• Title/Summary/Keyword: granule size

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Properties of Starch Isolated from Wet-milled Rice after Steeping at Elevated Temperatures for Annealing Effect (Annealing 수침처리에 따른 습식제분 쌀가루의 전분 특성)

  • Lee, Young-Tack;Yoo, Moon-Sik;Lee, Bo-Ram;Park, Jong-Hyun;Chang, Hak-Gil
    • Korean Journal of Food Science and Technology
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    • v.36 no.3
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    • pp.393-397
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    • 2004
  • Rice was steeped at elevated temperatures of $40,\;50,\;or\;60^{\circ}C$ for 2 hr, and physicochemical properties of starches isolated from wet-milled rice flour were investigated. Steeping at elevated temperatures slightly decreased lightness of rice starch, while increased yellowness and redness. Average granule size of rice starch was decreased by steeping treatment. Swelling power and solubility increased as temperature increased. Starch from rice steeped at $40^{\circ}C$ displayed highest swelling power and solubility. Differential scanning calorimetry data of starch obtained from steeped rice at $60^{\circ}C$ showed increased onset and peak temperatures, with narrower gelatinization temperature range, suggesting partial annealing effect. Pasting properties of starch measured by Rapid Visco-Analyzer indicated increased peak viscosity due to rice steeping at $40^{\circ}C$. Peak and breakdown viscosities decreased at $50\;and\;60^{\circ}C$, whereas setback and final viscosities increased.

Nondestructive investigation of clay wall structure containing traditional mural paintings. - The clay walls having mural paintings housed in the protective building in Muwisa Temple, Kangjin, Jeollanamde Province - (전통 벽화의 토벽체 비파괴진단 조사연구 - 강진 무위사 벽화보존각내 벽화를 중심으로 -)

  • Chae, Sang-Jeong;Yang, Hee-Jae;Han, Kyeong-Soon
    • Journal of Conservation Science
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    • v.18 s.18
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    • pp.51-62
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    • 2006
  • This study, in order to do a nondestructive research on the mural walls kept in the protective house in Muwisa Temple, Kangjin, took four examinations; particle size analysis, XRD analysis, ultrasonic investigation, and thermo-infrared investigation. Component ratio of mural wall varied; clay of wall bodies consisted of gravel of 1.78 g, sand of 5.39 g, silt of 4.91 g and clay of 6.26 g. Ultrasonic velocity and one-axis compression strength tests done with eight mural-painted walls yield results as follows; the value of ultrasonic velocity ranged between 71.63 and 3610.11 m/s with the average of 417.44 m/s and on-axis compression strength ranged between 70.34 and $533.28kg/cm^2$ with the average of $83.23kg/cm^2$. The value increased in the order of Bosaldo(No.6)

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Physicochemical Properties of Starch in Water Chestnut (Eleocharis kuroguwai Ohwi) (올방개 괴경 전분의 이화학적 특성)

  • Kim, Sang-Kuk;Shin, Jong-Hee;Kim, Su-Yong;Kim, Hak-Yoon;Park, Shin-Young
    • Korean Journal of Weed Science
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    • v.32 no.3
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    • pp.204-210
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    • 2012
  • The physicochemical properties of tuber starch in water chestnut have been studied. Peak viscosity, hot paste viscosity and cooling peak viscosity were 5679, 3146 and 4262 RVU, respectively. In three transition parameters, onset temperature ($T_o$), peak temperature ($T_p$), and conclusion temperature ($T_c$) were 64.1, 68.5 and $72.3^{\circ}C$, respectively. Gelatinization enthalpy (${\Delta}H$ gel) was 4.48 J/g. A-type starch has a smaller proportion (11.4%) of short chains ($DP{\geq}12$) and a larger proportion (57.2%) of short chains ($13{\leq}DP{\geq}24$). The tuber starch of water chestnut displayed an A-type X-ray diffraction pattern showing a strong diffraction peak at $2{\Theta}$ values of $15.18^{\circ}$, $17.13^{\circ}$, and $23.1^{\circ}$, and a weak peak at $2{\Theta}$ values of $18.1^{\circ}$, $20.06^{\circ}$, and $26.69^{\circ}$. Their crystallinity was 28.6% and the mean starch granule size was 21.5 ${\mu}m$.

