• Title/Summary/Keyword: growth behavior

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The influence of atomosphere on high temperature crystal growth

  • Klimm, D.;Schroder, W.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.4
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    • pp.360-364
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    • 1999
  • The growth of crystals with high melting point$t_{fus}$$\geq$$1600^{\circ}C$ faces the researcher with experimental problems, as the choice of materials that withstand such high t is rather limited. Many metallic construction materials are in this high t range already molten or exhibit at least a drastically reduced mechanical strength. The very few materials with$t_{fus}$$1600^{\circ}C$ as e.g. W, Mo, and partially even Ir are more or less sensitive against oxygen upon heating. Whenever possible, high t crystal growth is performed under inert atmosphere (noble gases). Unfortunately, many oxides are not thermodynamically stable under such conditions, as reduction takes place within such atmosphere. A thoroughly search for suitable growth conditions has to be performed, that are on the one side "oxidative enough" to keep the oxides stable and on the other side "reductive enough" to avoid destruction of constructive parts of the crystal growth assembly. The relevant parameters are t and the oxygen partial pressure${po}_{2}$. The paper discusses quantitatively relevant properties of interesting oxides and construction materials and wasy to forecast theri behavior under growth conditions.

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Charged Cluster Model as a New Paradigm of Crystal Growth

  • Nong-M. Hwang;In-D. Jeon;Kim, Doh-Y.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 2000.06a
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    • pp.87-125
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    • 2000
  • A new paradigm of crystal growth was suggested in a charged cluster model, where charged clusters of nanometer size are suspended in the gas phase in most thin film processes and are a major flux for thin film growth. The existence of these hypothetical clusters was experimentally confirmed in the diamond and silicon CVD processes as well as in gold and tungsten evaporation. These results imply new insights as to the low pressure diamond synthesis without hydrogen, epitaxial growth, selective deposition and fabrication of quantum dots, nanometer-sized powders and nanowires or nanotubes. Based on this concept, we produced such quantum dot structures of carbon, silicon, gold and tungsten. Charged clusters land preferably on conducting substrates over on insulating substrates, resulting in selective deposition. if the behavior of selective deposition is properly controlled, charged clusters can make highly anisotropic growth, leading to nanowires or nanotubes.

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Stress Corrosion Cracking Behavior under Cavitation Erosion-Corrosion in Sea Water-Part (II) (해수환경중 캐비테이션 침식-부식 하에서의 응력부식균열 거동 (II))

  • 안석환;임우조
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.36 no.2
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    • pp.139-146
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    • 2000
  • Cavitation can occur in pipes when liquid is moving at high velocity, especially at pittings where the smooth bore of the pipe is interrupted. The effect is usually to produce pitting on the downstream side of the turbulence. However, stress corrosion cracking behavior under cavitation erosion-corrosion was neatly unknown. In this study, therefore, some were investigated of stress corrosion cracking behavior, others were stress corrosion cracking behavior under cavitation erosion-corrosion of water injection. And datas obtained as the results of experiment were compared between the two. Mainresult obtained are as follows: 1) Stress corrosion cracking growth rate of heat affected zone under cavitation erosion-corrosion becomes most rapid, and stress intensity factor $K_1$becomes most high. 2) Stress corrosion cracking growth mechanism by cavitation erosion-corrosion is judgement on the strength of the film rupture model and the tunnel model. 3) The range of potential as passivation of heat affected zone is less noble than that of base metal, and that value is smaller. 4) Corrosion potential under cavitation erosion-corrosion in loaded stress is less noble than that of stress corrosion, and corrosion current density is higher.

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Acoustic emission behavior during fatigue crack propagation in 304 Stainless steel (피로균열진전에 따른 304 강의 음향방출 거동)

  • Oh, Kwang-Hwan;Jung, Chang-Kyu;Yang, Yoo-Chang;Han, Kyung-Seop
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.213-219
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    • 2003
  • Acoustic emission behavior during fatigue crack growth test was investigated under various loading condition. To describe the acoustic emission activity, counts rate (d/dn) was related with SIFR (stress intensity factor range, K). Results indicated that SIFR could be divided into two parts according to its relationship with counts rate. For $K<25_{MPa\sqrt{m}}$, counts rate was increased as the SIFR increased. However, for values greater than $25_{MPa\sqrt{m}}$ , decreasing behavior was shown. This behavior of counts rate corresponding SIFR was keeping the same trend regardless of load range or crack length. Acoustic emission response to the single overload was sudden drop and slow recovery in counts rate like crack growth retardation. Under variable loading condition, counts rate of each loading block was same as that of constant amplitude loading. Overall experimental data was somewhat scattered since sensitive characteristics of acoustic emission method. However, these empirical relations indicated that counts rate was uniquely correlate with single parameter, SIFR.

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A Study on the Recrystallization Behavior of Zr-0.8Sn-xFe Ternary Alloys (Zr-0.8Sn-xFe 3원계 합금의 재결정 거동에 관한 연구)

  • Lim, Yoon-Soo;Choi, Yang-Jin;Wey, Myeong-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.4
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    • pp.239-245
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    • 2000
  • Effect of tin and iron content on the recrystallization behavior of temary Zr-0.8Sn-x%Nb alloys were studied. The specimens with 0.1, 0.2 and 0.4 wt.% of iron were prepared under various annealing temperatures from $400^{\circ}C$ to $800^{\circ}C$ and times from 30 to 5000 minutes after vacuum arc remelting. The recrystallization behavior was observed using a polarized optical microscope, TEM and micro-vickers hardness tester. The recrystallization temperature of the alloys slightly increased with iron content due to increase of activation energy. The grain growth of the alloys with 0.1 and 0.2 wt.% of iron occured rapidly, however, that of the alloys with 0.4 wt.% iron was gradually retarded due to precipitation. The hardness of the alloy with a high iron slightly increased by the precipitation of beta phase after annealing at $800^{\circ}C$.

