• 한국레이저가공학회지
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• 제14권1호
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• pp.25-29
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• 2011

Micromachining of photosensitive glass by UV exposure, heat treatment, and etching processes is reported. Like photoresist, the photosensitive glass is also classified into positive and negative types by development characteristics. For the positive type, the exposed area is crystallized and etched away during the etching process in HF solution, whereas the unexposed area is crystallized and etched away for the negative type. The crystallized area of the photosensitive glass has an etch rate approximately 30~100 times faster than that of the amorphous area so that it becomes possible to fabricate microstructures in the glass. Based on the unique properties of glass such as high optical transparency, electrical insulation, and chemical/thermal stability, the glass micromachining technique introduced in this work could be widely applied to various devices in the fields of electronics, bio engineering, nanoelectonics and so on.

• 열처리공학회지
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• 제2권2호
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• pp.68-83
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• 1989

Physical metallurgy aspects of gaseous ferritic nitrocarburising are reviewed in the light of basic studies undertaken since 1975 which have illustrated inconsistencies between the iron-carbon-nitrogen ternary phase diagram at $570^{\circ}C$ and the experimental observation of the co-existence of the ${\varepsilon}$ carbonitride phase and ferrite. Thermodynamic investigations by Xu and Li together with those by Slycke et al are reviewed to illustrate compatability between a modified isothermal section of the Fe-C-N system and the formation and growth of a monophased ${\varepsilon}$ structure under a variety of processing conditions. The implications of the modified diagram in terms of innovations in industrial ferritic nitrocarburising practice are discussed, together with limitations on the control of the process. The importance of the developing technology of black nitrocarburising for enhanced wear, fatigue, and corrosion resistance is emphasised. Basic studies and industrial status of austenitic nitrocarburising treatments are also reviewed, which highlight the importance of substrate strengthening for high load bearing applications of anti-scuff thermochemical treatments.

• Fibers and Polymers
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• 제3권2호
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• pp.60-67
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• 2002

In the present study, the fluorescence behavior ova phenylethynyl-terminated imide (LaRC PETI-5) resin, a bismaleimide (BMI) resin, and various LaRC PETI-5/BMI blends with different blend compositions has been characterized as a function of heat-treatment temperature, using a steady-state fluorescence technique with a front-face illumination method far solid-state films. It is observed that there are distinguishable changes in the spectral shape, size, and position of fluorescence with varying heat-treatment temperature in the pure and blend samples. The result is qualitatively explained in terms of charge transfer complex formation as well as microenvironmental change with local mobility and viscosity occurring in the LaRC PETI-5, BMI, and their blends during the cure process. The result also implies that a steady-state fluorescence technique may be a useful tool to understand the processing conditions of polyimides and their blends in the film form on the basis of their thermo-photophysical responses.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.118-119
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• 2006

The development of Fe-based metal matrix composites (MMCs) with high content of hard phase has been approached by combining the use of advanced powder metallurgy techniques like high-energy milling (HEM), cold isostatic pressing (CIP) and vacuum sinterings. A 30% vol. of NbC particles was mixed with Fe powder by HEM in a planetary mill during 10h, characteristing the powder by the observation of morphology and microstructure by scanning electron microscopy (SEM). After of sintering process the variation of density, hardness,carbon content and the microstructural changes observed, permits to find the optimal conditions of processing. Afterwards, a heat treatment study was performed to study the hardenability of the composite.

• 열처리공학회지
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• 제22권4호
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• pp.223-227
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• 2009

The feasibility of plasma electrolytic polishing technology of stainless steel was examined. The results show that austenitic stainless steel can be polished clearly using potentiostatic regimes with various concentration of ammonium sulfate ($(NH_4)_2SO_4$) solution above certain initial temperature. The equipment and deposition produces for polishing process are described and the effect of processing parameters on the characterizations polished-samples has been investigated.

• 열처리공학회지
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• 제34권5호
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• pp.211-217
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• 2021

To predict mechanical properties of secondary hardening martensitic steels, a machine learning ensemble model was established. Based on ANN(Artificial Neural Network) architecture, some kinds of methods was considered to optimize the model. In particular, interaction features, which can reflect interactions between chemical compositions and processing conditions of real alloy system, was considered by means of feature engineering, and then K-Fold cross validation coupled with bagging ensemble were investigated to reduce R2_score and a factor indicating average learning errors owing to biased experimental database.

