• 제목/요약/키워드: finer grain size

검색결과 139건 처리시간 0.026초

급속응고한 AZ91합금의 미세조직 및 기계적 특성에 미치는 Y첨가의 영향 (The Effect of Y Addition on the Microstructure and Mechanical Property of Rapidly Solidified AZ91 Alloy)

  • 최재영;박훈모;남태운
    • 한국주조공학회지
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    • 제20권6호
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    • pp.386-394
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    • 2000
  • In the present study, the effect of yttrium addition on the microstructure and mechanical property of rapidly solidified AZ91 alloy by melt spinning process is estimated. As yttrium was added, the microstructure of RS ribbons and extrudates became finer than those of AZ91, and RE related phases $(Al_2RE)$ were formed. In the case of the addition of 3wt%Y, the microstructure of extrude showed the finest grain size. At room temperature, the AZ91 + 3wt%Y alloy showed the highest tensile strength, 352 MPA due to precipitation of ${\beta}(Mg_{17}Al_{12})$ phase and $Al_2RE$ phase. At the elevated temperature, the mechanical property of AZ91 + 3wt%Y alloy was higher than those of other Mg alloys. The reasons were that $Al_2Y$ compound was thermally stable and suppressed the grain growth. In contrast with $Al_2Y$ compounds, ${\beta}$ phase was thermally unstable and could not suppress the grain growth at the elevated temperature. Therefore, $Al_2Y$ phase contributed to improve the thermal stability of RS AZ91 alloy.

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강소성변형된 미세립 AM60 마그네슘 합금의 피로거동 (Fatigue Behavior of Fine Grained AM60 Magnesium Alloy Produced by Severe Plastic Deformation)

  • 유인동;이만석;김호경
    • 한국안전학회지
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    • 제27권3호
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    • pp.15-19
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    • 2012
  • The fatigue behavior of AM60 magnesium alloy produced by equal channel angular pressing(ECAP) process was investigated through fatigue lifetime and fatigue crack propagation rate tests. The grain structure of the material was refined from 19.2 ${\mu}m$ to 2.3 ${\mu}m$ after 6 passes of ECAP at 493 K. The yield strength(YS) and ultimate tensile strength (UTS) increase after two passes but decrease with further pressing, although the grain size becomes finer with increasing pass number. The softening effect due to texture anisotropy overwhelmed the strengthening effect due to grain refinement after 2 passes. A large enhancement in fatigue strength was achieved after two ECAP passes. The current finding suggests that two passed material is better than the multi-passed material in view of the static strength and fatigue performance.

Fe계 나노결정 분말코아의 연자성특성에 미치는 입도제어 및 바인더 첨가의 영향 (Effect of Grain Size Control and Binder Additions on the Soft Magnetic Properties of Fe-based Nanocrystalline Powder Cores)

  • 조은경;조현정;권훈태;조은민;류혁현;손근용;박원욱
    • 한국분말재료학회지
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    • 제13권4호
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    • pp.256-262
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    • 2006
  • The amorphous $Fe_{73}Si_{16}B_7Nb_3Cu_1$ alloy strip was pulverized to get a flake-shaped powder after annealing at $425^{\circ}C$ for 90 min and subsequently ground to obtain finer flake-shaped powder by using a ball mill. The powder was mixed with polyimide-based binder of $0.5{\sim}3wt%$, and then the mixture was cold compacted to make a toroidal powder core. After crystallization treatment for 1 hour at $380{\sim}600^{\circ}C$, the powder was transformed from amorphous to nanocrystalline with the grain size of $10{\sim}15nm$. Soft magnetic characteristics of the powder core was optimized at $550{\sim}600^{\circ}C$ with the insulating binder of 3wt%. As a result, the powder core showed the outstanding magnetic properties in terms of core loss and permeability, which were originated from the optimization of the grain size and distribution of the insulating binder.

