• Title/Summary/Keyword: heat treatment processing

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Characteristics of Strengthening for Thin Metals by Laser Beam (레이저 빔에 의한 박판금속의 강화특성)

  • Yang, Se-Young;Choi, Seong-Dae;Kim, Gi-Man;Jun, Jea-Mok;Gong, Byeong-Chae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.2
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    • pp.216-223
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    • 2010
  • The general way to process the surface by means of the laser was heat treatment for strengthening the surface hardness. They have used the laser for changing the property of the surface, especially for metal. Generally, it is recent increasing tendency to use the thin plate panel for making things smaller and lightweight. However, thin plate should be strengthened or let the thin plate panel have moment of inertia by means of engraving the groove or wave on them for lightweight and strengthening. Therefore it is expected that the thin plate panel can be harder and more stable through processing the metal surface by laser beam irradiation and the hardness of thin plate possibly can be also changed how many parts of them are harden. Through this research, it can be grasped how the hardness and mechanical characteristic changes according to width and depth of groove by laser affect the max stress by the ratio of $A_H/A_T$ (hardening area/total area) and characteristic of displacement and structural characteristic for making the thin plate harder by the strengthening metal surface of thin plate by laser through the experiment and analysis of FEA can be presented.

Processing Conditions of Low-Salt Fermented Squid and Its Flavor Components 3. Characterization of Protease Produced by Pseudomonas D2 Isolated from Squid Jeotkal (저염 오징어젓갈 제조 방법 및 향미 성분 3. 오징어젓갈에서 분리한 Pseudomonas D2가 생성하는 Protease의 효소학적 특성)

  • 허성호;이호재;김형선;최성희;김영만
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.24 no.4
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    • pp.636-641
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    • 1995
  • Proteolytic activities were compared using three species involving in squid jeotkal fermentation and showing positive reaction upon casein test : Pseudomonas D2, Flavovacterium odoratum and Acinetobacter calcoaceticus. Pseudomonas D2 produced highest activity of protease at 72h when incubated in our own modified medium(polypeptone, 0.5% ; tryptone, 0.5% ; NaCl, 3% ; pH, 7.5). Thus, this specie was selected for the further study. The growth pattern was coincided with the production of protease. Thus purification of protease was proceeded by ethanol precipitation, sephadex G-100 gel filtration, and DEAE sepharose ion exchange chromatography. The purified protease showed highest activity at pH 7.0 and 5$0^{\circ}C$. The enzyme was very stable over the wide ragnes of the temperature ; even with one hour heat treatment at 7$0^{\circ}C$, the enzyme showed substantial amount of the activity toward casein. In addition, the enzyme was stable over the wide range of pH. Molecular weight of the protease was determined to be 17.4 kD by SDS-PAGE.

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A Novel Solid Phase Epitaxy Emitter for Silicon Solar Cells

  • Kim, Hyeon-Ho;Park, Seong-Eun;Kim, Yeong-Do;Ji, Gwang-Seon;An, Se-Won;Lee, Heon-Min;Lee, Hae-Seok;Kim, Dong-Hwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.480.1-480.1
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    • 2014
  • In this study, we suggest the new emitter formation applied solid phase epitaxy (SPE) growth process using rapid thermal process (RTP). Preferentially, we describe the SPE growth of intrinsic a-Si thin film through RTP heat treatment by radio-frequency plasma-enhanced chemical vapor deposition (RF-PECVD). Phase transition of intrinsic a-Si thin films were taken place under $600^{\circ}C$ for 5 min annealing condition measured by spectroscopic ellipsometer (SE) applied to effective medium approximation (EMA). We confirmed the SPE growth using high resolution transmission electron microscope (HR-TEM) analysis. Similarly, phase transition of P doped a-Si thin films were arisen $700^{\circ}C$ for 1 min, however, crystallinity is lower than intrinsic a-Si thin films. It is referable to the interference of the dopant. Based on this, we fabricated 16.7% solar cell to apply emitter layer formed SPE growth of P doped a-Si thin films using RTP. We considered that is a relative short process time compare to make the phosphorus emitter such as diffusion using furnace. Also, it is causing process simplification that can be omitted phosphorus silicate glass (PSG) removal and edge isolation process.

