• Title/Summary/Keyword: growth behavior

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Growth Mechanism Evolution of ZnO Nanostructures by Leidenfrost Effect in Ultrasonic Spray Pyrolysis Deposition (초음파 분무 열분해법에 의한 ZnO 나노구조 성장시 Leidenfrost 효과에 의한 성장 거동 변화)

  • Han, In Sub;Park, Il-Kyu
    • Korean Journal of Materials Research
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    • v.27 no.11
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    • pp.609-616
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    • 2017
  • We investigated a Leidenfrost effect in the growth of ZnO nanostructures on silicon substrates by ultrasonic-assisted spray pyrolysis deposition(SPD). Structural and optical properties of the ZnO nanostructures grown by varying the growth parameters, such as substrate temperature, source concentration, and suction rate of the mist in the chambers, were investigated using field-emission scanning electron microscopy, X-ray diffraction, and photoluminescence spectrum analysis. Structural investigations of the ZnO nanostructures showed abnormal evolution of the morphologies with variation of the substrate temperatures. The shape of the ZnO nanostructures transformed from nanoplate, nanorod, nanopencil, and nanoprism shapes with increasing of the substrate temperature from 250 to $450^{\circ}C$; these shapes were significantly different from those seen for the conventional growth mechanisms in SPD. The observed growth behavior showed that a Leidenfrost effect dominantly affected the growth mechanism of the ZnO nanostructures.

Energetics of adsorptions on fcc(111) and binary system; An application of the modified embedded atom method

  • Hy. Shin;J. Seo;Kim, J.S.
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.188-188
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    • 1999
  • The embedded atom method (EAM) of Daw and Baskes as a semiempirical method, has been successfully applied to the fcc or nearly filled d-band transition metals due to its computational feasibility and its methodological simplicity. Then Baskes modified the EAM (MEAM) to include directional bonding and applied it to metals, semiconductors, and diatomic gases, all of which have different types of bondings. Here, we present a detailed study of the energetics of adsorption on the fcc(111) surfaces and binary system within the framework of MEAM. In adsorption on fcc(111) surfaces, there are two energetically favored sites, so called, fcc site and hcp site, which may trigger stacking fault in the growth of films and might switch growth mode between 3D growth and layer by layer growth. We scrutinized the role of the hcp sites, which would offer dynamic growth pathways although the dynamics are not yet clear within the limited experimental resolution. Featuring these transient motions in the atomic level should contribute to the understanding the growth mechanisms on fcc(111) surface. And we also applied MEAM for initial stage energetics at the Cr coverage of sub- monolayer on W(110). We hope that recently observed extraordinary growth behavior at the Cr coverage of 0.7 monolayer, self- organized nano-scale lines, can be resolved in this MEAM binary system calculation.

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A study on the growth behaviors of surface fatigue crack initiated from a small-surface defect of 2024-T3 and brass (2024-T3 및 황동의 작은 표면결함재의 피로균열 성장특성에 관한 연구)

  • 서창민;오명석
    • Journal of Ocean Engineering and Technology
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    • v.10 no.1
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    • pp.53-64
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    • 1996
  • In this paper, rotating bending fatigue tests have been carried out to investigate the growth behabiors of surface fatigue crack initiated from a small artificial surface defect, that might exist in real structures, on 2024-T3 and 6:4 brass. The test results are analysed in the viewpoints of both strength of materials and fracture mechanics, it can be concluded as follows. The effect of a small artificial surface defect upon the fatigue strength is very large. The sensitivity of 2024-T3 on the defect is higher than that of 6:4 brass. The growth behavior of the surface fatigue crack of 2024-T3 is different from that of 6:4 brass. The growth rate of the surface fatigue crack of 2024-T3 is considerably rapid in the early stage of the fatigue life and apt to decrease in the later stage. It was impossible to establish a unifying approach in the analysis of crack growth begabior of 2024-T3 and 6:4 brass using the maximum stress intensity factor because of their dependence on stress level. But if the elastic strain and cyclic total strain intensity factor range were applied to obtain the growth rate of surface fatigue cracks of the materials, the data were found to be nearly coincided.

