• 소성∙가공
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• 제13권5호
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• pp.441-448
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• 2004

Heat treatment is one of the critical manufacturing processes that determine the quality of a product. This paper presents experimental and analytical results for the quench of a ring gear in stagnant oil. The goal of this study is to develop heat transfer predicting model in an overall analysis of the quenching process, Thermal conductivities which are dependant on temperatures and convection coefficients which are obtained by inverse method are used to develop the accurate heat transfer model. The results of heat transfer model have a good agreement with experimental results.

• 열처리공학회지
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• 제7권4호
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• pp.288-297
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• 1994

In this study, lattice parameter, binding energy and microstructures of TiC layer according to the addition of Fe, Cr were investigated in the reactive deposition coating. From the results, the lattice parameters of the TiC layers by using ferro-titanium as a precursor were 4.329~4.339A but the lattice parameters of the TiC layers formed by ferro-titanium and ferro-chromium decreased to 4.316~4.330A. The hardness of the former's was HV(100g) 3,000~3,400kg/mm and the hardness of the latter's was HV (100g) 3,800~3,900. But, regardless of Cr and Fe, the binding energy of TiC layers were 454.75 eV for $Ti2p_{3/2}$ and were 281.85 eV for Cls. Meanwhile, the TiC layers were densified by addition of Fe, Cr and internal defects were reduced Therefore. it can be concluded that the remarkable hardness increment was obtained by the improvement of microstructures of TiC rather than the increase of bond strength or Peierls stress.

• 열처리공학회지
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• 제29권2호
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• pp.51-55
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• 2016

The P/M processing of titanium aluminide using amorphous TiAl is developed by which it is possible to overcome inherent fabricability problems and to obtain a fine microstructure. A high quality amorphous TiAl powder produced by reaction ball milling shows clear glass transition far below a temperature at the onset of crystallization in differential scanning calorimetry above a heating rate of 0.05 K/s. We obtained a fully dense compact of amorphous TiAl powders, encapsulated in a vacuumed can, via viscous flow by hot isostatic pressing (HIP). Isothermally annealing of HIP'ed amorphous compact under a pressure of 196 MPa shows a progressive growth of ${\gamma}-TiAl$ phase with ${\alpha}2$ ($Ti_3Al$), which is characterized by increasing sharpness of X-ray peaks with temperature. Fully dense HIP'ed compact of titanium aluminide TiAl shows a high hardness of 505 Hv, suggesting strengthening mechanisms by sub-micron sized grain of ${\gamma}-TiAl$ and particle-dispersion by second phase constituent, ${\alpha}2$.

• 열처리공학회지
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• 제28권6호
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• pp.315-321
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• 2015

Friction stir processing (FSP) was applied to fabricate AZ31/CNT (Carbon Nano Tube) surface composite for improvement of surface hardness of AZ31 Mg-based alloy. The effects of traverse speed of rotating tool and volume fraction of CNT (i.e., groove depth of 3 mm and 4 mm) on the soundness and hardness of the composite layer were investigated. Multi-walled CNTs were fully filled in a machined groove and stirring tool was rotated at the speed of 1400 rpm. Only under the tool traverse speed of 25 mm/min for the specimen with a groove depth of 3 mm, surface composite layer with no defect was successfully produced. Increased hardness of about 35% was observed in the composite layer.

• 한국주조공학회지
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• 제32권6호
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• pp.284-288
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• 2012

The effects of Si content on the variation of microstructure and processing window of austempered ductile cast iron were investigated. Four different Si contents between 2.42 and 3.37 wt.% were used. The influence of silicon on the microstructure and processing window of these materials were studied. Austenitizing was performed at $900^{\circ}C$ for 60min and austempering temperature were both $340^{\circ}C$ and $360^{\circ}C$ and austempering time were for 4min upto 119min and for 5min upto 160min respectively. After heat treatment, the evolution of stage I and stage II were performed by optical metallography, XRD, hardness test. The results showed that $t_2$ was delayed as Si contents was increased due to the fact that Si retarded the formation of cementite ($Fe_3C$). The high silicon content promoted the stability of the metastable two-phase combination of austenite and ausferrite.