Study on Improvement of Tungsten Alloy Granular Powder in Defense Industry (방산 분야 텅스텐 합금 과립분말 개선 연구)

  • Ji, Sangyong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.10
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    • pp.206-211
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    • 2020
  • Tungsten alloys are used widely in general industrial fields, but they are difficult to cast, so products are manufactured using powder metallurgy. In this study, a mixed powder of tungsten, nickel, and iron homogenized using a ball mill was added to pure water as a solvent, and PVA as a binder was added to prepare a spray drying mixture. The mixed liquid was prepared using a spraying machine. A study was carried out to produce a granular powder that can reduce the variations between products during the molding and sintering process of the powder metallurgy method. A preliminary experiment was conducted to confirm the influence of the variables in the granulation process. Through the preliminary test results, this experiment was performed with the volume of solvent of the spray drying the mixture as an independent variable, and granular powder having a mean particle size similar to that of the existing mass-production conditions and an increased apparent density was prepared. In addition, a pilot test was conducted for the molding and sintering process. The improved granular powder reduced the characteristic variation (weight variation) of the mass-produced product.

Microstructure and Thermoelectric Properties of n-Type $\textrm{Bi}_{2}(\textrm{Te}_{0.9}\textrm{Se}_{0.1})_3$ Fabricated by Mechanical Alloying and Hot Pressing Methods (기계적 합금화 공정으로 제조한 n형 $\textrm{Bi}_{2}(\textrm{Te}_{0.9}\textrm{Se}_{0.1})_3$ 가압소결체의 미세구조와 열전특성)

  • Kim, Hui-Jeong;Choe, Jae-Sik;Hyeon, Do-Bin;O, Tae-Seong
    • Korean Journal of Materials Research
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    • v.7 no.1
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    • pp.40-49
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    • 1997
  • $Bi_{2}(Te_{0.9}Se_{0.1})_{3}$ thermoelectric matcrials havc 11et:n fahricxted hy mechanical alloying and hot pressing methods. Microstructure and thermoelectric properties of the hot 11resseii $Bi_{2}(Te_{0.9}Se_{0.1})_{3}$ have been investigated Lvith variations of hot pressing temperature and dopmt atltiition Formation of $Bi_{2}(Te_{0.9}Se_{0.1})_{3}$ alloy powders was completed by mechanical alloying of the as-mixed Ri. Te, arid Sc grmules of ~3.6mm size for 3 hours at ball-to-material weight ratio of 5 : 1. Figure of merit of $Bi_{2}(Te_{0.9}Se_{0.1})_{3}$ was markedly incrcwieti hy hot pressing at temperatures above $450^{\circ}C$, and value of $1.9{\times}10^{-3}/K$ was obtained for the specimen hot pressed at $550^{\circ}C$. With addition of 0.015 wt% Ri as acceptor dopant, figure of merit ol $Bi_{2}(Te_{0.9}Se_{0.1})_{3}$ hot pressed $550^{\circ}C$$2.1{\times}10^{-3}/K$.

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Study on Rheological and Sensory Properties of Cooked Rices -I. Changes in Flavor and Appearance of Cooked Rices during Storge- (쌀 품종에 따른 쌀밥의 물리적 및 관능적 특성 연구 -I. 저장중 쌀밥의 풍미 및 겉모양의 변화-)

