• 대한치과기공학회지
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• 제35권1호
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• pp.19-27
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• 2013

Purpose: The aim of this research was to evaluate the shear bond strength of different zirconia veneering ceramics with and without liner glass materials to yttria partially-stabilized tetragonal zirconia polycrystalline(Y-TZP). Methods: Five co mmercial zirconia veneering ceramics were used in this study, E-Max(EM), Creation ZI(CR), Cercon ceram kiss(CE), Triceram(TR) and Zirkonzahn ICE(ZI). All samples were prepared according to manufacturer's instructions. Experimental industrially manufactured Y-TZP ceramic blocks(diameter: 2.7 mm; height: 13.5 mm) were used in this study. Shear bond strength between zirconia ceramic coping and zirconia veneering ceramics were evaluated by the push-shear bond test. The fracture load data were analyzed using ANOVA and Scheffe's test(${\alpha}$=0.05). The fractured surfaces of zirconia core ceraimc and zirconia veneering ceramics were observed using a scanning electron microscope(SEM). Results: The mean shear bond strengths ranged from 20 MPa ($20.12{\pm}6.34$ MPa) to 66.6 MPa ($66.62{\pm}10.01$ MPa). The Triceram(TRG) showed the highest value and Creation ZI(CR) showed the lowest value. In all groups, Zirconia liner and glass material groups was significantly higher shear bond strength than without liner(P<0.05), with the exception of Cercon ceram kiss(CE)groups. Conclusion: Zirconia bonding materials may have the advantage of improved bond strength between zirconia ceramic core and veneering ceramics.

• 대한기계학회논문집A
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• 제29권5호
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• pp.663-670
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• 2005

DIN CK35 (JIS S35CK) steels have been used as a material in fuel pump blocks for marine engines. Failures in the inner surface of a drilling hole, due to the initiation of fatigue cracks have been frequently reported. However, the mechanism initiating these cracks and growths has not been clearly diagnosed yet. This study was conducted using a scraped fuel pump block, containing an initiated fatigue crack in the inner surface of a drilling hole. Initially, the cracks and fractured surfaces inside the block were investigated using an optical microscope and a SEM (Scanning Electron Microscope). In addition, microstructure observation, fatigue life test and fatigue crack growth test were performed using a specimen, which was taken from the same block. Results from these tests are summarized as follows; (1) The early crack in the block was supposed to occur inside the inner surface of the drilling hole. (2) The fatigue endurance of this material was about 330 Mpa. (3) The early crack was generated in the cavitations created by the breakdown of a big inclusion, or separation between the big inclusion and the base metal, in which the fundamental ingredients of the inclusion were C, 5, and Mn. (4) In order to prevent these types of failures, the suppression of inclusions inflow by improving the casting process, formation of fine inclusions by applying a heat treatment process, and coating of the surface of the drilling hole were required.

• Journal of Welding and Joining
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• 제34권1호
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• pp.59-67
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• 2016

The automotive manufactures increase their use of lightweight materials to improve fuel economy and energy usage has a significant influence on the choice of developing materials. To meet this requirements manufacturers are replacing individual body parts with lightweight metals, for these the process treating and painting surfaces is changing. The pre-coated steels are newly developed to avoid the conventional complex and non-environmental painting process in the body-in-white car manufacturing. The development of new joining techniques is critically needed for pre-coated steel sheets, which are electrically non-conductive materials. In the present study, dissimilar combination of pre-coated steel and galvanized steel sheets were joined by the self-piercing rivet, adhesive bonding and hybrid joining techniques. The tensile shear test and free falling high speed crash test were conducted to evaluate the mechanical properties of the joints. The highest tensile peak load with large deformation was observed for the hybrid joining process which has attained 48% higher than the self-piercing rivet. Moreover, the hybrid and adhesive joints were observed better strain energy compared to self-piercing rivet. The fractography analyses were revealed that the mixed mode of cohesive and interfacial fracture for both the hybrid and adhesive bonding joints.

• 폴리머
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• 제27권3호
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• pp.183-188
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• 2003

유전체 분광계를 사용하여 불소함유 에폭시 수지, 벤조트리플루오라이드의 다이글리시딜 에테르(FER)/다이아미노다이페닐메탄 (DDM)과 비스페놀 A의 다이글리시딜 에테르 (DGEBA)DDM 시스템의 유전상수를 측정하였으며, DMA와 TGA에 의한 열분석을 통하여 유리 전이 온도 및 열분해 개시온도, 최대 무게 감량시 온도, 그리고 분해 활성화 에너지 등 열안정성 인자를 고찰하였다. 경화된 시편의 기계적 물성은 파괴 인성, 굴곡강도 및 충격강도 실험을 통하여 알아보았으며, 주사전자 현미경을 사용하여 시편의 파단 특성을 조사하였다. 실험 결과, DGEBA/DDM 시스템에 비해 FER/DDM 시스템은 낮은 유전 상수를 나타내었으며, 경화된 시편의 기계적 물성은 높은 값을 나타내었다. 이는 trifluoromethyl (CF$_3$) 기의 도입으로 인하여 전기적 특성과 기계적 물성이 증가한 것으로 사료된다.

