• 제목/요약/키워드: grain-size distribution

검색결과 657건 처리시간 0.025초

Pb($Zr_{0.52}$ $Ti_{0.48}$)$O_3$세라믹스의 유전 및 압전성에 미치는 $MnO_2$ 의 영향 (Effects of $MnO_2$ on the Dielectric and Piezoelectric Properties of Pb($Zr_{0.52}$ $Ti_{0.48}$)$O_3$ Ceramics)

  • 김종선;윤기현;최병현;박종옥;이종민
    • 한국세라믹학회지
    • /
    • 제27권2호
    • /
    • pp.187-194
    • /
    • 1990
  • Effects of MnO2 addition ranged from 0.0wt% to 5.0wt% on the microstructure and dielectric and piezoelectric properties of the Pb(Zr0.52 Ti0.48)O3 Ceramics have been investigated. The solubility limit of MnO2 in Pb(Zr0.52 Ti0.48)O3 is about 0.5wt%, and MnO2 as a valence state of Mn3+ is substituted for (Zr, Ti) lattice site in PZT solid-solution. The addition of MnO2 up to 0.5wt% in Pb(Zr0.52 Ti0.48)O3 brings increase of density, but decreased of grain size and tetragonality. Dielectric constant slightly decreases, but both coupling factor(Kp) and mechanical quality factor(Qm) increase with the addition of MnO2. However, excess amount of MnO2 addition more than 0.75wt% results in rapid decrease of resistance. Dielectric constant and tan $\delta$ increase due to the second phase and inhomogeneous Mn distribution.

  • PDF

시추코어 분석 및 데이터베이스화를 위한 칼라 코어스캐너의 응용 (Applicability of Color Corescanner to the Analysis and Data-base of Drill Cores)

  • 김중열;;김유성;현혜자
    • 한국지반공학회:학술대회논문집
    • /
    • 한국지반공학회 2001년도 봄 학술발표회 논문집
    • /
    • pp.249-256
    • /
    • 2001
  • Optical Color Corescanner firstly developed by DMT-GeoTec, Germany and further upgraded through the Korea-Germany joint project is capable of duplicating the core surfaces. The tool uses a digital CCD line camera. As the core is rotated by an electric motor, the camera scans the uppermost line, everytime with a circumferential increment of up to 0.05mm(20pixels/mm) and hence a complete 360$^{\circ}$ unwrapped image(core image) is produced. This paper illustrated diverse research benefits of such core images from several test sites in our country. All scanned images could be stored as a data-base one and easily used with software facilities \circled1 to evaluate a percental distribution of mineral components or grain size etc. not only for the rock classification but also for e.g. the assessment of building stones, \circled2 to study potential reservoirs as a hydrocarbon indicator using ultraviolet fluorescence reflection from cores, \circled3 to facilitate the qualitative and quantitative analysis of fractures, \circled4 to evaluate the fractures and thin bedded reservoirs using spectral color responses. Based on abundant scanning experiments, it would seem that this imaging work should lead to reflecting the future trend in underground survey toward a more comprehensive understanding of the properties and behaviors of in situ rocks.

  • PDF

Depositional Environment and Distribution of Heavy Metal off the Shihwa Dam

  • Oh, Jae-Kyung
    • Journal of the korean society of oceanography
    • /
    • 제32권3호
    • /
    • pp.120-127
    • /
    • 1997
  • Depositional environment off the Shihwa Dam has been studied to investigate the change of sedimentation process and the pollution. In order to understand how the sediments are distributed, polluted and modified, depositional factors have been analyzed and compared with the previous data. Study area, located off the Shihwa Dam, was surveyed to collect 25 bottom samples and 2 cores in 1996 and echo-sounding in 1997. These sediments were analyzed for the study of the global characteristics of sediment such as grain size and organic matter. Among these samples, the selected twenty surface sediments were analyzed for the comparison with their contents of metallic elements (Al, Mn, Fe, V, Cr, Co, Ni, Cu, Zn, Cd, Pb, As). According to field and lab analysis of sediments, three sedimentological zones have been generally identified around study area; near the dam (sandy Silt), near the dike (Sand) and offshore (silty Sand) zones. Textural parameters show that the content of silt and clay is dominant near the dam excepting the dike zone of LNG Storage Base and offshore (Palmido). The total concentration of Mn, Ni, Fe, Zn and Cd in bulk sediments was increased after the construction of the dam, while the content of Mn and Cr were higher near tidal channel than in the offshore area. Meanwhile, the annual increasing pattern of some heavy metal has appeared in this area. Based on this primary study, modification of the depositional environment may be caused by the construction of the dam and LNG Storage Base. Additionally, environmental evaluation on organic/inorganic factors has been suggested for interpreting environmental changes caused by coastal development in the nearshore such as the Shihwa coastal area.

