• Title/Summary/Keyword: finishing shrinkage

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Alkaline Hydrolysis of Polyester/Acetate Union Fabric (폴리에스테르/아세테이트 혼용직물의 알칼리 가수분해)

  • Ju, Young Min;Kim, Myung Kyoon;Ahn, Kyoung Ryoul;Lee, Jeong Min
    • Textile Coloration and Finishing
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    • v.8 no.4
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    • pp.42-51
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    • 1996
  • Alkaline hydrolysis to improve the hand of PET/acetate union fabric was studied in relation to skin saponification and retarding effect of salts on the alkaline hydrolysis of cellulose acetate fiber, accelerating effect of salts on the alkaline hydrolysis of PET fiber, and changes of total hand value(T.H.V) of PET/acetate union fabric treated with alkali/salt solution. It was found that the rate of saponification of acetate was delayed by the addition of salts such as LiCl, NaCl and CH$_{3}$COONa into NaOH solution below 10 minutes. The rate of shrinkage of acetate fabric treated with 5g/l NaOH solution at 9$0^{\circ}C$ and 60 minutes showed 20 % but it was decreased 8% by. the addition of 120g/l Concentration of inorganic salts. We could know that the rate of alkaline hydrolysis of filament yarn treated with alkali solution at 9$0^{\circ}C$ and 60 minutes was delayed about 3 % using 2,000T/M of hard twist yarn, especially acetate filament treated with alkali solution at 9$0^{\circ}C$ and 10 minutes was delayed about 10%. T.H.V. of PET/acetate union fabric was increased from 2.77 to 3.04~3.18 by the addition of salts into alkali solution.

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Mechanical Properties of Woven Fabrics Made from Thick & Thin Yarn (태세사(Thick & Thin Yarn)로 제작된 직물의 역학적 특성)

  • Shin Hyun-Sae;Kim Young-Sang;Son Jun-Sik
    • Textile Coloration and Finishing
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    • v.18 no.2 s.87
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    • pp.39-45
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    • 2006
  • The aim of this work is to develop sense-differentiated textiles using Thick-Thin polyester yarn(T-T yarn) with finer than 1 denier mono filament. The ITY(Interlace Textured Yarn) using T-T yarn with various over feed ratios of PET filament was manufactured with different shrinking percentage of core yarn and then the fabrics were woven on the same weaving 100m using ITY produced. The mechanical properties and the handles of the fabrics were examined with KES-FB system suggested by Kawabata. The shrinkage of ITY was increased with decreasing over feed ratio and increased with increasing heat treatment temperature of T-T yarn. The initial elasticity modulus of ITY was decreased with increasing over feed ratio and heat treatment temperature of T-T yarn. The tensile energy of fabrics was decreased with increasing of over feed ratio, but bending rigidity and shear rigidity of fabrics were increased with increasing of over feed ratio of PET filament. The results indicate that the fabric using T-T yarn with finer than I denier mono filament can be used for the purpose of sense-differentiated textile.

The Optimum Processing Conditions of ATY for PET Braiding for Automotive Hoses (자동차호스용 PET 브레이딩 직물의 최적 ATY 공정조건)

  • Kim, Seung-Jin;Choi, Woo-Hyuk;Kim, Sang-Ryong;Jo, Jin-Hwang;Moon, Chan
    • Textile Coloration and Finishing
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    • v.21 no.4
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    • pp.11-22
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    • 2009
  • This study surveys the optimum processing conditions of ATY for PET braiding for automotive hoses. For this purpose, high tenacity and low shrinkable PET filaments with three types of deniers are prepared. Twenty seven ATY specimens are manufactured with variation of feed speed and overfeed on the air jet texturing machine. The physical properties of various yam according to the ATY processing conditions are measured and analysed for deciding the optimum ATY processing condition. Two kinds of ATY filaments made under the optimum air texturing conditions are processed with variation of tpm, heat setting temperature and heat setting time on the 2-for-l twister and setting chamber, respectively. The optimum twisting and heat setting conditions are decided through analysis of the yam physical properties. Finally, the braiding fabric specimens are manufactured using conventional filament and newly developed filament made under optimum twisting and heat setting conditions. The bursting strengths of these braiding specimens are compared and discussed between two types of specimens.