목포-해남 연안 조간대 퇴적물중 유기물 및 미량금속 분포 특성 (Distributions of Organic Matter and Trace Metals in Intertidal Surface Sediment from the Mokpo-Haenam Coast)

  • 황동운;김평중;정래홍;윤상필
    • 한국수산과학회지
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    • 제46권4호
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    • pp.454-466
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    • 2013
  • To evaluate the organic matter and trace metal pollution in intertidal sediment of the coastal zone, various geochemical parameters (grain size, ignition loss [IL], chemical oxygen demand [COD], acid volatile sulfide [AVS], and metals [Al, Fe, Cu, Pb, Zn, Cd, Cr, Mn, Hg, and As]) were measured for the intertidal surface sediment of the mainland and islands between Mokpo and Haenam in the southwestern coast of Korea. The surface sediments consist mainly of finer sediments, such as mud and silt. The concentrations of IL, COD, and trace metals in intertidal sediment were relatively high in the shoreline of the mainland than in that of islands and those in some stations exceeded the sediment quality guidelines (SQGs). Moreover, the concentrations of IL, COD, and trace metals (except As) in sediment showed relatively good positive correlations with mean grain size, indicating that the concentrations of organic matter and trace metals in intertidal sediment of the study region are dependent on grain size of sediment. Pollution evaluation for trace metals using geochemical assessment techniques, such as enrichment factor, geoaccumulation index, and SQGs, suggested that the intertidal sediments in the study region show light pollution with Cr and moderate pollution with As. More extensive interdisciplinary studies are required to determine the potential causes of As pollution in intertidal sediment.

Inconel 706의 열간단조 공정 중 재가열과 변형양에 따른 결정립 미세화에 대한 분석 (Analysis of Microstructural Refinement for Inconel 706 during Hot Forging Process through Reheating and Strain)

  • 성상규;강현준;이영선;이상용;이의종;제환일;신정호;윤은유
    • 소성∙가공
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    • 제32권5호
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    • pp.239-246
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    • 2023
  • To reduce the forming load due to the temperature drop, during the hot forging process, a reheating hot forging process design is required that to repeat heating and forging. However, if the critical strain required for recrystallization is not induced during forging and grain growth becomes dominant due to the reduction in dislocation density due to repeated heating, the mechanical properties may deteriorate. Therefore, in this study, Inconel 706 alloy was applied, and the grain refinement behavior was comparatively analyzed according to the number of reheating times and effective strain during reheating hot forging process. Reheating was carried out with a total compression rate of 40% up to 4 times. The Inconel 706 compression test specimens heated once showed finer grains as the effective strain increased due to the dynamic recrystallization phenomenon. However, as the number of heating increases, grain refinement was observed even in a low effective strain distribution of 0.43 due to static recrystallization during reheating. Moreover, grain growth occurs at a relatively low effective strain of 0.43 when the number of reheating is four or more. Therefore, it was effective to apply an effective strain of 0.43 or more during hot forging to Inconel 706 in order to induce crystallization through grain refinement and improve the properties of forged products. In addition, we could notice that up to three reheating times condition was appropriate to prevent grain growth and maintain fine grain size.

조립토 입도분포곡선의 프랙탈차원을 이용한 투수계수의 예측 (Estimation of Permeability Coefficient Using Fractal Dimension of Particle Size Distribution Curve in Granular Soils)

  • 박재성;장병욱;손영환;김성필
    • 한국농공학회논문집
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    • 제48권4호
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    • pp.41-49
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    • 2006
  • Since particle size distribution curves are useful to estimate permeability of soil, many formulae for permeability coefficient (k) have been published using the parameter from the curves and factors, such as grain size, particle shape and void ratio of soils. However, the parameters such as $C_c,\;C_u$ and $D_n$ derived from only some discrete points on the curve are insufficient to represent the whole gradation. In this paper fractal dimension which is quite new concept and known to be able to represent the entire curve of particle size distribution is employed for the parameters. An empirical formula of permeability coefficient has been developed with fractal dimension and percent of finer than 0.075 mm. The formula developed from this study has confirmed its effectiveness by a series of laboratory tests and comparison to other published formulae. It is found that permeability coefficient is proportional to fractal dimension and inversely proportional to percent of fines.