  • PDF

시멘트함량 및 다짐함수비가 Soil Cement의 압축강도에 미치는 영향에 관한 연구 (A Study on the Effects of Molding Water Content and Cement Content on Unconfined Compressive Strength of Soil Cement Mixtures)

  • 김재영;강예묵
    • 한국농공학회지
    • /
    • 제17권1호
    • /
    • pp.3685-3701
    • /
    • 1975
  • This study was conducted to investigate the strength of soil cements for varied molding water content and cement content(3,6,9,12%) in four cementstabilized soils(KY: sand, MH: sad, SS: sandy loam, JJ: loam). The eoperimental results obtainedfrom unconfined compressive strength tests are asfollows: 1. The optimum moisture content increased in accordance with the increase of the cement while maximum dry density didn't change uniformly. 2. The moisture content for maximum strength was higher than the optimum moisture content in the higher cement content. Moisture-density curves showed a dull peak in the higher cement contents, on the other hand, a sharp peak in the lower cement contents. 3. In molding the specimen with the approximate optimum moisture content, the maximum strength showed at the wet side of the optimum moisture content. 4. SS and JJ maybe used as cement-stabilized base of road to require 300PSI of compressive strength cured seven days, but MH and KY may be not adequate. 5. In soil cement, the better the grain size distribution was, the stronger the compressive strength was itn general. 6. The relation between 28-day strengh and 7-day strength in the cementstabilized four soils may be expressed as follows: q28=1.55q7+1.5 in which q28:28-day strength. q7:7-day strength.

  • PDF

화강암질 풍화토의 시멘트에 의한 안정처리에 관한 연구 (내구성을 중심으로) (The Study on Portland Cement Stabilization on the Weathered Granite Soils (on the Durability))

  • 도덕현
    • 한국농공학회지
    • /
    • 제22권3호
    • /
    • pp.60-74
    • /
    • 1980
  • Soil-cement mixtures involve problems in it's durability in grain size distribution and mineral composition of the used soils as well as in cement content, compaction energy, molding water content, and curing. As an attempt to solve the problems associated with durability of weathered granite soil with cement treated was investigated by conducting tests such as unconfined compression test, it's moisture, immers, wet-dry and freeze-thaw curing, mesurement of loss of weight with wet-dry and freeze-thaw by KS F criteria and CBR test with moisture curing on the five soil samples different in weathering and mineral composition. The experimental results are summarized as follows; The unconfined compressive strength was higher in moisture curing rather than in the immers and wet-dry, while it was lowest in freeze-thaw. Decreasing ratio of unconfined compressive strength in soil-cement mixtures were lowest in optimum moisture content or in the dry side rather than optimum moisture content with freeze-thaw. The highly significant ceofficient was obtained between the cement content and loss of weight with freeze-thaw and wet-dry. It was possible to obtain the durability of soil-cement mixtures, as the materials of base for roads, containing above 4 % of cement content, above 3Okg/cm$_2$ of unconfined compressive trength with seven days moisture curing or 12 cycle of freeze-thaw after it, above 100% of relative unconfined compressive strength, 80% of index of resistance, below 14% of loss of weight with 12 cycle of wet-dry and above 1. 80g/cm$_2$ of dry density.

  • PDF

The Effect of Uni-nanoadditive Manufactured Using RF Plasma Processing on Core-shell Structure in MLCC

  • Song, Soon-Mo;Kim, Hyo-Sub;Park, Kum-Jin;Sohn, Sung-Bum;Kim, Young-Tae;Hur, Kang-Heon
    • 한국세라믹학회지
    • /
    • 제46권2호
    • /
    • pp.131-136
    • /
    • 2009
  • Radio frequency (RF) plasma treatment is studied for the size reduction and the spheroidization of coarse particles to change them into nano-sized powders of spherical shape in MLCC fields. The uni-nanoadditives manufactured by RF plasma processing for high dispersion have been investigated for the effect on core-shell structure in dielectrics of MLCC. Microstructures have been characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and Electron Probe Micro Analyzer (EPMA). We compared the distribution of core-shell grains between specimens manufactured using uni-nanoadditive and using mixed additive. In addition, the uniformity of rare earth elements in the core-shell structured grains was analyzed. It was shown, from TEM observations, that the sintered specimen manufactured using uni-nanoadditives had more dense small grains with well-developed core-shell structure than the specimen using mixed additives, which had a homogeneous microstructure without abnormal grain growth and shows broad temperature coefficient of capacitance (TCC) curves in all temperature ranges because of well dispersed additives.