Enhancement in the Thermal Stability of Microporous UHMWPE Membrane by LED-UV Crosslinking (LED-UV 가교에 의한 UHMWPE 미세다공막의 열 안정성 향상)

  • Jeong-Hwan Kim;Jinho Jang
    • Textile Coloration and Finishing
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    • v.35 no.4
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    • pp.231-238
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    • 2023
  • Microporous gel films of 29 m were prepared by the gel drawing of UHMWPE/soybean oil blend (4:6, w/w) up to 800%. The stretched films containing the optimal photoinitiator concentration, depending on the film thickness, was cross-linked under 365 nm LED-UV irradiation and the oil was extracted with n-hexane, resulting in a gel fraction of 95 % or more. With the formation of the cross-linked structure, the melt-down temperature and melt-down elongation increased by 16 ℃ and by 63% respectively. Also the thermal stability of the crosslinked UHMWPE was proved by the area shrinkage under the heat treatment decreased to 3.8 % compared to 17.4 % for the pristine film, and by the reductions in the combustion heat. The enhanced thermal stability of the crosslinked UHMWPE microporous membranes can be used for various industrial applications such as filters, electric vehicles and energy storage systems.

EFFECT OF $CEO_2$ ADDITION IN GLASS COMPOSITION ON THE STRENGTH OF ALUMINA-GLASS COMPOSITES (알루미나-유리 복합체용 글래스의 조성에서 $CeO_2$의 함량변화가 강도에 미치는 영향)

  • Lee, Hwa-Jin;Song, Kwang-Yeob;Kang, Jeong-Kil
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.5
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    • pp.595-605
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    • 2000
  • Dental ceramics have good aesthetics, biocompatibility, low thermal conductivity, abrasion resistance, and color stability. However poor resistance to fracture and shrinkage during firing process have been limiting factors in their use, particularly in multiunit ceramic restorations. A new method for making all-ceramic crowns that have high strength and low processing shrinkage has been developed and is referred to as the Vita In-Ceram method. This study was performed to investigate the effect of $CeO_2$ addition in borosilicate glasses on the strength of alumina-glass composites. Porous alumina compacts were prepared by slip casting and sintered at $1,100^{\circ}C$ for 2 hours. Dense composites were made by infiltration of molten glass into partially sintered alumina at $1,140^{\circ}C$ for 4 hours. Specimens were polished sequentially from #800 to #2000 diamond disk. and the final surface finishing on the tensile side was received an additional polishing sequence through $1{\mu}m$ diamond paste. Biaxial flexure test was conducted by using ball-on-three-ball method at a crosshead speed of 0.5mm/min. To examine the microstructural aspect of crack propagation in the alumina-glass composites, Vickers-produced indentation crack was made on the tensile surface at a load of 98.0 N and dwell time of 15 sec, and the radial crack patterns were examined by an optical microscope and a scanning electron microscope. The results obtained were summarized as follows; 1. The porosity rates of partially sintered alumina decreased with the rising of firing temperature. 2. The maximum biaxial flexure strength of 423.5MPa in alumina-glass composites was obtained with an addition of 3 mol% $CeO_2$ in glass composition and strength values showed the aspect of decrease with the increase of $CeO_2$ content. 3 The biaxial flexure strength values of alumina-glass composites were decreased with rising the firing temperature. 4. Observation of the fracture surfaces of alumina-glass composites indicated that the enhancement of strength in alumina-glass composites was due to the frictional or geometrical inter-locking of rough fracture surfaces and ligamentary bridging by intact islands of materials left behind the fracture front.

