• Title/Summary/Keyword: gas getter

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How to Eliminate CO, CO2 and CH4 in H2 & Inert Gas -Possibility of Fuel Cell Application- (수소와 불활성 가스 중 일산화탄소, 이산화탄소, 메탄 제거에 관한 연구 -연료전지에의 적용 가능성-)

  • Lee, Taek-Hong;Cheon, Young-Ki
    • Transactions of the Korean hydrogen and new energy society
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    • v.15 no.3
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    • pp.220-227
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    • 2004
  • The purpose of this paper is, based on the theoretical background of the principle of gas purification and absorption, and the absorbing ability of metals, to syudy the efficiency of gas purification of inorganic gases using Zr alloys, so as to contribute to the IT industry. To produce and distribute gas with high purity and ultra-high purity, different types of gas purifier are currently being used: distillation type, getter type, catalyst type, absorption at low-temperature type, and membrane separation equipment. From the different purification methods mentioned above, the getter type gas purifier is capable of not only high performance and capacity but also P.O.U(Point Of Use) method. The key of the getter type gas purifier is its efficiency of gas purification, which is the subject chosen for this study.

Fabrication and Characterization of Hydrogen Getter Based on Palladium Oxide Doped Nanoporous SiO2/Si Substrate (PdOx가 도핑된 나노 기공구조 SiO2/Si 기반의 수소 게터 제작 및 특성평가)

  • Eom, Nu Si A;Lim, Hyo Ryoung;Choi, Yo-Min;Jeong, Young-Hun;Cho, Jeong-Ho;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • v.24 no.11
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    • pp.573-577
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    • 2014
  • The existing metal getters are invariably covered with thin oxide layers in air and the native oxide layer must be dissolved into the getter materials for activation. However, high temperature is needed for the activation, which leads to unavoidable deleterious effects on the devices. Therefore, to improve the device efficiency and gas-adsorption properties of the device, it is essential to synthesize the getter with a method that does not require a thermal activation temperature. In this study, getter material was synthesized using palladium oxide (PdOx) which can adsorb $H_2$ gas. To enhance the efficiency of the hydrogen and moisture absorption, a porous layer with a large specific area was fabricated by an etching process and used as supporting substrates. It was confirmed that the moisture-absorption performance of the $SiO_2/Si$ was characterized by water vapor volume with relative humidity. The gas-adsorption properties occurred in the absence of the activation process.

Pumping Performance Test of the NEG Elements (비증발형 게터소자 배기특성 평가시험)

  • 인상렬;박미영;정기석
    • Journal of the Korean Vacuum Society
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    • v.13 no.2
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    • pp.47-53
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    • 2004
  • A getter pump test system is being developed as a core item of the national project for establishing the foundation of the vacuum technology in our country. A preliminary test system was prepared for developing the getter test procedure, and providing design requirements and system specifications before setting up the getter pump test system. The pumping speed and the pumping capacity of getter elements of low activation temperature used in the seal-off vacuum devices, for the hydrogen, carbon monoxide and nitrogen gases, were measured using the preliminary test system. The pumping characteristics of a domestic getter, developed mainly for the gas purifier, were compared with those of a foreign getter used widely in the lamp factories.

Characterization of the Hydrogen Reservoir for a High Power Gas Switch

  • Lee, B.J.;Park, S.S.;Kim, S.H.;Kwon, S.J.;Jang, S.D.;Joo, Y.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.261-261
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    • 2012
  • This paper presents the understandings carried out for the installation of the hydrogen reservoir of the multi-gap pseudospark switch under developing for the accelerator applications. As a cold cold cathode switch, the pseudospark switch could replace the thyratron switch which has hot cathode and being used well currently in the high power field such as laser and accelerator applications. Especially in the klystron modulator, the key component is a switch which mostly defines the jitter and the instability of the modulator system. To get the less jitter and the instability, we need to find proper range of the pressure for the gas discharge inside gas switch. This could be achieved by the understanding of the characteristic of the nonevaporable getter (NEG) which is used as a hydrogen reservoir for the switch. Therefore we verified the characteristics of the NEG (St 172, Saes) and its installation in the switch. Finally we controlled the getter to find best pressure point for the pseudospark switch.