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Development of Fluorine-free MOD Precursor Solution for fabricating REBCO Superconducting Films (REBCO 초전도 박막제조를 위한 Fluorine-free MOD 전구체 용액 개발)

  • Kim, Byeong-Joo;Lim, Sun-Weon;Kim, Ho-Jin;Hong, Gye-Won;Lee, Hee-Gyoun
    • Progress in Superconductivity
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    • v.7 no.2
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    • pp.152-157
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    • 2006
  • New precursor solution with dichloroacetic acid (DCA) was developed for fabricating high $J_c$ REBCO film. DCA based-precursor solution was coated on $LaAlO_3$(001) substrate by dip coating method. Processing parameters such as oxygen partial pressure, water vapor, ramping rate and pyrolysis temperature were controlled in order to obtain a good epitaxial film. The film with thickness of 0.5 micrometer was obtained by single coating and no crack was observed at calcined films. Oxygen partial pressure was controlled in the range of $100{\sim}1,000$ ppm and conversion heat treatment was carried out at the temperature range of $705-765^{\circ}C$. A critical transition temperature ($T_c$) of 90 K and a critical transport current density ($J_c$) of $>0.5\;MA/cm^2$ (77 K and self-field) were obtained for the GdBCO film. It is thought that fluorine-free MOD solution using DCA is promising precursor solution for fabricating high quality REBCO films.

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Preparation and Properties of Functional PET Textured Yarn Coated with Aromatic Polymer (아로마틱 고분자를 적용한 기능성 PET 가공사 제조 및 특성)

  • Ahn, Dajeong;Choi, Chulhoon;Lee, Jaewoong;Lee, Sang Oh
    • Textile Coloration and Finishing
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    • v.29 no.3
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    • pp.148-154
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    • 2017
  • Many researches have been made on the processing technology of Poly(ethylene terephthalate) (PET), which is widely used for clothing and non-clothing applications. In this study, we coated PET filaments with m-aramid resin to improve heat resistance and antimicrobial properties. In order to enhance adhesion between PET and m-aramid polymer, the adhesive polymer was coated on the PET filaments using a winding speed of 100m/min and then treated with m-aramid. Scanning electron microscopy was used to analyze the surface of the adhesive polymer and m-aramid treated PET filament. The change of initial degradation temperature according to treatment was confirmed by thermogravimetric analysis. Antimicrobial activity analysis using bacterial reduction method showed that PET filament treated with adhesive polymer and m-aramid had an increased antibacterial effect compared to untreated PET filament.

Study on crystal texture of PIT processed Bi-2223 multi-filamentary tape (PIT 공정으로 제조한 Bi-2223 다심 고온 초전도 선재의 결정 배향성에 관한 연구)

  • Choi, J.K.;Oh, S.S.;Ha, H.S.;Yang, J.S.;Yun, J.K.;Lee, N.J.;Ha, D.W.;Kwan, Y.K.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.04a
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    • pp.59-63
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    • 2002
  • The purpose of this paper is to investigate the crystal texture of the 2223 phase and its relationship with PIT processing parameter. Ag-sheathed Bi-2223 multi-filament tapes were prepared by changing rolling reduction ratio. We analysed the degree of texture for 2223 phase after heat-treatment. According to X-ray pole-figure, the texture of the filaments located near surface and center were not so different each other for all rolling conditions. we found a little higher degree of texture for 60% rolling reduction. But its difference is not so high compared with those tapes with a lower rolling reduction ratio. Reaction induced texturing seemed to contribute with a large portion under present condition.

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Proton Conductivity of Niobium Phosphate Glass Thin Films

  • Kim, Dae Ho;Park, Sung Bum;Park, Yong-il
    • Korean Journal of Materials Research
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    • v.28 no.5
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    • pp.308-314
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    • 2018
  • Among the fuel cell electrolyte candidates in the intermediate temperature range, glass materials show stable physical properties and are also expected to have higher ion conductivity than crystalline materials. In particular, phosphate glass has a high mobility of protons since such a structure maintains a hydrogen bond network that leads to high proton conductivity. Recently, defects like volatilization of phosphorus and destruction of the bonding structure have remarkably improved with introduction of cations, such as Zr4+ and Nb5+, into phosphate. In particular, niobium has proton conductivity on the surface because of higher surface acidity. It can also retain phosphorus content during heat treatment and improve chemical stability by bonding with phosphorus. In this study, we fabricate niobium phosphate glass thin films through sol-gel processing, and we report the chemical stability and electrical properties. The existence of the hydroxyl group in the phosphate is confirmed and found to be preserved at the intermediate temperature region of $150-450^{\circ}C$.

