• Title/Summary/Keyword: heat treatment condition

Search Result 971, Processing Time 0.031 seconds

Phosphate Removal from Aqueous Solution according to Activation Methods of Red Mud (알루미늄 제련 폐기물(Red Mud)의 활성화 방법에 따른 수용상의 인산염 제거특성)

  • Kim, I-Tae;Bae, Woo-keun;Kim, Woo-jeong
    • Journal of Korean Society on Water Environment
    • /
    • v.20 no.5
    • /
    • pp.466-472
    • /
    • 2004
  • Red mud is formed as a waste during bauxite refining known as Bayer's process. Its main constituents are iron, aluminium, sodium and silica. The disposal of large quantities of wasted red mud causes a serious ecological problem. In this study, the red mud wasted from the bauxite refinery was studied for phosphate removal from aqueous solution according to activation methods. The influence of heat treatment, and neutralization with sea water and acid treatment level for the optimum conditions for phosphate removal have been determined. Heat treatment combined with acid treatment is most suitable for the removal of phosphate from aqueous solution. The optimal condition was activated with 1 N HCl solution after heating in $600^{\circ}C$ during 4 hours. Acid and heat treatment causes sodalite compounds which hinder the phosphate adsorption to leach out. The adsorption data obtained followed a first-order rate expression and fitted well with the Freundlich Isotherm well.

Changes of Paeoniflorin Content in Peony Roots by Heat-treatment (열처리에 의한 작약의 Paeoniflorin 함량 변화)

  • 김태강;김광중
    • Food Science and Preservation
    • /
    • v.4 no.1
    • /
    • pp.69-75
    • /
    • 1997
  • Peony is a medicinal herb which have utilized widely as chineses medicine. The paeoniflorin is the predominant component In peony root, monoterpene glucoside containing pinane structure. The effective components were extracted with the cold water from the intact peony roots, and effectively extracted with 70% ethanol from the dry powder of peony roots. The changes of paeoniflorin contents were investigated during the drying process of peony roots and processing of peony extract by the heat-treatment. Air-drying was the best condition for the preservation of paeoniflorin content among the drying processes of peony roots. But convective drying at 6$0^{\circ}C$ was recommended for the drying process of peony roots in large scale. The paeoniflorin in peony extracts was not destroyed by the treatment at 6$0^{\circ}C$ and 8$0^{\circ}C$ for 5 hrs, but destroyed 30%, 28% and 40% of paeoniflorin by treatment at 10$0^{\circ}C$ for 5 hrs, 115$^{\circ}C$ and 121$^{\circ}C$ for 10 minutes, respectively. The paeoniflorin was continueously extracted for 4 hrs from the dry pieces of peony roots(0.5$\times$0.5$\times$0.5cm) in boiling water but destroyed gradually after 4 hrs at 10$0^{\circ}C$. Paeoniflorins in 70% ethanol extracts of peony root were not destroyed at all in the process of concentration to dry powder at 60"C on vacuum.cuum.

  • PDF

A Case Study of Polyarthritis Treated with Dokhwaljihwang-tang (독활지황탕으로 호전된 다발성 관절염 환자 치험 1례)

  • Lee, Jae-Wook;Choi, Hyun-Min;Lim, Eun-Chul
    • Journal of Sasang Constitutional Medicine
    • /
    • v.29 no.4
    • /
    • pp.369-375
    • /
    • 2017
  • Objectives The purpose of this study is to report a case of improving various symptoms such as polyarthritis, dyspnea, fatigue, heat sensation. In addition, the promising explanation on the perspective of the heat and cold syndrome could be elicited. Methods Dokhwaljihwang-tang was prescribed for an outpatient for 3 weeks without any other therapy such as acupuncture, moxibustion and Western medicine. To evaluate the results of this treatment, polyarthritis was assessed by Visual Analogue Scale(VAS). The patient's general condition such as digestion and defecation discomfort is assessed by the progress notes. Results&Conclusions Most of the various symptoms have improved by about 80 percent. It is more important to observe defecation, urine, cold symptoms and condition of hands and feet synthetically.