  • Kim, Chong-Kun;Hwang, Jeen-Sun;Kim, Woo-Jung
    • Applied Biological Chemistry
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    • v.30 no.2
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    • pp.109-117
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    • 1987
  • Three rice varieties of Akibare (japonica), Milyang 30 (indica) and Taebaeg (indica) were investiated for sensory and physical qualities of cooked rices during storage at the temperature range of $4^{\circ}C$ and $70^{\circ}C$ for 25 hours. The qualities studied were sensory attributes of odor, taste and appearance which were evaluated by multiple comparison method. The other properties were size of rice granule and separation Property of individual cooked rices in water. The sensory results showed that all of the descriptions except moldy odor and oily taste were scored higher values for cooked rices of Akibare than those values of Milyang 30 and Taebaeg. It was found that storage of cooked rices at various temperatures resulted a significant decrease in most of sensory qualities except moldy odor and oily taste which were rather increased. The quality change was more affected at storage at low temperature, particularly at $4^{\circ}C$, than at higher temperatures. The property of individual separation of cooked rices in water for freshly cooked rices showed that Akibare was separated 44.4% after 1 minute shaking while Milyang 30 and Taebaeg had the higher separation value of 53.1%, and 51.0%, respectively. This characteristic was noticeably reduced after 3 hours storage and then steady increased during further storage. It was also found that the separation percent was generality increased as the storage temperature increased from $4^{\circ}$ to $70^{\circ}C$.

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Ultrastructure of Sarcocystis grueneri-like Sarcocysts from Cardiac Muscle of Red Deer (Cervus elaphus) in Korea (한국산 Red Deer (Cervus elaphus)의 심근에서 관찰된 Sarcocystis grueneri 양 포낭의 투과전자현미경 소견)

  • Son, Hwa-Young;Kim, Nam-Soo;Ryu, Si-Yun;Kim, Hyeon-Cheol;Rhee, Ju-Hee;Cho, Jeong-Gon;Park, Bae-Keun
    • Journal of Veterinary Clinics
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    • v.26 no.6
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    • pp.595-599
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    • 2009
  • Sarcocystis grueneri-like sarcocysts were found from the cardiac muscles of a rearing red deer (Cervus elaphus) carcass in Korea. In the light microscopical examination of sarcocysts, they were oval to spherical cysts and 90-170$\times$110-380 ${\mu}m$ in size. However, there was no inflammation and myofiber degeneration. In the transmission electron microscope, these cysts were located within the sarcoplasm of the host cell and filled with merozoites. The sarcocysts were enclosed by a very thin wall (0.45-0.6 ${\mu}m$ thick) that consists of protrusions and ground substance. The primary cyst wall formed numerous strip-like protrusions which were 0.2-0.3 ${\mu}m$ wide and up to 4.2 ${\mu}m$ long. The protrusions were running in parallel with the surface of the cyst. A characteristic of the cyst wall was absent of fibrils inside the protrusions. Merozoites in the compartment measured about $15\times4\;{\mu}m$. The merozoite consisted of four regions: micronemes and rhoptries, amylopectin granule, nucleus, and amylopectin granules. The number of rhoptry was counted in 7-13.

AN EXPERIMENTAL STUDY ON THE HEALING PROCESS OF TOOTHASH, PLASTER OF PARIS AND AUTOGENOUS BONE COMPOSITE GRAFTING IN DOGS (치아회분과 석고혼합제재 매식과 자가골 동시 이식후 치유과정에 관한 실험적 연구)

  • Yeo, Hwan-Ho;Jung, Jae-Hun;Lee, Sang-Ho;Kim, Heung-Jung;Kim, Young-Kyun;Lim, Seung-Cheul;Sul, In-Tak
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.22 no.1
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    • pp.1-14
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    • 2000
  • The purpose of this study was to evaluate the efficacy of adding autogenous bone to the toothash-plaster mixture in the healing process of bone. Full-thickness round osseous defects with the diameter of 20mm were made at the calvarial bone of adult dogs (n=19) bilaterally, which were thought to be critical size defect. The right defects were repaired with the toothash-plaster mixture plus autogenous bone (compressed volume 0.3cc) and the left defects with only toothash-plaster mixture. At 2-, 4-, 8-, 12- and 20- week after implantation, dogs were sacrificed and evaluated the osseous healing of bony defects clinically, radiographically, and microscopically. The results were as follows; 1. At the clinical observation, the wound healed very well without any problem except severe swelling in the early period after operation. Slight depression was recognized at the both sides when the portions of cranial defect were palpated. 2. There were statistically significant differences between toothash-plaster mixture groups and autogenous bone added groups at the same period, and among the groups in the bone density of the digital radiograms (P<0.001). There was a tendency that bone density was increasing with time. 3. In light microscopic examination, new bone formation was more active in the autogenous bone added groups than toothash-plaster mixture groups at the early period after implantation but there is little difference at 20-week after implantation. 4. In fluorescent microscopic examination, the fluorescent band could be observed at the area of active bone formation and the band was more distinct in the autogenous bone added groups then toothash-plaster mixture groups. 5. In transmitted electron microscopic examination, organelles such as rER, Golgi complex and secretory granule and osteoblast were observed. In summary higher volume ratio of autogenous bone is needed to improve the bone healing in that there is little difference between toothash-plaster mixture group and autogenous bone added group at the 20-week after implantation in spite of new bone formation was more active in the autogenous bone added groups than toothash-plaster mixture groups at the early period after operation.