중기 플라이스토세 전이기 전후 북태평양 중앙 해역 퇴적물에 기록된 풍성 퇴적물 입자 퇴적 양상 변화 복원 (Reconstruction of Changes in Eolian Particle Deposition Across the Mid-Pleistocene Transition in the Central Part of the North Pacific)

  • 이소정;서인아;형기성
    • Ocean and Polar Research
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    • 제41권4호
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    • pp.275-288
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    • 2019
  • We investigated flux, grain size distribution, Nd-Sr isotope composition, mineral composition, and trace metal composition (REEs and Sc) of inorganic silicate fraction (ISF, mainly Asian dust with an unrestricted amount of volcanic materials) deposited during 600~1000 ka across the Mid-Pleistocene Transition at core NPGP 1401-2A (32°01'N, 178°59'E, 5205m) taken from the central part of the North Pacific. Our results reveal about a 2-fold increase in ISF flux after 800 ka, which is associated with an increase in La/Sc and a decrease in mean grain size. Asian dusts are finer than volcanic materials and La/Sc increases with the enhanced contribution of Asian dusts. Thus, increased flux after 800 ka can be explained by the increased contribution of Asian dusts relative to volcanic materials, likely due to an intensified Westerly Jet (WJ) and the drying of the Asian continent after the MPT. Mean grain size of ISF varies systematically in relation to glacial-interglacial cycles with a decrease during glacial stages, which is consistent with the previous results in the study area. Such a cyclical pattern is also attributed to the increase in the relative contribution of Asian dusts over volcanic components in glacial stages due to intensified WJ and drying of the Asian continent. Thus, it can be concluded that climate changes that had occurred across the MPT were similar to those of interglacial to glacial transitions at least in terms of the dust budget. Different from the Shatsky Rise, however, compositional changes associated with glacial-interglacial mean grain size fluctuations are not observed in Nd-Sr isotope ratios and trace element composition in our study of the Hess Rise. This may be attributed to the location of the study site far (> 4,000 km) from the volcanic sources. The volcanic component at the study site comprises less than 10% and varies within 3% over glacial-interglacial cycles. Such a small variation was not enough to imprint geochemical signals.

표층퇴적물 분석을 통한 동계 안면도 바람아래해수욕장 주변의 퇴적환경 변화특성 (Characteristics Variation of the Sedimentary Environment in Winter Season around the Baramarae Beach of Anmyeondo Using Surface Sediment Analysis)

  • 장동호;김장수;박노욱
    • 한국지형학회지
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    • 제17권1호
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    • pp.15-27
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    • 2010
  • 이 연구는 바람아래해수욕장 주변의 퇴적물 입도조성을 시·공간적으로 분석하여 퇴적환경 변화특성을 고찰하고자 하였다. 연구결과, 2009년 겨울철 표층퇴적물은 크게 자갈, 모래, 역질사, 역니질사, 니질사, 실트질사, 모래질실트 등의 7개 퇴적상으로 구분되었다. 평균입도를 시계열 분석(2002~2009)한 결과, 간석지 퇴적물은 평균 입도가 세립해지고, 분급은 불량해졌다. 그러나 해빈지역은 동일시기에 퇴적물의 입도가 조립화 되었고 분급이 양호해졌다. 이러한 결과는 해빈과 간석지의 퇴적환경 변화가 서로 다른 경향성을 가지고 있기 때문이다. 즉, 할미섬을 중심으로 남서쪽 해빈지역은 외해로 열려 있어 상대적으로 고에너지 환경으로 세립질 퇴적물이 제거되는 환경에서 퇴적된 결과이다. 간석지 중 가장 안쪽의 만입지의 세립화는 왕복성 조류에 의해서 유입된 퇴적물이 정조시에 퇴적되었거나 지형적인 영향에 의한 에너지 감소로 퇴적된 것으로 판단된다. 남서쪽 외해 쪽의 간석지들의 세립화 원인은 규모가 큰 섬옷섬이 외해로부터 유입되는 파랑을 막아주어 상대적으로 저에너지 환경 하에 놓이면서 조석의 영향을 받으면서 세립질 퇴적물질들이 지속적으로 퇴적된 결과로 판단된다.