Development of Forged Aluminum Lower Arm (알루미늄 단조 Lower Arm 개발)

  • 조용기;윤병은
    • Proceedings of the Korean Society for Technology of Plasticity Conference
    • /
    • 1995.06a
    • /
    • pp.74-80
    • /
    • 1995
  • Forged aluminum lower arm has been developed to provide weight reduction of suspension parts. It was utilized FEM analysis in design of parts. Prototype parts were producted to two shape & different forging condition. Difference of forging condition was manufacturing process of stock, forging press, forging die, heat treatment condition. As a result, weight reduction of 44%, 38% was achived. Strength and fatigue endurance of forged aluminum lower arm was excellent.

Fracture Properties of Mo-Ni-Cu Austempered Ductile Iron Cast in Permanent Mold with Austempering Temperature and Time (금형주조한 Mo-Ni-Cu계 구상흑연주철의 오스템퍼링 온도 및 시간에 따른 파괴특성)

  • Yi, Young-Sang;Kang, In-Chan
    • Journal of Korea Foundry Society
    • /
    • v.11 no.4
    • /
    • pp.331-337
    • /
    • 1991
  • Various test specimens were prepared by austempering low alloyed Mo-Ni-Cu ductile iron blocks of high graphite nodule count at 270, 320 or $370^{\circ}C$ for 0.5, 1, 3 or 9hrs. Tensile test, CVN impact test and plane-strain fracture toughness test(compact tension specimen of 50mm W) were done for each heat treatment condition at room temperature. X-ray diffractometer and optical microscope were used to investigate the change of microstructure and relationships between microstructure and test results. The highest retained austenite volume percent at each austempering temperature was corresponded to the highest mechanical property. The highest elongation value of 17%, U.T.S. value of 1,600 MPa or $K_{IC}$ value of 90MPa${\surd}$m were reached at each optimum condition. The best heat treatment condition for fracture toughness were 3hrs' holding time combined with the austempering temperature of 270 and $320^{\circ}C$, and 1hr's of $370^{\circ}C$.

  • PDF

Thermal Analysis of Nickel-Base Superalloys by Differential Scanning Calorimetry (시차주사열량측정법에 의한 니켈기 초내열 합금의 열분석)

  • Yun, Jihyeon;Oh, Junhyeob;Kim, Hongkyu;Yun, Jondo
    • Korean Journal of Materials Research
    • /
    • v.26 no.5
    • /
    • pp.235-240
    • /
    • 2016
  • Appropriate thermo-mechanical properties of nickel-based superalloys are achieved by heat treatment, which induces precipitation and solid solution hardening; thus, information on the temperature ranges of precipitation and dissolution of the precipitates is essential for the determination of the heat treatment condition. In this study, thermal analyses of nickel-based superalloys were performed by differential scanning calorimetry method under conditions of various heating rates of 5, 10, 20, or 40K/min in a temperature range of 298~1573K. Precipitation and dissolution temperatures were determined by measuring peak temperatures, constructing trend lines, and extrapolating those lines to the zero heating rate to find the exact temperature under isothermal condition. Determined temperatures for the precipitation reactions were 813, 952, and 1062K. Determined onset, peak, and offset temperatures of the first dissolution reaction were 1302, 1388, and 1406K, respectively, and those values of the second dissolution reaction were 1405, 1414, and 1462K. Determined solvus temperature was 1462K. The study showed that it was possible to use a simple method to obtain accurate phase transition temperatures under isothermal condition.

Cutting Chip Forms on the Cutting Condition and Tempering Temperatures of Lead-free Brass (무연황동의 절삭 칩 형태에 미치는 절삭조건과 템퍼링 온도의 영향)

  • Joo, Y.S.;Lee, S.B.;Kim, S.Y.;Joo, C.S.;Jung, B.H
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.25 no.1
    • /
    • pp.14-21
    • /
    • 2012
  • The effects of cutting condition and tempering temperature for the shape of cutting chip were investigated. For this purpose, a lead-free brass containing 1wt.% of Bi extruded at $750^{\circ}C$ in straight turning was used in this study. The cutting chip preferred was mainly found to be loose form of arc chips with curling discontinuity, and these were formed by shear fracture. However, some of fragmental element chip were found to be mixed when tempering temperature was as high as $500^{\circ}C$. The form and size of chip was more affected by feed rate than by tempering temperature and cutting rate. In addition, the cutting surface was observed to be formed more rough in the case of high feed rate and low cutting rate compared to low feed rate and high cutting rate.