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Marco and Microscopic Observations of Fatigue Crack Growth in Friction Stir Welded 7075-T651 Aluminum Alloy Plates (마찰교반용접된 7075-T651 알루미늄 판재의 피로균열전파의 거시적 및 미시적 관찰)

  • Kong, Yu-Sik;Kim, Seon-Jin
    • Journal of Power System Engineering
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    • v.18 no.2
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    • pp.62-69
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    • 2014
  • In this paper, in order to investigate the effects of marco and microscopic observations of fatigue crack growth in friction stir welded (FSWed) 7075-T651 aluminum alloy plates, fatigue crack growth tests were performed under constant amplitude loading condition at room temperature with three different pre-cack locations, namely base metal (BM-CL) and two kinds of pre-crack locations in welded joints, weld metal (WM-CL) and heat affected zone (HAZ-CL) specimens. The fatigue crack growth behavior of FSWed 7075-T651 aluminum alloy plates were discussed based on the marco and microscopic fractographic observations. The marcoscopic aspects of surface crack growth path for BM-CL and HAZ-CL specimens indicate relatively straight lines, however, the crack growth paths of WM-CL specimens grow first straight and by followed toward the TMAZ and HAZ. The microscopic aspects of fatigue fracture for BM-CL and HAZ-CL specimens indicate typical fatigue striation, but WM-CL showed intergranular fracture pattern by micro structural changes of FSW process.

Fabrication of a high magnetization YBCO bulk superconductor by a bottom-seeded melt growth method

  • Hong, Yi-Seul;Park, Soon-dong;Kim, Chan-Joong;Lee, Hee-Gyoun
    • Progress in Superconductivity and Cryogenics
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    • v.21 no.4
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    • pp.19-23
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    • 2019
  • A large grain YBCO bulk superconductor is fabricated by the top-seeded melt growth (TSMG) method. In the TSMG process, the seed crystal is placed on the top surface of a partially melted compact and therefore the seed crystal is frequently tilted during the melt process due to intrinsic unstable nature of Y211 particle +liquid phase mixture. In this work, we report the successful growth of single-domain YBCO bulk superconductors by a bottom-seeded melt growth (BSMG) method. Investigations on the trapped magnetic field and the microstructures of the synthesized specimens show that a bottom-seeded melt growth method has hardly affected on the crystal growth behavior, the microstructure development and the magnetic properties of the large grain YBCO bulk superconductors. The bottom-seeded melt growth method is clearly beneficial for the stable control of seed orientation through the melt process for the fabrication of a large grain YBCO bulk superconductor.

Fatigue Crack Growth Characteristics of $SiC_p/Al-Si$ Alloy Composites for Automotive Structures (자동차구조용 $SiC_p/Al-Si$복합재의 피로균열 진전특성에 대한 연구)

  • Koh Seungkee;Lee Haemoo
    • Transactions of the Korean Society of Automotive Engineers
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    • v.13 no.4
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    • pp.174-181
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    • 2005
  • In order to investigate the behavior of fatigue crack growth of SiC-particulate- reinforced Al-Si alloy composites, fatigue tests using single edge notched tension(SENT) specimens were performed. Composite materials were manufactured by using both permanent die casting and extrusion processes with different volume fractions of $10\%\;and\;20\%$. $SiC_p-reinfurced$ Al-Si composites showed the increased levels of threshold stress intensity factor range, ${\Delta}K_{th}$, for the increased volume fractions of SiC particles, which implies the increased fatigue crack growth resistance at the threshold or low ${\Delta}K$ levels, compared to the unreinforced Al-Si alloy. In the Paris region, however, the composites showed the increased rate of crack growth resulting in the unfavorable effects on the fatigue crack growth resistance. Critical stress intensity factor range at unstable crack growth leading to final fracture decreased as the volume fraction of SiC particle increased, because of the reduced fracture toughness of the composites. Extruded materials showed higher threshold and critical values than the cast materials.

