• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.27-36
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• 2004

Contemporary objectives for steel rod rolling processing are increasingly complex and often contrasting i.e. obtaining a desired product with optimum combination of properties such as strength, toughness and formability at lower cost. Low-alloy steel rods have been produced with several heat treatments for drawing and forging processes at room temperature. In order to reduce these heat treatments much of the researches concerning of high temperature mechanical behavior of steel rods have been conducted at wire rod mill of POSCO. In this present work, optimizations of rolling temperature and cooling rate for JS-SCM435 are performed to eliminate softening heat treatment(Low Temperature Annealing) for drawing process. The results from the optimization changed the microstructure of rods after rod rolling from Bainite with high tensile strength of 1000Mpa to Pearlite and Ferrite with appropriate strength of 750Mpa that is equivalent tensile strength after softening heat treatment.

• New & Renewable Energy
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• v.4 no.2
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• pp.81-86
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• 2008

Rotary kiln in cement work has been evaluated for a wide variety of organic wastes such as wood, used tyres, plastic wastes and automobile shredder residue (ASR). However the presence of chlorine hampers the use of ASR as fuel in rotary kiln. Therefore, the behavior characteristics of chlorine components in rotary kiln should be considered to develop an effective method for ASR treatment to recovery energy resources. The aim of this paper is to present the chlorine control system applied to a cement manufacturing process for ASR use as an alternative fuel. In this work, the simulation of bypass unit and cyclones for chlorine control in rotary kiln has been studied and compared with the operation results of field test.

• Journal of the Korea Institute of Military Science and Technology
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• v.24 no.1
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• pp.79-83
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• 2021

The expiration date of high energetic materials(HEM), such as HMX, RDX, TNT, is important. If the expiration date is violated, the expected specification of HEM would not be satisfied which may cause a different conclusion in an urgent situation. As a result, this HEM should maintain fresh conditions which cause the accumulation of waste HEM. If HEM is landfilled during demilitarization, the impact on living organizations is serious. Additionally, landfilling HEM has a possibility of explosion. In this research, the process flow diagram of the demilitarization gas treatment process was simulated while satisfying the law of the environment in Korea. After validation of simulation, it was optimized thermodynamically using Heat Exchanger Network Synthesis(HENs). This study is expected to enhance the energy efficiency of the original facility by suggesting developed designs. This research was supported by Agency of Defense Development NE32 Korea. Thanks to Agency of Defense Development, Korea

• Korean Journal of Materials Research
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• v.34 no.10
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• pp.475-481
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• 2024

Lithium-ion batteries are widely used in various advanced devices, including electric vehicles and energy storage devices. As the application range of lithium-ion batteries expands, it will be increasingly important to improve their gravimetric and volumetric energy density. Layer-structured oxide materials have been widely adopted as cathode materials in Li-ion batteries. Among them, LiNiO₂ has attracted interest because of its high theoretical capacity, ~274 mAh g^-1, assuming reversible one Li⁺-(de)intercalation from the structure. Presently, such layered structure cathode materials are prepared by calcination of precursors. The precursors are typically hydroxides synthesized by coprecipitation reaction. Precursors synthesized by coprecipitation reaction have a spherical morphology with a size larger than 10 ㎛. Spherical precursors in the several micrometer range are difficult to obtain due to the limited coprecipitation reaction time, and can lead to vigorous collisions between the precursor particles. In this study, spherical and small-sized Ni(OH)₂ precursors were synthesized using a new synthesis method instead of the conventional precipitation method. The highest capacity, 170 mAh g^-1, could be achieved in the temperature range of 730~760 ℃. The improved capacity was confirmed to be due to the higher quality of the layered structure.

• Transactions of Materials Processing
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• v.15 no.8 s.89
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• pp.568-573
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• 2006

In order to numerically evaluate automotive hydro-formed DP-steel tubes on crash performance considering welding heat effects, the finite element simulations of crash behavior were performed for hydro-formed tubes with and without heat treatment effects. This work involves the mechanical characterization of the base material and the HAG-welded zone as well as finite element simulations of the crash test of hydro-formed tubes with welded brackets and hydro-forming of tubes. The welding heat effects on the crash performance are evaluated in efforts to improve the process optimization procedure of the engine cradle in the design stage. In particular, FEM simulations on indentations have been performed and experimentally verified for material properties of weld zone and heat affected zone.