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Estimation of Empirical Fatigue Crack Propagation Model of AZ31 Magnesium Alloys under Different Maximum Loads (최대하중 조건에 따른 AZ31 마그네슘합금의 실험적 피로균열전파모델 평가)

  • Choi, Seon-Soon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.2
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    • pp.522-528
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    • 2012
  • It is the aim of this paper to propose the empirical fatigue crack propagation model fit to describe a crack growth behavior of AZ31 magnesium alloys. The statistical data of a crack growth for an estimation are obtained by fatigue crack propagation tests under the three cases of maximum load. The empirical models estimated are Paris-Erdogan model, Walker model, Forman model, and modified-Forman model. It is found that the empirical model fit to describe a crack growth behavior of AZ31 magnesium alloys is Paris-Erdogan model and Walker model. It is also verified that a fatigue crack growth rate exponent of a empirical model is to be a material constant.

Relationship between Pattern of Fatigue Crack Surface and Fatigue Crack Growth Behavior under $K_{III}$ Mode-Four Point Shear in Al 5083-O

  • Kim Gun-Ho;Won Young-Jun;Sakakur Keigo;Fujimot Takehiro;Nishioka Toshihisa
    • Journal of Advanced Marine Engineering and Technology
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    • v.30 no.4
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    • pp.474-482
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    • 2006
  • Generally almost all fatigue crack growth is affected by mode I. For this reason a study on mode I has concentrated in the field of fracture mechanics. However the fatigue crack initiation and growth in machines and structures usually occur in mixed mode loading. If there is any relationship between the cause of fracture in mixed mode loading and fracture surface, fracture surface pattern will be the main mean explaining reasons of fatigue fracture and obtaining further information about fracture process. In this paper low point shear-fatigue test with Aluminum alloy hi 5083-O is carried out from this prospect and then the mixed mode distribution of fracture surface is examined from the result after identifying the generation of fatigue crack surface pattern. It was found from the experimental results that the fatigue crack surface pattern and the fatigue crack shear direction are remarkably consistent. Furthermore It is possible that the analysis of distribution of mixed mode through the fatigue crack surface pattern.

Fatigue Crack Propagation Behavior of Fine Grained Al-5083 Alloy Produced by Severe Plastic Deformation (강소성법을 이용한 미세립 Al-5083 합금의 피로균열전파 거동)

  • Kim, Ho-Kyung;Yang, Kyoung-Tak;Kim, Hyun-Jun
    • Journal of the Korean Society of Safety
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    • v.22 no.2 s.80
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    • pp.15-21
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    • 2007
  • Fine grained Al-5083 alloy produced by equal channel angular pressing (ECAP) at $120^{\circ}C$ was tested for investigating mechanical properties and crack growth propagation behavior. Also, FEM stress and strain analysis for the samples during ECAP were investigated, using a plastic deformation analysis software DEFORM 2-D. Coarse grained as-received samples exhibited UTS of 255.6MPa with a elongation to failure of 34.4%. By contrast, the ECAPed fine grained samples exhibited UTS of 362.0MPa with a elongation to failure of 12.9%. Fatigue crack growth resistance and threshold of fine grained samples were lower than that of as-received coarse grained samples. The higher fatigue crack growth rate in the fine grained ECAPed samples may partially arise from small roughness closure effect due to smoother fracture surfaces.

Description of crack growth behavior of SB41 steel in terms of J integral (J적분에 의한 SB41강의 피로균열 진전 특성 평가)

  • 배원호;김상태;이택순
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.6
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    • pp.1568-1575
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    • 1990
  • Fatigue crack growth behavior was investigated in the center cracked plate of KS SB41 steel and the relation between the crack growth rate and various mechanical parameters was studied at small scale yielding, large scale yielding and full scale yielding. The crack opening ratio U was about 0.6-0.8 and had the larger value in the case of load control than that of strain control. Effective stress intensity factor range, .DELTA.K$_{eff}$ and J integral range, .DELTA.J were obtained from the notion of crack opening, and the crack growth rate was expressed with these values. The value of J integral range increased rapidly at stress ratio, R=0 in full scale yielding of load control test. COD value also increased rapidly with the increase of ligament net stress at large scale yielding of load control test.t.

Relationship between Pattern of Fatigue Crack Surface and Fatigue Crack Growth Behavior under $K_{III}$ Mode-Four Point Shear in Al 5083-O (Al 5083-O재에 있어서 $K_{III}$ 모드 4점 전단 하에서의 피로파단면 무늬와 피로균열진전거동의 관계)

  • Kim, Gun-Ho;Won, Young-Jun;Sakakura, Keigo;Fujimoto, Takehiro;Nishioka, Toshihisa
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2006.06a
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    • pp.43-44
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    • 2006
  • Generally almost all fatigue crack growth is affected by model. For this reason a study on model has concentrated in the field of fracture mechanics. However the fatigue crack initiation and growth in machines and structures usually occur in mixed mode loading. If there is any relationship between the cause of fracture in mixed mode loading and fracture surface, fracture surface pattern will be the main mean explaining reasons of fatigue fracture and obtaining further information about fracture process. In this paper four point shear-fatigue test with Aluminum alloy Al 5083-O is carried out from this prospect and then the mixed mode distribution of fracture surface is examined from the result after identifying the generation of fatigue crack surface pattern. It was found from the experimental results that the fatigue crack surface pattern and the fatigue crack shear direction are remarkably consistent. Furthermore It is possible that the analysis of distribution of mixed mode through the fatigue crack surface pattern.

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