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Development of Shape refining process of VLM-ST Parts Using Noncontacting Hot Tool (비접촉식 열공구를 이용한 VLM-ST 제품의 미세 형상 가공 공정 개발에 관한 연구)

  • 김효찬;이상호;안동규;양동열
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.1
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    • pp.149-158
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    • 2004
  • In most RP processes, the inherent stair-stepped surfaces and shrinkage-induced warping of the parts require post processing such as surface finishing. To minimize such defects, VLH-ST, a newly developed RP process, employs a 3.9-mm thick expandable polystyrene (EPS) foam sheet and a hot wire to contour it to have slant linear-interpolated sides. The use of relatively thick sheets for layers, however, limits the process capability of constructing fine details, especially smaller than the layer thickness. This study is focused on the development of a post processing method fo fine details of VLM-ST parts. The post-processing tool was designed to meet all the requirements for the desirable post processing. It adopted a hot wire as a means of melting the EPS foam sheet. Various basic experiments on the post processing were carried out to obtain the optimal process conditions. The dominant process parameters such as the radiated heat input, the tool speed, and the gap between the tool tip and the foam sheet (tool height) were considered in the experiments. The effectiveness of the developed post-processing method fo forming or engraving fine details on the VLM-ST parts has been thus demonstrated. The experiments on engraving several sets of letters, such as CANESM, 인간, and 한국과학기술원, on the EPS foam sheet were carried out. In addition, a flowery shape was engraved on a three-dimensionally curved surface of a pottery-shape VLM-ST part.

The Effect of Drawing and Annealing Condition on the Fine Structure of PET Film (연신 및 열처리 조건이 PET film의 미세구조에 미치는 영향)

  • Park, Jong-Bum;Choi, Suk-Chui;Cho, Hyun-Hok
    • Textile Coloration and Finishing
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    • v.3 no.1
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    • pp.8-16
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    • 1991
  • In order to investigate the fine structure of PET films, PET films were stretchd at various draw ratios (2, 3, 4, 5) below $T_g$ ($72^{\circ}C$) and then annealed at various temperatures (125, 150, 175, $200^{\circ}C$) under free-annealed (FA) and taut-annealed (TA) conditions. Such changes as thermal shrinkage, crystallinity, crystallite size, dynamic viscoelasticity and thermal behaviour were measured in relation to the draw ratio and annealing condition.The following results were obtained. 1. Thermal shirinkage increased with increasing annealing temperature and draw ratio, but decreased in case of draw ratio 4 (draw ratio 3 at $200^{\circ}C$) and above it. 2. The degree of crystallinity of FA samples were higher than those of TA samples. 3. Tan 5 of TA samples were less than those of FA samples, and storage moduli (E') and loss moduli (E") of FA samples were less than those of TA samples; moreover, maximum tan '||'&'||' temperature of FA samples were shifted toward higher temperature than those of TA samples. 4. The melting endotherm ($T_m$) and heat of fusion $(\DeltaH)$ of the PET film increased with the draw ratio and annealing temperature; in addition, premelting endotherm ($T_m$) and heat of fusion $(\DeltaH)$ of the local crystallization in the FA samples were larger than those of TA samples. 5. The X-ray diffraction pattern displayed sharp peaks gradually with the draw ratio and annealing temperature. 6. Crystallite sizes of FA samples were larger than those of TA samples.

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A Study on the Formulation Selection of Self Leveling Floor Mortar with Fluidity and Early Strength Improvements (유동성 및 조기강도 확보가 가능한 자기수평 모르타르 배합선정에 관한 연구)

  • Ryu, Hwa-Sung;Kim, Deuck-Mo;Kwon, Seung-Jun;Park, Won-Jun;Shin, Sang-Heon
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.1
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    • pp.41-49
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    • 2018
  • The purpose of this study is to develop a floor mortar construction technique which has high strength and inherent mechanical properties and does not cause cracks due to shrinkage after construction. It has been demonstrated that compressive strength, bending strength, flow with floor mortar, and crack reduction performance. As a result, it was confirmed that the developed floor mortar had the same or better performance comparing with the existing foreign products. The results of this experiment can be used as a validation material for high performance and high flowable mortar construction technology with excellent material performance, economical efficiency and construction ability by securing the required performance as floor mortar and selecting the optimal formulation.