A Study on the Process for Improving Mechanical Property of Sand Casting by Using the Binder Jetting Method (사형 주조에서 바인더 젯 3D 프린터를 이용한 기계적 물성 향상을 위한 공정 연구)

  • Jung-Chul Hwang;Tae-Sung Kim
    • Journal of the Korea Safety Management & Science
    • /
    • v.25 no.1
    • /
    • pp.23-29
    • /
    • 2023
  • Among the Additive Manufacturing (AM) technologies, the Binder-Jetting printing technology is a method of spraying an adhesive on the surface of powder and laminate layer by layer. Recently, this technique has become a major issue in the production of large casting products such as ship-building, custom vehicles and so on. In this study, we performed research to make actual mold castings and increase mechanical property by using special sand and water-based binders. For use as a mold, it has a strength of more than 3MPa and permeability. Various experiments were carried out to obtain suitable them. The major process parameters were binder jetting volume, binder types, layer thickness and heat treatment condition. As a result of this study, the binder drop quantity was measured to be about 60 pico-liter, layer thickness was 100㎛ and the heat treatment condition was measured about 1,000℃ and compressive strength were measured to be more than 5MPa. The optimum condition of this experiment was established through actual casting of aluminum. The equipment used in this study was a Freeforms T400 model (SFS Co., Ltd.), and the printing area of 420 * 300 * 250mm and resolution of 600dpi can be realized.

Transformation Behavior on Heat Treatment Condition in Grain-Refined Cu-Zn-Al Shape Memory Alloy (결정립 미세화된 Cu-Zn-Al 형상기억합금의 열처리 조건에 따른 변태거동)

  • Kang, J.W.;Jang, W.Y.;Yang, G.S.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.4 no.4
    • /
    • pp.34-43
    • /
    • 1991
  • A small amount of misch metal and/or Zr was added as a dopant to 70.5wt----Cu-26wt----Zn-3.5wt----Al shape memory alloy in order to study the effect of grain refinement and heat treatments on the transformation behavior, stabilization of martensite, and shape memory ability. It was found that the addition of misch metal and Zr was very effective for reducing the grain size. The fracture mode has been changed from intergranular brittle fracture to ductile fracture with void formation and coalescence by the addition of misch metal and Zr. Aging of the ${\beta}$-phase decreases the $M_s$ temperature, but that of the martensite phase increases the $A_s$ temperature. The hysteresis of transformation temperature ${\Delta}T(A_s-M_s)$ has an increasing tendancy by grain refinement. The crystal structure of martensite was identified as monoclinic structure. As the grain size decreased, martensite stabilization more easily occured and the shape, memory ability has been reduced by the grain size refined.

  • PDF

A Study on the Improvement of Machinability in Hot-Forged Aluminum Alloy Product(Al 7075) (알루미늄 합금(Al 7075) 절삭성 향상을 위한 열간단조 후처리 방법에 관한 연구)

  • 김진복;임학진;강범수
    • Journal of the Korean Society of Propulsion Engineers
    • /
    • v.4 no.2
    • /
    • pp.46-53
    • /
    • 2000
  • Hot forging of aluminum alloy has the bad machinability due to continuous chip formation caused from the ductility The bad machinability requires a labor and a high cost to produce final products after hot forging. In industrial field, T4 heat treatment is performed to improve the machinability, and the annealing and the cold sizing are followed. In this study, a series of heat treatments are introduced during hot forging operation without T4 heat treatment after forming so that it improves the machinability with reduction of the number of operations and machining cost. Instead of T4 heat treatment, water cooling and air cooling are tried and compared to find out an optimum cooling condition

  • PDF