퇴적물 이동경로 식별을 위한 입도경향 분석법의 가능성과 한계 (Grain-Size Trend Analysis for Identifying Net Sediment Transport Pathways: Potentials and Limitations)

  • 김성환;류호상;유근배
    • 대한지리학회지
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    • 제42권4호
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    • pp.469-487
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    • 2007
  • 입도경향 분석법은 파이척도로 표현된 평균입도, 분급, 왜도 등 퇴적물 입도조직변수가 퇴적물의 이동경로를 따라 특정한 경향을 보이는 성질을 이용한 퇴적물 이동경로 식별 방법론이다. 적용이 간편하고 저렴하여 지형학 연구에 널리 응용될 수 있는 가능성을 지니고 있으나 방법론상의 한계도 몇 가지 측면에서 지적되고 있어 주의가 필요하다. 이 연구는 McLaren과 Bowles의 1차원 경로분석법, Gao와 Collins, Le Roux의 2차원 이동벡터법 등 현재까지 정립된 입도경향 분석의 대표적인 세 가지 기법을 비교 평가하여 적절한 활용법을 도출하고, 입도경향 분석의 추후 연구과제를 제안한 것이다. McLaren-Bowles의 1차원 경로분석법은 연구자의 현장경험을 분석에 효과적으로 결합시킬 수 있고 X-분포를 통해 퇴적환경에 대한 해석을 제공해주며 장기적인 퇴적물 순이동 패턴을 파악하는데 효과적이나 연구자의 주관적 해석에 의존해야 한다는 점, 식별할 수 있는 시간 해상도가 낮다는 점등이 단점이다. Gao-Collins의 2차원 이동벡터법은 명확한 절차, 2차원적인 시각화, 세밀한 시간 해상도 등이 장점이지만, 임계거리 선정, 잡벡터 제거과정 등이 문제를 유발할 수 있으므로 분석 시 주의를 요한다. 셋째, Le Roux의 2차원 이동벡터법은 확장된 경험규칙과 조직변수 간의 구배를 고려하고 시간해상도도 세밀하지만, 분석개념이 모호하고 복잡하다. 입도경향 분석은 현장에 대한 연구자의 이해도, 조사하고자 하는 퇴적물 순이동 패턴의 시간적 스케일, 초점을 맞추고자 하는 정보 등에 따라 적절한 기법을 선택하고, 거기에 부합되는 시료채취방안을 기획하는 것이 중요하다. 또한 입도경향 분석이 지형학 연구에 기여하기 위해서는 시료채취 깊이, 교란층의 두께 등 시료채취 과정의 요소들과 퇴적물 순이동 패턴이 지시하는 시간스케일 간의 관계가 체계적으로 규명되어야 한다고 판단된다.

분사주조한 입자강화 알루미늄 복합재료의 미세조직 특성 (Characteristics in Microstructure of Particle Reinforced Al Matrix Composites Fabricated by Spray-Cast Forming Process)

  • 박종성;이인우;김명호
    • 한국주조공학회지
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    • 제14권6호
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    • pp.530-540
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    • 1994
  • Aluminium-silicon alloy(JIS AC8A) matrix composites reinforced with SiC particles were fabricated by spray-cast forming process, and the microstructure of powders and preforms produced were studied by using an optical and scanning electron microscopy. SiC particles were co-sprayed by mixed phase injection method during the spray casting process. Most of the composite powders formed by this mixed phase injection method exhibit morphology of particle-embedded type, and some exhibits the morphology of particle attached type due to additional attachment of the SiC particles on the surface of the powders in flight. The preforms deposited were resulted in dispersed type microstructure. The pre-solidified droplets and the deposited preform of SiC-reinforced aluminium alloy exhibit finer equiaxed grain size than that of unreinforced aluminium alloy. Eutectic silicons of granular type are crystallized at the corner of the aluminum grains in the preforms deposited, and some SiC particles seem to act as nucleation sites for primary/eutectic silicon during solidification. Such primary/eutectic silicons seem to retard grain growth during the continued spray casting process. It is envisaged from the microstructural observations for the deposited preform that the resultant distribution of SiC injected particles in the Al-Si microsturcture is affected by the amount of liquid phase in the top part of the preform and by the solidification rate of the preform deposited.

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