Eco-friendly Leather Dyeing Using Biomass Wastes(III): Imparting Functionality by Combination Dyeing with Marigold (Tagetes erecta L.) and Hinoki Cypress(Chamaecyparis obtusa) Leave Extracts (생물자원 폐기물을 활용한 친환경 가죽염색(III): 매리골드와 편백나무 잎 추출물의 복합염색에 의한 기능성 부여)

  • Lee, Geonhee;Shin, Younsook
    • Textile Coloration and Finishing
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    • v.31 no.1
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    • pp.1-13
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    • 2019
  • In this study, eco-friendly functional leather was developed by recycling wastes such as eel skin, marigold(Tagetas erecta l.), hinoki cypress(Chamaecyparis obtusa). The hot water extracts of marigold and hinoki cypress leaves were freeze-dried at $-80^{\circ}C$ to prepare colorant powder. The dyeing of eel leather with marigold was carried out to investigate the effects of dyeing conditions, mordanting on dye uptake, color, morphological change, and color fastness. Considering shrinkage of eel leather caused by dyeing, the optimum dyeing conditions were $60^{\circ}C$ of dyeing temperature and 60 min of dyeing time at 1:100 of bath ratio, and color of the dyed eel leather was Y to YR Munsell series. In order to prevent the degradation of leather from microbe, we conducted combination dyeing with marigold and hinoki cypress leave colorants. In this case, the combination dyed eel leathers showed excellent antimicrobial activity with above 99% bacterial reduction rate against S. aurieus and K. pneumoniae. It was confirmed that all of the dyed eel leathers were sufficient to meet the Korean Standard for color fastness of leather products. It can be applied practically for the development of eco-friendly functional leather by utilizing some useful active components extracted from plant resources and by recycling food wastes.

Consumer recognition and mechanical property comparison of wetsuit material for diving (다이빙용 웨트수트(wetsuit) 소재에 대한 소비자 인식조사와 물성 비교)

  • Sang, Jeong Seon;Oh, Kyung Wha
    • Journal of the Korea Fashion and Costume Design Association
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    • v.20 no.4
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    • pp.163-174
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    • 2018
  • Consumer and property evaluation of wetsuit materials were conducted to obtain useful data for developing competitive products that meet consumer expectations and improving industrial competitiveness. Data were collected through online surveys of 213 domestic consumers who have experienced wearing wetsuit among marine leisure activities. Five types of commercial wet suit materials by brand and four types of commercial wet suit materials with the same quality by thickness were collected. Then, their physical properties, salt water resistance and thermal insulation rate were evaluated and compared. As a result, the most commonly used wetsuit material is 3 to 5 mm thick, and the basic jersey material is bonded on both sides. As a processing for imparting functionality, processing for improving warmth and reducing surface resistance are most frequently used. Consumers often feel uncomfortable when wearing a wetsuit, such as wearing comfort, weight, ease of movement, stretchability, and clothing pressure, which are different from those of casual wear. Also, mechanical strength and warmth were considered to be the most important criteria for selection of wetsuit material for purchase or rental. The mechanical properties of brand A and B were better than those of brand C, D, and E. Resilience and thermal shrinkage were better in brand C, D, and E. On the other hand, there was no significant difference in the physical properties due to the difference in thickness of the material at the same quality. Also, it was found that the thicker the material, the more stable it is in the heat. Brand A and B had superior salt water resistance than brand C, D, and E. In the thermal insulation test, brand A and B showed better insulation characteristics than brand C, D, and E, but the types of bonded fabric and surface finishing of materials were thought to have affected. In comparison of the thickness, the thicker the materials, the better the salt resistance and the thermal insulation.