• Journal of Surface Science and Engineering
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• v.57 no.3
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• pp.179-191
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• 2024

This study focuses on improving the photocatalytic degradation efficiency by synthesizing a TiO₂/WO₃ composite. Given the environmental significance of photocatalysis and the limitations posed by TiO₂'s large bandgap and high electron recombination rate, we explored doping, surface modification, and synthesis strategies. The composite was created using a ball mill process and heat treatment, analyzed with field emission scanning electron microscope, high resolution X-ray diffraction, Raman microscope, and UV-Vis/NIR spectrometer to examine its morphology, composition and absorbance. We found that incorporating WO₃ into the TiO₂ lattice forms a W_x-Ti_1-x-O₂ solution, with optimal WO₃ content reducing the band gap and enhancing sterilization efficiency by inhibiting the anatasese to rutile transition. This contributes to the field by offering a way to overcome TiO₂'s limitations and improve photocatalytic performance.

• Korean Journal of Organic Agriculture
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• v.20 no.3
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• pp.399-409
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• 2012

Effects of pretreatment and extraction conditions on total polyphenol yield from licorice root were investigated using statistical method. For pretreatment, heat treatment at $121^{\circ}C$ for 10 min was applied. Licorice root content in solvent (10, 20, and 30%) ethanol concentration (20, 40, and 60%) and reaction time (1, 2, and 3 h) were used as variables for extraction conditions. Two experiments, with heat treated and no treated licorice, were prepared with same experimental design. Box behnken design was employed and produced a total of 15 trials. Total polyphenol yield from licorice root was not affected by heat treatment. Among variables, licorice content in solvent showed most significant effect regardless of other variables (p<0.05). Finally, optimum conditions for the extraction of total polyphenol from licorice root was detected as following: 10% of licorice in solvent, 52% ethanol as solvent, 2 h of reaction time and non-heat treatment and the extraction yield from optimized condition was 17.6 mg/g licorice root.

• Journal of the Korean Society for Heat Treatment
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• v.19 no.3
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• pp.149-155
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• 2006

The effects of eight types of spheroidizing annealing conditions including annealing temperature, annealing time, cooling rate, and gas atmosphere in the annealing furnace on the microstructure were determined in SM45C steel which has been widely used for automotive parts. The well-developed spheroidized structure and minimum hardness were obtained when the steel was heat-treated 6 hours at $740^{\circ}C$, cooled to $710^{\circ}C$ at a cooling rate of $24^{\circ}C/h$, and then kept for 7 hours at the $710^{\circ}C$ followed by air cooling. In order to increase the productivity and to save the manufacturing cost, it is desirable to apply a faster cooling rate in the spheroidizing annealing. It was found that air cooling was the fastest cooling rate applicable to the SM45C steel. The steel heat treated in air showed the decarburized layer of about $110{\mu}m$ in thickness at the surface of the specimen, resulting in serious problems in the quality of the quenched product.

• Journal of the Korean Society for Heat Treatment
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• v.19 no.5
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• pp.270-279
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• 2006

The effects of eight types of spheroidizing annealing conditions including annealing temperature, annealing time, cooling rate, and furnace atmosphere on the microstructure and hardeness were determined in SCM440 steel which has been widely used for automotive parts. The well-spheroidized structure and minimum hardness were obtained when the steel was heat-treated at $770^{\circ}C$ for 6 hours, cooled to $720^{\circ}C$ at a cooling rate of $24^{\circ}C/h$, and then kept for 7 hours at the $720^{\circ}C$ followed by air cooling. In order to increase the productivity and to save the manufacturing cost, it is desirable to apply a faster cooling rate to the spheroidizing annealing. It was found that a cooling rate of $100^{\circ}C/hr$ was the fastest cooling rate applicable to the SCM440 steel among the four cooling rates used in this study. The microstructure consisted of ferrite and very fine spheroidized cementite when the steel was annealed for 13 hours at $720^{\circ}C$ below $A_{C1}$ temperature. This was caused by the short annealing time and the retarding effect of Cr and Mo on both the dissolution of pearlite to cementite and coarsening of spheroidized cementite. The steel heat treated in air showed the decarburized layer of about $125{\mu}m$ in thickness at the surface.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.30 no.3
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• pp.30-38
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• 2016

In this research, a 6W white LED package with a Glass Remote Phosphor was developed to improve the life of an LED package. The Glass Remote Phosphor was fabricated by the Phosphor in Glass (PiG) method, wherein phosphor YAG:Ce was mixed with glass frit and then heat treated. A paste with 75wt.% of a phosphor substance and 25wt.% glass frit was coated on a glass substrate two times using the screen-printing technique and heat-treated at $800^{\circ}C$ ; this structure gave a luminous efficacy of 136.1lm/W, color rendering index of 74Ra, and color temperature of 5,342K, thus satisfying the requirements as a light source for lighting. Moreover, an IES LM-80 accelerated life test was conducted on the same LED package for 6,000h in order to estimate the L70 lifetime based on IES TM-21. The results showed guaranteed lifetimes of 213,000h at $55^{\circ}C$, 245,000h at $85^{\circ}C$, and 209,000h at $95^{\circ}C$.