• 열처리공학회지
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• 제35권5호
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• pp.255-261
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• 2022

In this work, the strain-amplitude independent and strain-amplitude dependent damping capacities of Mg-5%Sn alloy have been investigated as a function of its age-hardening response. The hardness increased with an increase in aging time, reached a peak value after 48 h, and then it gradually decreased. The damping capacities of the Mg-5%Sn alloy exhibited a decreasing tendency in the order of solution-treated, under-aged, peakaged, and over-aged states in the strain-amplitude dependent region, whereas they increased continuously with aging time in the strain-amplitude independent region. The microstructural examination during aging revealed that the lower concentration of Sn solutes in the α-(Mg) matrix and the lower density of the Mg₂Sn precipitate particles may well be the crucial factors for better damping values in the strain-amplitude independent and strain-amplitude dependent regions, respectively.

• 열처리공학회지
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• 제37권3호
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• pp.114-120
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• 2024

AA 2026, which is used as an aviation material, is an improved version of 2024 and has higher physical properties, and is a material that has the potential to be applied to supersonic aircraft to be developed in the future. However, when an aircraft exceeds supersonic speeds, the surface heats up and the material must be resistant to this. Therefore, this study confirmed the high-temperature properties of AA 2026, an aviation structural material. AA 2026, solution treated at 500℃ for 4hr, was naturally aged at room temperature for more than 168 hr. Changes in microstructure and physical properties were confirmed over several hours of exposure to 100℃, 200℃, and 300℃, respectively. As a result of microstructure analysis, there was no significant change at 100℃, and from 200℃, GPB, a strengthening mechanism, grew and formed an S Phase. It was confirmed that the S Phase grew as the exposure time increased. Through a tensile test, it was confirmed that physical properties deteriorated as the precipitates grew. However, it was confirmed that the properties were stably maintained at 100℃, which is the temperature when the speed of a supersonic aircraft is less than Mach 2.

• 한국산학기술학회논문지
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• 제18권9호
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• pp.61-67
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• 2017

프레스금형 제작 시 사용목적에 맞는 적합한 소재선택과 빠른 가공방법에 대한 연구는 금형제작시간을 줄이고 금형원가를 절감하는데 절대적으로 필요한 연구분야이다. 특히 장수명 프레스금형을 개발하기 위해선 열에 대한 고찰이 반드시 이루어져야 한다. 일반적으로 프레스금형의 주요부품 소재로는 Cr, W계 저합금 공구강, 고탄소 고크롬강, 고속도강 등 냉간 금형용 합금공구강이 많이 쓰이고 있다. 프레스금형부품을 가공하는 데는 주로 공작기계와 와이어 컷 방전가공을 사용하고 있다. 가공공정에 따라 금형부품의 가공시간 및 수명이 많은 차이가 난다. 밀링가공과 연삭가공으로 제작된 부품의 경우 제작시간과 비용은 많이 드는데 비해 금형의 수명이 길고 밀링가공과 와이어 컷 방전가공을 사용하면 제작시간과 비용은 절감되는 반면 금형수명은 줄어드는 현상이 나타난다. 따라서 본 연구에선 가공시간과 비용이 절감되는 가공방법으로 열처리를 사용하여 금형의 사용수명을 향상시키는 방법에 대해 고찰하고자 한다. 밀링가공-연삭가공, 밀링가공-와이어 컷 방전가공, 밀링가공-와이어 컷-고온템퍼링, 3가지 가공방법으로 시편을 제작하여 가공표면과 중심부를 SEM, EDS분석 및 표면조도분석으로 문제점을 고찰하였고 밀링가공-와이어 컷 방전가공-고온템퍼링의 가공방법으로 밀링가공-연삭가공과 동일한 금형의 수명을 만드는 방법을 도출하였다.

• 소성∙가공
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• 제15권2호
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• pp.143-147
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• 2006

Effect of processing condition on the hot extrusion of Al-Zn-Mg-Sc alloy was investigated. For this purpose, hot compression test and FE-simulation were conducted via Thermecmaster-Z and DEFORM-3D, respectively. The microstructure evolution during hot extrusion and post heat-treatment was investigated and deformation mechanisms were analyzed by constructing processing map. FE-simulation results show that the temperature difference between container and billet has considerable influence on the final shape of extruded T-shape bar. The relation between applied load and processing time was predicted by the FE-analysis as well as punch speed vs. stroke chart.