• Title/Summary/Keyword: fibrous phase

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Corrosion Resistance of Super Duplex Stainless Steel (수퍼 2상 스테인리스강의 부식 저항성에 관한 연구)

  • 강흥주;남기우;안석환;강창룡;도재윤;박인덕
    • Journal of Ocean Engineering and Technology
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    • v.17 no.2
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    • pp.40-46
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    • 2003
  • The corrosion resistance of super duplex stainless steel on both its fibrous and dispersed phase was investigated. These structures consist of various volume fraction and distribution of austenite structure, which were obtained by changing the heat treatment temperature and cycle. The fibrous phase had higher austenite volume fraction than that of the dispersed phase at the same temperature. Corrosion resistance of super duplex stainless steel was evaluated through an immersion test and an impingement test, using 35% HCI and sea water, respectively. Super duplex stainless steel was compared with STS316L and STS304. The corrosion resistance of super duplex stainless steel was superior to ST316L and STS304. The dispersed phase of super duplex stainless steel was more stabilized than the fibrous phase in corrosion. The magnitude of corrosion rate was in order STS304, STS316L, fibrous phase of super duplex stainless steel and dispersed phase of super duplex stainless steel.

Preparation of Titanium Carbide Fiber-Reinforced Alumina Ceramic Matrix Composites by Self-Propagating High-Temperature Synthesis

  • Yun, Jondo;Bang, Hwancheol
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.171-175
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    • 1998
  • $Al_2O_3$-TiC composites were prepared from aluminum, titanium oxide, and carbon fibers by self-propagating high-temperature synthesis(SHS). After the SHS reaction, the TiC phase in the sample was found either fibrous or non-fibrous shape. The fraction of the fibrous TiC phase varied with the amount of $Al_2O_3$ diluent addition. The optimum amount of diluent to make fibrous carbide was determined to be 30%. The fibers were hollow inside and made of multiple grains with a composition of titanium carbide. The hollow fiber formation mechanism was suggested and discussed. The synthesized powders were consolidated to dense composites by hot pressing at $1750^{\circ}C$ under 30 MPa.

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Microstructures and Fracture Characteristic of Pressureless-Sintered DyNbO4 body (상압소경에 의해 제조된 DyNbO4 소결체의 미세조직과 파괴특성)

  • 김기만;안종관;이병택
    • Journal of Powder Materials
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    • v.9 no.3
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    • pp.148-152
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    • 2002
  • The microstructures and indentation fracture of pressureless-sintered $DyNbO_4$ crystalline were investigated as a basic study for the application of weak phase of fibrous monolithic composites. They were comprised with many lamella twins as well as micro-cracks at the grain boundaries. The hardness at room temperature was remarkably low value(575 Hv) due to the low relative density and existence of microcracks at grain boundaries. The main fracture mode was a typical intergranular fracture, and showed remarkable micro-cracking effect. The heavy plastic deformation was observed around the site of indentation. In addition, the $DyNbO_4$ was expected to apply as a weak phase in the fibrous monolithic composites because of the low hardness and easily plastic deformation that could be led the preferable pulled-out and microcracking toughening under the failure.

Mechanical Characteristics and Fatigue Crack Propagation of Super Duplex Stainless Steel by Distribution of Austenite (오스테나이트 분포에 따른 수퍼 2상 스테인리스강의 기계적 특성과 피로균열 진전거동)

  • Do, J.Y.;Lee, S.K.;Ahn, S.H.;Nam, K.W.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.4
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    • pp.205-211
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    • 2001
  • The characteristics of super duplex stainless steel were investigated on its fibrous structure and dispersed structure. These structures consist of various volume fractions and distributions of the austenite phase that were obtained by changing the heat treatment temperature and cycle. The fibrous structure had higher austenite volume fraction than dispersed structure on the same temperature. As the austenite volume fraction increased in both structures, tensile strength and elongation increased, but hardness decreased. Fatigue life of fibrous structure parallel to rolling direction was shorter than that of perpendicular to rolling direction. Fatigue life of dispersed structure was longer than parallel fibrous structure, and shorter than perpendicular fibrous structure. Fatigue crack propagation rate of fibrous structure was faster than that of dispersed structure.

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Microstructure Control of Fibrous Monolithic Al2O3-ZrO2 Composites (섬유단상 Al2O3-ZrO2 세라믹 복합재료의 미세조직제어)

  • Kim, Ki-Hyun;Kim, Taek-Soo;Lee, Byong-Taek
    • Korean Journal of Materials Research
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    • v.13 no.4
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    • pp.213-218
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    • 2003
  • Fibrous monolithic control of$ Al_2$$O_3$ -$ZrO_2$composite was investigated by multi-pass extrusion process. To obtain sound $Al_2$$O_3$-X $O_2$sintered bodies, burning out and sintering process were carefully carried out. The sintered bodies showed continuous, fibrous monolithic microstructure without any swelling. Many microcracks were observed at the $Al_2$$O_3$-$ZrO_2$interfaces due to the mismatching of thermal expansion coefficient between $Al_2$$O_3$ and $ZrO_2$phase. Most of m- $ZrO_2$grains included twin defects such as (001), (010) and (011) type to accommodate the phase transformation induced stress.