Crystallographic and Magnetic Properties of Li0.7Co0.2Ti0.2V0.2Fe1.7O4 Ferrite

  • Chae, Kwang-Pyo;Kwon, Woo-Hyun;Lee, Jae-Gwang
    • Journal of Magnetics
    • /
    • 제15권1호
    • /
    • pp.25-28
    • /
    • 2010
  • This study examined the crystallographic and magnetic properties of vanadium-substituted lithium cobalt titanium ferrite, $Li_{0.7}Co_{0.2}Ti_{0.2}V_{0.2}Fe_{1.7}O_4$. Ferrite was synthesized using a conventional ceramic method. The samples annealed below $1040^{\circ}C$ showed X-ray diffraction peaks for spinel and other phases. However, the sample annealed above $1040^{\circ}C$ showed a single spinel phase. The lattice constant of the sample was $8.351\;{\AA}$, which was relatively unaffected by vanadium-substitution. The average grain size after vanadium-substitution was $13.90\;{\mu}m$, as determined by scanning electron microscopy. The M$\ddot{o}$ssbauer spectrum could be fitted to two Zeeman sextets, which is the typical spinel ferrite spectra of $Fe^{3+}$ with A and B sites, and one doublet. From the absorption area ratio of the M$\ddot{o}$ssbauer spectrum, the cation distribution was found to be ($Co_{0.2}V_{0.2}Fe_{0.6})[Li_{0.7}Ti_{0.2}Fe_{1.1}]O_4$. Vibrating sample magnetometry revealed a saturation magnetization and coercivity of 36.9 emu/g and 88.6 Oe, respectively, which were decreased by vanadium-substitution.

A5083-0 알루미늄 합금재의 용접부위의 평면 굽힘 피로에 의한 피로균열성장 특성에 관한 연구 (A study on the fatigue crack growth characteristics of weldments of A5083-0 Al-alloy by plane bending fatigue)

  • 김원녕;김기준;임종문
    • Journal of Advanced Marine Engineering and Technology
    • /
    • 제10권1호
    • /
    • pp.65-73
    • /
    • 1986
  • Surface fatigue crack propagation tests by plane bending fatigue were conducted on the welding specimens of an aluminium alloy, A5083-0, having an edge through thickness notch to study the fatigue crack growth characteristics. Moreover, the experiments were performed in order to clarify the fatigue crack initiation and growth. The properties of fatigue crack growth were quantitatively inspected in welded metal, heat-affected zone and base metal of the welding specimens. The main results obtained are summarized as follows: 1. It is found that the hardness distributions of A5083-0 aluminium alloy weldments are quite different with those of steel material weldments, so that the hardness distribution becomes lower in the following order: base metal, heat-affected zone and weld metal. 2. It is observed that the grain size of this specimen weldment appears to be almost equal to the base metal, when TIC welding method is adopted. 3. In a surface fatigue crack initiation and growth, the fatigue crack does not begin by opening-closing mechanism until hardening is saturated at the crack tip. 4. The fatigue crack growth characteristics of A5083-0 alluminium alloy weldments can be concluded.$${\frac{da}{dn}}=C({\Delta}K)^n=3.8{\times}10^{-9}{({\frac}{1}{2}{\Delta}S_t{\sqrt{{\pi}a}})}^{2.4}$$

  • PDF

하상사력재를 이용한 CFRD의 연구 (A Study of CFRD using a Gravel Fill)

  • 정찬균;노태길;이송
    • 한국지반공학회:학술대회논문집
    • /
    • 한국지반공학회 2008년도 추계 학술발표회
    • /
    • pp.842-853
    • /
    • 2008
  • In the construction of dam, the key factor which decides the type of dam is security of materials resource. Because of the large scale earth work, the ability to supply the materials is essential part about economical efficiency. The research is the case study about controlling the plan to secure the material resources in the design of Buhang multipurpose dam. In case of Buhang multipurpose dam, at that time of basic design, it was planned to use a rock fill material. From the detail investigation about the river bed accumulative layer widely spread on the submerged district on the basic design, the research is accomplished to replace rock material with gravel material. After the investigation of whole reserves of gravel material, estimation of conformity as dam construction material from analysis of grain size distribution, the case study of oversea construction, and the material property comparison between rock fill material and gravel fill material, it is verified th possibility of using the gravel fill. Thereafter, the analysis of dam stability using a gravel fill material is accomplished. Finally, A gravel fill material can be used as the main construction material of CFRD, therefore the efficiency of resource recycling in the submerged area is maximized, and the established plan is more advantageous to stability, constructibility, environmentibility than the case of using a rock fill.

  • PDF

Effect of Microstructure on the Corrosion Resistance of Nd-Fe-B Permanent Magnets

  • Li, Jiajie;Li, Wei;Li, Anhua;Zhao, Rui;Lai, Bin;Zhu, Minggang
    • Journal of Magnetics
    • /
    • 제16권3호
    • /
    • pp.304-307
    • /
    • 2011
  • High performance Nd-Fe-B magnets can be manufactured by both sintering and hot deformation. The corrosion behaviors of the magnets prepared by the two processes were compared. Effect of microstructure on the corrosion resistance of Nd-Fe-B magnets was also investigated. A neutral salt spray test (NSS) was performed for the different-processed magnets. The weight losses of the samples after the corrosion test were measured. The corrosion microstructures were observed using a scanning electron microscope. It shows that the corrosion resistance of hot deformed magnets is much better than that of the sintered ones because the grain size and the distribution of Nd-rich phases of the hot deformed magnets are much finer and more uniform than those of the sintered ones. The different microstructure between the sintered and the hot deformed magnets causes the different corrosion behavior.