• Progress in Superconductivity
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• 제9권1호
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• pp.115-118
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• 2007

This study investigated the effects of different kinds of seed crystals with miscut angles and pretreatment on the characteristics of a RE-123 superconductor processed by a top-seeded melt-growth (TSMG) method. When the seed crystal was heat-treated in an oxygen atmosphere, the surface structure was cleaned removing hydroxide. When the seed crystal had a miscut angle, in addition, the surface structure showed a well defined hill-and-valley structure after heat-treatment. A better microstructure, with a well-distributed small RE-123 phase, was obtained using a high miscut angle after heat-treatment in an oxygen atmosphere. As a result of the microstructure improvement, the magnetic characteristics also improved. The experimental result can be explained by reduction of nucleation activation energy.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2001년도 The 6th International Symposium of East Asian Resources Recycling Technology
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• pp.173-178
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• 2001

The materials processing factors such as remelting and casting, heat treatment and microstructure, sheet rolling and can body forming in the aluminum can-to-can recycling procedure have been investigated. Aluminum used beverage can(UBC) was remelted together with virgin aluminum. The ceramic filter was used during casting to remove large impurities. As-cast microstructure was composed of large intermetallic compound (mainly $\beta$ -phase) distributed in the aluminum matrix. By heat treatment, $\beta$ -phase was transformed to $\alpha$ -phase which was also formed from $Mg_2$Si particles. The heat treated ingots were hot-rolled at 48$0^{\circ}C$ and cold-rolled to thin sheets. Can making from this thin sheets was successful and earing was measured after can making. There was a critical cold reduction rate for minimum earing. Some cracks were initiated from the impurity particles which was not removed during filtering.

• 한국식품영양학회지
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• 제17권2호
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• pp.186-192
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• 2004

본 연구는 다시마 가공식품과 증간소재를 개발하기 위하여 다시마의 연화방법을 검토하였다. 그 결과 가열하면서 sodium triphospto를 0.3％첨가한 것이 연화에 가장 좋은 효과를 나타내었으며 이 때 다시마의 유연성과 퍼짐성도 좋은 것으로 나타났다. 다시마의 블랜칭은 microwave를 사용하는 것이 연화에 좋았으며, 그 정도는 microwave>스팀>끓는 물 순이었다. 또한 블랜칭할 경우 sodium triphosphate를 0.3％ 첨가하면 연화에 시너지효과가 나타났다. 색깔의 변화는 p<0.05 수준에서 블랜칭 방법과 연화제 첨가량에 대한 유의성은 확인되었다.

• 한국작물학회:학술대회논문집
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• 한국작물학회 2022년도 추계학술대회
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• pp.314-314
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• 2022

In the production of rice flour, wet milling is a method of milling rice after soaking it in water, and it takes a lot of time and cost from milling to drying. To overcome this problem, the floury type rice was developed for dry milling and it is known to have round starch granules, low content of damaged starch after milling, and a starch structure similar to wheat. Because of its unique properties different from normal rice, it is necessary to research on processing and characteristics of floury-type rice to expand its utility in the food industry. Therefore, this study aimed to prepare the pregelatinized floury type rice (Baromi2) by autoclave and investigate their physicochemical properties. As the heat treatment time increased, the brightness decreased from 83.8 to 76.8, however, both redness and yellowness increased from 0.57 to 4.5 and from 14.58 to 21.13, respectively. Despite of same treatment time, soaking in water (10 min) before autoclaving increased the solubility and swelling power of Baromi2 over 2 times. The peak viscosity of native Baromi2 was over 2000 RVU, on the other hand, there was a significantly decrease to less than 1000 RVU of pregelatinized Baromi2. Heat treatment without immersion caused partial gelatinization of starch, resulting that some starch granules maintaining their integrity. Whereas there were no starch granules in heat treatment with soaking in water due to complete gelatinization. This study would be helpful to the suggestion of using heat-treated floury-type rice as an intermediate material in the food industry in the future.

• 한국식생활문화학회지
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• 제36권5호
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• pp.484-491
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• 2021

This study investigated the effect of dry heat treatment (DHT) on the physicochemical properties of hard type (HR) and floury type (FR) rice to improve the processing aptitude of rice flour. The rice flour was heated at 130℃ for 0, 2 and 4 hours, and the color value, water absorption index (WAI), water soluble index (WSI), swelling power, solubility, pasting properties, particle shape and the X-ray diffraction were measured. After DHT, the L value of rice flour decreased, and the b value increased. The WAI, WSI, swelling power and solubility of HR and FR increased with the increase of treatment time. The cold viscosity and setback increased, while breakdown decreased. Cracks and lumps formed with fine particles were observed. The X-ray diffraction pattern was A-type, while the diffraction intensity decreased. According to the results of the two-way analysis of variance (ANOVA) test, the hydration and pasting properties were significantly different between HR and FR and were affected by DHT time. The results suggest that the properties of modified rice flour by DHT can be used in the food industry.