• Smart Structures and Systems
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• 제3권1호
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• pp.51-68
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• 2007

High-strength concrete (HSC) is becoming increasingly attractive for various construction projects since it offers a multitude of benefits over normal-strength concrete (NSC). Unfortunately, current design provisions for shear capacity of RC slender beams are generally based on data developed for NSC members having a compressive strength of up to 50 MPa, with limited recommendations on the use of HSC. The failure of HSC beams is noticeably different than that of NSC beams since the transition zone between the cement paste and aggregates is much denser in HSC. Thus, unlike NSC beams in which micro-cracks propagate around aggregates, providing significant aggregate interlock, micro-cracks in HSC are trans-granular, resulting in relatively smoother fracture surfaces, thereby inhibiting aggregate interlock as a shear transfer mechanism and reducing the influence of compressive strength on the ultimate shear strength of HSC beams. In this study, a new approach based on genetic algorithms (GAs) was used to predict the shear capacity of both NSC and HSC slender beams without shear reinforcement. Shear capacity predictions of the GA model were compared to calculations of four other commonly used methods: the ACI method, CSA method, Eurocode-2, and Zsutty's equation. A parametric study was conducted to evaluate the ability of the GA model to capture the effect of basic shear design parameters on the behaviour of reinforced concrete (RC) beams under shear loading. The parameters investigated include compressivestrength, amount of longitudinal reinforcement, and beam's depth. It was found that the GA model provided more accurate evaluation of shear capacity compared to that of the other common methods and better captured the influence of the significant shear design parameters. Therefore, the GA model offers an attractive user-friendly alternative to conventional shear design methods.

• 한국터널지하공간학회 논문집
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• 제15권1호
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• pp.1-11
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• 2013

강섬유 보강콘크리트는 NATM 터널의 숏크리트와 세그먼트 등 라이닝에 주로 적용된다. 터널화재시 라이닝은 화재에 직접적으로 노출되기 때문에 고온노출시 SFRC의 성능변화는 매우 중요하다. 본 연구에서는 고온에 노출된 강섬유보강콘크리트의 인장성능을 DPT 실험을 통하여 검토하였다. 고온 노출온도, 강섬유 혼입률 및 종류가 파괴형태, DPT 인장강도, 실험의 변동계수에 미치는 영향을 분석하였다. 실험결과, 강섬유 보강으로 인한 잔존인장강도의 증가를 확인하였으며, 혼입률이 증가할수록 효과적임을 확인하였다. 그러나, DPT 인장강도는 고온노출로 인한 파괴면의 변화를 고려할 수 없기 때문에 파괴에너지의 고찰이 필요한 것으로 판단된다.

• 접착 및 계면
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• 제18권3호
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• pp.118-126
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• 2017

천연섬유강화 복합재료에서 여러 가지 섬유표면 개질을 통해서 천연섬유와 고분자매트릭스 사이에 계면접착과 복합재료 특성을 향상시키고자 하는 많은 연구 노력이 있었다. 본 연구에서는 폐양모섬유 강화 폴리프로필렌 매트릭스 복합재료를 압축성형공정 방법으로 제조하였고, 그들의 기계적 특성 및 충격 특성을 분석하였다. 그 결과, 폐양모/폴리프로필렌 복합재료의 인장 및 굴곡 특성 그리고 충격강도는 수산화나트륨(NaOH)을 이용한 알칼리처리와 3-glycidylpropylsilane(GPS)을 이용한 실란처리와 같은 처리매체에 크게 의존하였다. 실란처리를 한 폐양모섬유를 포함한 복합재료는 알칼리처리를 한 폐양모섬유를 포함한 것보다 더 우수한 기계적 특성과 충격저항성을 나타내었다. 복합재료 파단면은 특성 증가가 폐양모섬유와 폴리프로필렌 매트릭스 사이에 계면결합의 향상에 의한 것임을 정성적으로 뒷받침해주었다.