Protective effect of ginsenoside Rh3 against anticancer drug-induced apoptosis in LLC-PK1 kidney cells

  • Lee, Hye Lim;Kang, Ki Sung
    • Journal of Ginseng Research
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    • v.41 no.2
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    • pp.227-231
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    • 2017
  • Background: Ginsenosides are active components of Panax ginseng that exert various health benefits including kidney protection effect. The medicinal activity of ginsenosides can be enhanced by modulating their stereospecificity by heat processing. Ginsenosides Rk2 and Rh3 represent positional isomers of the double bond at C-20(21) or C-20(22). Methods: The present study investigated the kidney-protective effects of ginsenosides Rk2 and Rh3 against cisplatin, a platinum based anticancer drug, induced apoptotic damage in renal proximal LLC-PK1 cells. Results: As a result, ginsenoside Rh3 shows a stronger protective effect than that shown by Rk2. Cisplatin-induced elevated protein levels of phosphorylated c-Jun N-terminal kinase (JNK), extracellular signal-regulated kinase (ERK), p38, and cleaved caspase-3 decreased after cotreatment with ginsenoside Rh3. The increase in the percentage of apoptotic LLC-PK1 cells induced by cisplatin treatment also significantly reduced after cotreatment with ginsenoside Rh3. Conclusion: These results demonstrate that inhibition of the JNK and ERK mitogen-activated protein kinase signaling cascade plays a critical role in mediating the renoprotective effect of ginsenoside Rh3.

Effect of Microstructure on Dynamic Tensile Characteristics of SPRC440 Sheet (SPRC440 강판재의 미세조직 구성이 동적 인장 특성에 미치는 영향)

  • Lee, S.H.;Rhyim, Y.M.;Lee, J.H.;Kim, I.B.;Kim, Y.D.
    • Transactions of Materials Processing
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    • v.20 no.4
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    • pp.309-315
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    • 2011
  • The behavior of metallic materials at high strain rates shows different characteristics from those in quasi-static deformation. Therefore, the strain rate should be considered when simulating crash events. The objective of this paper is to evaluate the dynamic tensile characteristics of SPRC440 as a function of the volume fraction of phases. As-received SPRC440 is composed of ferrite and pearlite phases. However, ferrite and martensite phases were observed after heat treatment at $730^{\circ}C$ and $780^{\circ}C$ for 5 minutes, as expected by calculations based on the curves from dilatometry tests. High cross-head speed tensile tests were performed to acquire strain-stress curves at various strain rates ranging from 0.001 to $300\;s^{-1}$, which are typical in real vehicle crashes. It was observed that the flow stress increases with the strain rate and this trend was more pronounced in the as-received specimens consisting of ferrite and pearlite phases. It is speculated that the dislocation density in each phase has an influence on the strain rate sensitivity.

Synthesis of Nanopowders by Hydrothermal Method and their Application to Dye-sentisized Solar Cell Materials (수열합성을 이용한 나노분말 합성 및 연료감응태양전지 응용)

  • Lim, JinYoung;Ahn, Jeongseok;Ahn, Jung-Ho
    • Journal of Powder Materials
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    • v.25 no.4
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    • pp.309-315
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    • 2018
  • In the present work, we synthesize nano-sized ZnO, $SnO_2$, and $TiO_2$ powders by hydrothermal reaction using metal chlorides. We also examine the energy-storage characteristics of the resulting materials to evaluate the potential application of these powders to dye-sensitized solar cells. The control of processing parameters such as pressure, temperature, and the concentration of aqueous solution results in the formation of a variety of powder morphologies with different sizes. Nano-rod, nano-flower, and spherical powders are easily formed with the present method. Heat treatment after the hydrothermal reaction usually increases the size of the powder. At temperatures above $1000^{\circ}C$, a complete collapse of the shape occurs. With regard to the capacity of DSSC materials, the hydrothermally synthesized $TiO_2$ results in the highest current density of $9.1mA/cm^2$ among the examined oxides. This is attributed to the fine particle size and morphology with large specific surface area.