Fabrication of gelatin-amorphous CaP nano fibrous mat forusing as fast bone healing material

  • Sarkar, Swapan Kumar;Song, Ho-Yeon;Lee, Byong-Taek
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.40.2-40.2
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    • 2009
  • Using the favorable resorption behavior of amorphous Calcium phosphate (CaP) we fabricated a gelatin basednano fibrous mat by electrospinning for using as a fast healing patch for minorbone defects. Bone is predominantly formed by an inorganic phase of nano-crystalline HAp materials and nano fibrous protein material of collagen. The osteoblast cells, which are the bone formation cells and are key to the new bone formation, receive these materials to form new bone. Taking these considerations we make a new nano fibrous mat of amorphous CaP and gelatin, which is derived from collagen itself. A polymer carrier of poly caprolactone(PCL) was used in the system to stabilize the materials in biological condition. The electrospinning conditions were optimized for smooth mat without any droplet formation. The fabricated mat was characterized for its morphologyby SEM. Mechanical properties like tensile strength was evaluated. To investigate the bio-compatibility we performed the MTT assay and investigated its resorption behavior and apatite formation behavior by SBF immersion.

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Consideration of Analysis Method of Asbestos and Existing Condition for Fibrous Materials in Domestic Air (국내 공기 중 섬유상 물질의 존재실태와 석면의 분석방법에 대한 고찰)

  • Hwang, Jinyeon;Oh, Jiho;Lee, Hyomin;Lee, Jinhyun;Son, Byeongseo
    • Journal of the Mineralogical Society of Korea
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    • v.28 no.2
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    • pp.165-171
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    • 2015
  • Dust samples collected from air in metropolitan areas of Busan and Ulsan were analyzed by phase contrast microscopy, phase contrast dispersion microscopy and SEM. Asbestos concentration in dust samples was lower than detection limit. Many fibrous materials were observed in dust samples, but most of them were organic fibers. Inorganic fibers such as rock fiber, ceramic fiber and gypsum were contained in the samples and non-fibrous minerals such as quartz, calcite and feldspar were also occasionally observed. Domestic law requires that asbestos in air dust is mainly analyzed by phase contrast microscopy. From this study, however, precise analysis of asbestos was almost impossible by this method only. As indicated in JIS method of Japan, therefore, count and identification of asbestos were more efficient by dispersion staining method after removing organic materials in samples by low temperature incinerator.

Algorithm Development for Infiltration Control in Component Fabrication Process of Metal Matrix Composites and Their Evaluation (금속기복합재료의 부품 제조공정에 관한 함침제어알고리즘 개발 및 평가)

  • Kang, Chung-Gil;Yun, Kung-Sik
    • Journal of Korea Foundry Society
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    • v.16 no.6
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    • pp.523-536
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    • 1996
  • This paper relates to fabrication processing analysis of metal matrix composites by the injection of liquid metal into a fibrous preforms. One dimensional heat transfer analysis during squeeze infiltration process of aluminum base composites has been studied. An analysis method was investigated for the temperature distribution, infiltration velocity and melt infiltration characteristics with the commercial preform with short fiber array. When molten metal is infiltrated in a fibrous preform with random orientation, phase transformation will be occurred in a region such as molten metal, solidified region, preform region and infiltration composites region. a mathematical modelling for a solidification phenomena in fabrication process of metal matrix composites using a squeeze infiltration technique was investigated by the basic relations for liquid metal into a fibrous preform. The temperature distribution of theoretical results was compared with experimental data.

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A Study on the Chromatographic Separation of Proteins Using Fibrous Beds(I) -Adsorbent Fiber Manufactures and Data Handling- (섬유층을 이용한 단백질의 크로마토그래피적 분리에 관한 연구(I) -흡착성 섬유제조 및 자료처리-)

  • 박돈희;박주정
    • KSBB Journal
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    • v.9 no.2
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    • pp.98-103
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    • 1994
  • A bed configuration wherein sheets of modified fibrous polyethylene are potted within a Millipore Filter Cartridge matrix has been developed. Polyethylene fibers form sturdy beds but the native hydrophobicity and inertness of polyethylene have precluded their use in protein chromatography The polyethylene fibers used in this system were modified by plasma oxidation and further derivatization. The resulting fibers are hydrophilic, bind protein reversibly and serve as an anion-exchange stationary phase. Separation of Bovine Serum Albumin on this bed, as well as results of basic studies on capacity and reversibility of binding within a fibrous bed and experimental data handling system are shown.

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The Synthesis of Long Fibrous Potassium Tetratitanate by the Calcination Process and Phase Transformation (소성법에 의한 4티탄산칼륨 장섬유의 합성 및 상전이)

  • Lee, Chul-Tae;Lee, Jin-Sik;Kim, Hyun-Joong
    • Applied Chemistry for Engineering
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    • v.7 no.3
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    • pp.580-587
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    • 1996
  • Synthesis of long fibrous $K_2Ti_4O_9$ was attempted to find a method to produce long fibrous $K_2Ti_6O_{13}$ and other derivatives and also phase transformation of $K_2Ti_4O_9$ synthesized was investigated. Long fibrous $K_2Ti_4O_9$ was succesively synthesized by the calcination reaction under the following reaction conditions ; reaction temperature of $1050^{\circ}C$, $TiO_2$ mole ratio to $K_2CO_3$ of 2.8 and reaction time of 3hrs, and scattering of calcined products for 10hrs with hot boiling water. $K_2Ti_4O_9$ showed lower structural stability under heat treatment and the structure of $K_2Ti_4O_9$ was converted to $K_2Ti_6O_{13}$ under heating temperature of over $250^{\circ}C$.

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