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Ultrastructural Study on the Cutaneous Granular Glands in Bombina orientalis Boulenger (무당개구리(Bombina orientail Boulenger) 피부 과립선의 미세구조에 관한 연구)

  • 김기영;김관선;문명진;김우갑
    • The Korean Journal of Zoology
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    • v.32 no.2
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    • pp.107-119
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    • 1989
  • The histochemical characteristics of the cutaneous granular glands and its fine structure of the Korean fire bellied toad, Bombino orientalis Boulenger the only species inhabitated in Korea, were studied with light and electron microscopes. By the granular size and histochemical properties, the granular glands were subdivided into two types. The type I glands have small secretory granules (3.6 $\mu$ m), whereas the type II glands contain relatively larger granules (7.5 $\mu$ m). These two types of glands were simple alveolar gland, and they were commonly composed of inner glandular epithelial cells and outermost myoepithelial cells. By the histochemical reactions, these two secretory granules were not responsed to Alcian blue, but weakly positive reaction was observed in type I granular glands by the PAS reaction. And by the scanning electron microscopic observation, extemal morphology of the opening site of the gland duct was resembled to the stomata of the plant leaves. Especially the epithelial cells of the type I glands had fine reticular surface whereas, type II glands had large vesicular surface. These types of the glands conimonly had larger cavities than those of mucous glands, and forming the multinucleated unicellulr structure (syncytium) at the glandular epithelial layers. Secretory granules of these glands were originated from the rough endoplasmic reticulum of the glandular epithelial cells, and by the maturation level of the granule, morphological diversities appeared.

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Morphological Change of Men's Hair Shaft by Weathering (풍화작용에 의한 정상모발의 형태학적 변화)

  • Hong, Wan-Sung;Chang, Byung-Soo;Lim, Do-Seon;Park, Sang-Ock;Yoe, Sung-Moon
    • Applied Microscopy
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    • v.30 no.1
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    • pp.11-20
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    • 2000
  • The morphological changes in normal and weathering hair shafts of the human scalp were investigated by using the transmission and scanning electron microscopes. The hair shaft composed of cuticular layer, cortex and medula. The surface of normal hairs are smooth and covered by imbricated cuticular scales. The cuticular layer consists of five to seven cuticle cells. These cells, which are flat and thin, measuring about $100{\mu}m$ long and $0.4{\mu}m$ thick, appears intercellular membrane complex in diameter 25 nm. The cortex composed of melanin granules and cornified cells, which multicomponent concentric microfibrils in diameter about 8 nm give rise to macrofibrils in diameter $0.5{\mu}m$ to $0.8{\mu}m$ encased in limiting membrane. The melanin granules are spherical shaped about $0.5{\mu}m$ in size and scattered between macrofibrils. The medulla in the normal hairs are $16{\mu}m$ in diameter centrally region of cortex. Normal hair shafts undergo progressive degenerative changes due to a variety of environmental insults. In the initial weathering process of hair, the cuticular scales became irregularly raised and broken, and then cuticle cells formed cytoplasmic vacuolation, following dissociated intercellular membrane complex, ultimately entirely lost and nuded cortex. Occasionally, transverse fissures were seen at hair shafts indicating that the hairs were deteriorated. Complete removal of the cuticular layer in the heavily damaged cortex portions appeared splitting of the cortical cell into its macrofibrils and scattering of melanin granules.

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