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When Methane is decomposed on the CRT Manufacturing Process

  • Lee, Byoung-Joo;Hong, Sang-Pyo;Ko, Byoung-Doo;Hwang, Cheol-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.1051-1052
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    • 2002
  • Vacuum surroundings in Cathode Ray Tubes (CRT) are very important factor for CRT lifetime, especially cathode & getter's. A getter is a very good vacuum pump; unfortunately, it cannot absorb an inert gas and hydrocarbons. There are only argon and helium in CRT after $1^{st}$ emission test because other active gases are absorbed by getter and methane is decomposed during CRT working. It is also very important to know exactly where and when methane is decomposed during the CRT manufacturing process, because methane is known to be harmful to cathode when its amount is high, and getter can't absorb the methane.

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Synthesis of Zirconium-Based Nanopowder by the Plasma Arc Discharge Process (플라즈마 아크 방전법에 의한 Zr계 나노분말 제조)

  • Lee, Gil-Geun;Kim, Kyong-Ju;Park, Je-Shin
    • Journal of Powder Materials
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    • v.14 no.1 s.60
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    • pp.63-69
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    • 2007
  • The present study was focused on the synthesis of a zirconium-based alloyed nanopowder by the plasma arc discharge process. The chemical composition, phase structure, particle size and hydrogen sorption property of the synthesized powders under various synthesis conditions were analyzed using XRF, XRD, SEM, XPS and the ASTM-F798 method. The chemical composition of the synthesized Zr-V-Fe-based powders approached that of the raw material with an increasing hydrogen fraction in the powder synthesis atmosphere. The synthesized $Zr_{55}V_{29}Fe_{16}$ powder consist of a mixed phase structure of the $Zr,\;ZrH_2,\;FeV\;and\;Zr(V_{1-x}Fe_{x})_2$ phases. This powder has an average particle size of about 20 nm. The synthesized $Zr_{55}V_{29}Fe_{16}$ nanopowder showed getter characteristics, even though it had a lower hydrogen sorption speed than the $Zr_{57}\;V{36}\;Fe_7$ getter powder. However, the synthesized Zr nanopowder with an average particle size of 20 nm showed higher hydrogen sorption speed than the $Zr_{57}\;V{36}\;Fe_7$ getter powder.

An impurity analysis study in ultra high purity Hydrogen stream: The utilization of Atmosperic Pressure Ionization Mass Spectrometer (고순도 수소가스내에 존재하는 불순물의 분석 연구: 대기압 이온화 질량분석기의 이용)

  • Lee, H.S.;Lee, T.H.
    • Transactions of the Korean hydrogen and new energy society
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    • v.16 no.3
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    • pp.290-295
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    • 2005
  • For the application of fuel cell, the content and concentration of impurities in hydrogen stream must be classified. The purpose of this study is to provide analysis tool for the determination of impurities in hydrogen with ultra high purity. To produce UHT hydrogen, we purified hydrogen gas by both getter-based catridge and liquid-nitrogen soaked catridge. We compare two methods and propose new method to know about what is in hydrogen stream.

Study on the measurement of activation temperature of Non-Evaporable Getter (비증발형 게터의 활성화 온도 측정방법에 관한 연구)

  • Lee D. J.;Kim K. B.;In S. R.;Lim J. Y,;Kim W. B.
    • Journal of the Korean Vacuum Society
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    • v.14 no.1
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    • pp.1-6
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    • 2005
  • Getters are invariably covered with thin layers of oxides even in air. For the getter to function properly it is necessary to activate them by heating in vacuum during which the oxide layer is removed exposing clean surface. The so-called activation temperature is an important parameter along with gas sorption capacity since it determines the maximum temperature of a device in which a getter can be installed. Nevertheless, no standard method to measure activation temperature has been documented yet. In this study, a relatively simple method to measure the activation temperature based on the ultimate pressure measurement was suggested. The activation temperature of TiZrV alloy measured by the method was between 100℃~200℃.

Design of Tritium Handling System(II): Injection System, Regeneration System (삼중수소취급계통의 설계(II): 주입계통, 재생계통)

  • 김광신;김경숙;정은수;손순환;김위수
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2003.11a
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    • pp.117-123
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    • 2003
  • In succession to the previous paper, the tritium injection system and the regeneration system of the tritium handling system are presented. Both systems should be placed inside glove boxes since there can be potential leakage of tritium from these systems. The tritium injection system should be capable of measuring the exact amount of the injected tritium to keep track of the tritium inventory. The tritium injection system is designed to recover the remaining tritium from the system after injection for the minimization of tritum release to the environment as well as for the recovery of precious resource. TRS equipment such as MS, Ni catalyst bed, and metal getter are regenerated with a standalone regeneration system. Unlike other equipments which can be regenerated by heating and purging with appropriate gas, regeneration of the metal getter used to recover tritium is somewhat complicated.

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