Study on the Single Bubble Growth During Nucleate Boiling at Saturated Pool (포화상태 풀비등시 단일기포의 성장에 관한 연구)

  • Kim Jeongbae;Lee Han Choon;Oh Byung Do;Kim Moo Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.29 no.2 s.233
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    • pp.169-179
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    • 2005
  • Nucleate boiling experiments on heating surface of constant wall temperature were performed using R113 for almost saturated pool boiling conditions. A microscale heater array and Wheatstone bridge circuits were used to maintain a constant wall temperature condition of heating surface and to measure the heat flow rate with high temporal and spatial resolutions. Bubble images during the bubble growth were taken as 5000 frames per second using a high-speed CCD camera synchronized with the heat flow rate measurements. The bubble growth behavior was analyzed using the new dimensionless parameters for each growth regions to permit comparisons with previous experimental results at the same scale. We found that the new dimensionless parameters can describe the whole growth region as initial and later (thermal) respectively. The comparisons showed good agreement in the initial and thermal growth regions. In the initial growth region including surface tension controlled, transition and inertia controlled regions as divided by Robinson and Judd, the bubble growth rate showed that the bubble radius was proportional to $t^{2/3}$ regardless of working fluids and heating conditions. And in the thermal growth region as also called asymptotic region, the bubble showed a growth rate that was proportional to $t^{1/5}$, also. Those growth rates were slower than the growth rates proposed in previous analytical analyses. The required heat flow rate for the volume change of the observed bubble was estimated to be larger than the heat flow rate measured at the wall. Heat, which is different from the instantaneous heat supplied through the heating wall, can be estimated as being transferred through the interface between bubble and liquid even with saturated pool condition. This phenomenon under a saturated pool condition needs to be analyzed and the data from this study can supply the good experimental data with the precise boundary condition (constant wall temperature).

A Coverage Function for Arbitrary Testing Profile and Its Performance

  • Park Joong-Yang;Fujiwara Takaji;Park Jae-Heung
    • International Journal of Reliability and Applications
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    • v.6 no.2
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    • pp.87-99
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    • 2005
  • Coverage-based software reliability growth models (SRGMs) have been developed and successfully applied in practice. Performance of a coverage-based SRG M depends on the coverage function employed by the SRGM. When the coverage function represents the coverage growth behavior well irrespective of type of the testing profile the corresponding coverage-based SRGM is expected to be widely applicable. This paper first conducts a study of selecting the most representative coverage functions among the available coverage functions. Then their performances are empirically evaluated and compared. The result provides a foundation for developing widely applicable coverage-based SRGMs and monitoring the progress of a testing process.

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A Study of Crack Growth Behavior of Al2024 (Al2024의 균열성장거동에 관한 연구)

  • Lee, Won-Seok;Lee, Hyun-Woo
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.10
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    • pp.49-55
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    • 2000
  • This study describes the fatigue characteristics for Al2024 alloy, which is aircraft structure material. For this work, the plane-strain fracture toughness test, the plane-stress fracture toughness test and the crack growth rates test were conducted under the standard testing method. Test equipment is a computer-controlled closed-loop fatigue testing machine. The data of each test result is very important to aircraft structure reliability estimation, life prediction, design analysis, endurance analysis and damage tolerance analysis. In addition, the fatigue crack growth threshold($\DeltaKth$) value decreased as the stress ratio increased. Also, $\DeltaKth$ decreased as the thickness increased in LT, TL directions.

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INVESTIGATION OF ENERGETIC DEPOSITION OF Au/Au (001) THIN FILMS BY COMPUTER SIMULATION

  • Zhang, Q. Y.;Pan, Z. Y.;Zhao, G. O.
    • Journal of the Korean Vacuum Society
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    • v.7 no.s1
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    • pp.183-189
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    • 1998
  • A new computer simulation method for film growth, the kinetic Monte Carlo simulation in combination with the results obtained from molecular dynamics simulation for the transient process induced by deposited atoms, was developed. The behavior of energetic atom in Au/Au(100) thin film deposition was investigated by the method. The atomistic mechanism of energetic atom deposition that led to the smoothness enhancement and the relationship between the role of transient process and film growth mechanism were discussed. We found that energetic atoms cannot affect the film growth mode in layer-by-layer at high temperature. However, at temperature of film growth in 3-dimensional mode and in quasi-two-dimensional mode, energetic atoms can enhance the smoothness of film surface. The enhancement of smoothness is caused by the transient mobility of energetic atoms and the suppression for the formation of 3-dimensional islands.

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