• The Journal of Advanced Prosthodontics
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• 제6권2호
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• pp.79-87
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• 2014

PURPOSE. The aim of this study was to determine the efficiency of Erbium, Chromium: Yttrium-Scandium-Gallium-Garnet laser in different output powers for removing permanent resin cement residues and therefore its influence on microshear bond strength compared to other cleaning methods. MATERIALS AND METHODS. 90 extracted human molars were sectioned in 1 mm thickness. Resin cement was applied to surface of sliced teeth. After the removal of initial cement, 6 test groups were prepared by various dentin surface treatment methods as follows: no treatment (Group 1), ethylene diamine tetra acetic acid application (Group 2), Endosolv R application (Group 3), 1.25 W Erbium, Chromium:Yttrium-Scandium-Gallium-Garnet laser irradiation (Group 4), 2 W Erbium, Chromium:Yttrium-Scandium-Gallium-Garnet laser irradiation (Group 5) and 3.5 W Erbium, Chromium:Yttrium-Scandium-Gallium-Garnet laser irradiation (Group 6). The topography and morphology of the treated dentin surfaces were investigated by scanning electron microscopy (n=2 for each group). Following the repetitive cementation, microshear bond strength between dentin and cement (n=26 in per group) were measured with universal testing machine and the data were analyzed by Kruskal Wallis H Test with Bonferroni correction (P<.05). Fracture patterns were investigated by light microscope. RESULTS. Mean microshear bond strength ${\pm}$ SD (MPa) for each group was $34.9{\pm}17.7$, $32.1{\pm}15.8$, $37.8{\pm}19.3$, $31.3{\pm}12.7$, $44.4{\pm}13.6$, $40.2{\pm}13.2$ respectively. Group 5 showed significantly difference from Group 1, Group 2 and Group 4. Also, Group 6 was found statistically different from Group 4. CONCLUSION. 2 W and 3.5 W Erbium, Chromium: Yttrium-Scandium-Gallium-Garnet laser application were found efficient in removing resin residues.

• The Journal of Advanced Prosthodontics
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• 제10권4호
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• pp.286-290
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• 2018

PURPOSE. Conventional resin-bonded fixed partial dentures (RBFPDs) are usually made with a two-retainer design. Unlike conventional RBFPDs, cantilever resin-bonded fixed partial dentures (Cantilever RBFPDs) are, for their part, made with a single-retainer design. The aim of this study was to compare the effect of tooth surface preparation on the bond strength of zirconia cantilever single-retainer RBFPDs. The objective is to evaluate the shear bond strength of these single-retainer RBFPDs bonded on 3 different amount of tooth surface preparation. MATERIALS AND METHODS. Thirty extracted bovine incisors were categorized to 3 groups (n=10), with different amounts of tooth surface preparations. Teeth were restored with single-retainer RBFPDs with different retainer surfaces: large retainer of $32mm^2$; medium retainer of $22mm^2$; no retainer and only a proximal connecting box of $12mm^2$. All RBFPDs were made of zirconia and were bonded using an adhesive system without adhesive capacity. Shear forces were applied to these restorations until debonding. RESULTS. Mean shear bond strength values for the groups I, II, and II were $2.39{\pm}0.53MPa$, $3.13{\pm}0.69MPa$, and $5.40{\pm}0.96MPa$, respectively. Statistical analyses were performed using a one-way ANOVA test with Bonferroni post-hoc test, at a significance level of 0.001. Failure modes were observed and showed a 100% adhesive fracture. CONCLUSION. It can be concluded that the preparation of large tooth surface preparation might be irrelevant. For zirconia single-retainer RBFPD, only the preparation of a proximal connecting box seems to be a reliable and minimally invasive approach. The differences are statistically significant.

• Composites Research
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• 제29권4호
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• pp.203-208
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• 2016

금속/고분자 샌드위치 복합재는 경량성과 제진, 방음 등의 다기능성의 측면에서 기존의 스틸 강판을 대체할 후보 중 하나로서 연구되고 있다. 금속/고분자 복합재의 활용하기 위해서는 접착력을 바탕으로 한 박리 거동 예측이 매우 중요한 요소이다. 본 연구에서는 응집요소를 사용하여 유한요소 해석을 통해 접착제를 사용한 고분자 테이프의 박리거동 해석을 수행하였다. 응집요소의 특성은 박리시험과 역학 관계로부터 도출한 파괴인성을 통해 정의하였고 이를 해석에 적용하였다. 스틸 강판에서 고분자 테이프를 박리하는 시험을 모사하였고, 해석결과와 시험결과를 비교하여 박리 거동 모사가 가능함을 확인하였다.