteristics distribution of the radionuclide have been investigated for the effects of the heating and grinding test for aggregate size such as gravel, sand and paste from decommissioning of the TRIGA MARK II research reactor and uranium conversion plant. The experimental results showed that most of the radionuclide could be removed from the gravel, sand aggregate and concentrated into a paste. Especially, we found that the heating temperature played an important role in separating the radionuclide from the concrete waste. Contamination of concrete is mainly concentrated in the porous paste and not in the dense aggregate such as the gravel and sand. The volume reduction rate could be achieved about 80% of activated concrete waste and about 75% of dismantled concrete waste generated from UCP.

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