• Title/Summary/Keyword: fiber surface treatment

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Effect of Surface Properties on Adhesive Strength of Joint of Glass Fiber/Polyester Composite Panels (유리섬유/폴리에스테르 복합재료 패널 접합부의 접착강도에 관한 표면성질의 효과)

  • Nhut, Pham Thanh;Yum, Young Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.12
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    • pp.1591-1597
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    • 2012
  • Adherend samples were made from unsaturated polyester and woven and mat glass fibers by the hand layup and vacuum methods. The mechanical properties of the adhesive, composite adherends, and terminal-joint and secondary-joint specimens were determined experimentally. Combinations of the experiment results and the bonding theory were used in this study. The maximum and average shear stresses were calculated based on the maximum tensile force and geometry parameters of the joint specimens. The results of the maximum and average shear stresses were compared and evaluated for six joints. The results showed that the grinding and grind/acetone joint had the highest strength among three types of terminal-joints. Similarly, the mat-mat and mat-woven joints had the highest strength among three types of secondary-joints with the same value. Conversely, no treatment and woven-woven bonding had very low strength. In each case, failure occurred always at two ends and then moved toward the middle area of the overlap length.

An Addition Effect of Amine and Cethyl Trimethyl Ammonium Bromide on Alkali-treatment of Polyester (폴리에스테르직물의 수산화나트륨 처리시 아민과 CTAB의 첨가효과)

  • Lee Jung Soon;Ryu Hyo Seon
    • Journal of the Korean Society of Clothing and Textiles
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    • v.16 no.3 s.43
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    • pp.335-344
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    • 1992
  • This study was conducted to investigate the influence of addition of cetyl trimethyl ammo­nium bromide (CTAB), and amine [ethylamine (EA) or ethylene diamine (EDA)] to aqueous sodium hydroxide (NaOH) solution on polyester alkaline hydrolysis, The experimental vari­ables such as CTAB concentration, EA or EDA concentration, NaOH concentration, tempera­ture and time were compared, and the changes in physical and chemical properties of alkaline­hydrolyzed PET fabrics depending on their treated conditions were measured, The results are as follows: 1. By adding CTAB and amine in aqueous NaOH solution, increasing effect on weight loss of PET fabrics was obtained in simultaneous addition of CTAB and EDA, but not in CTAB and EA. 2. By adding CTAB & EDA simultaneously, increasing effect on weight loss was obtained regardless of EDA concentration, time and temperature, and it was more effective at lower NaOH concentration. :l. The increase of void space (or irregularly grooved surface), of softness, of wickability, of dyeability on PET fabric, and the decrease of tensile strength, of molecular weight were observed according to the weight loss on the PET fabrics. These changes were equal to all alkaline-hydrolyzed PET fabrics regardless of addition of CTAB and amine. l. There was little changes on crystallinity, thermal behavior when PET fiber was treated with ,aqueous NaOH solution with CTAB and EDA. These results supported that increasing effect on weight loss take place without inducing of fine structural change of PET fibers.

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Delignification Effect on Properties of Lignocellulose Nanofibers from Korean White Pine and Their Nanopapers (잣나무 유래 리그노셀룰로오스 나노섬유 및 나노종이 특성에 미치는 탈리그닌의 영향)

  • Jang, Jae-Hyuk;Lee, Seung-Hwan;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.1
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    • pp.9-16
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    • 2015
  • This study was carried out to investigate the effect of delignification on properties of lignocellulose nanofibers (LCNFs) prepared by wet disk-milling (WDM) after steam and ozone oxidation pre-treatments and their nanopaper sheets. Delignification treatment was effective to obtain fine morphology with uniform fiber diameter less than 35 nm without aggregation, and increased the specific surface area (SSA) and filtration time of LCNFs. In particular, SSA and filtration time of the LCNFs prepared by WDM after ozone pretreatment increased 1.5 and 5.4 times after further delignification. Delignification also increased whiteness and decreased the redness of nanopaper sheets. The highest color difference (41.9) before and after the delignification was obtained in LCNFs prepared by WDM after the steam pretreatment. Tensile properties of nanopaper sheets were also increased by further delignification. The highest tensile strength was found to be 142 MPa.

Quality Characteristics of Wet Noodles after Addition of Grape-Peel Powder (포도 과피 첨가량에 따른 생면의 품질 특성)

  • Jo, Yong-Gi;Kim, Jang-Eix
    • Journal of the East Asian Society of Dietary Life
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    • v.18 no.5
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    • pp.822-828
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    • 2008
  • Optimal Chinese-noodle product in the aspect of preference and quality that added functionality, the focus was put on developing the stable high value-added product in a farm household. Experimental results showed that the value for infrared water-content analysis of moisture was $85.74{\pm}0.12%$, crude protein was $1.31{\pm}0.01%$, the crude fat $3.91{\pm}0.08%$, the ash $1.83{\pm}0.01%$, carbohydrate $1.08{\pm}0.03%$, and crude fiber $6.12{\pm}0.10%$. For all experiments with Chinese noodles, the grape peels were frozen and dried, powdered, and filtered with a 150-mesh strainer. The grape-peel powder, was added to the composite flour in a proportion of 0%, 1%, 3%, 5%, and 7%. The color of the cooked noodle appeared brown, demonstrating that the L-value decreased as the amount of grape-peel powder increased. The value of a, which corresponds to the level of redness, increased and the cooked noodle appeared brown as the amount of grape-peel powder added increased. The yellowness of the cooked noodle tended to decrease as the value of b, which corresponds to the level of yellowness, gradually (p<0.05). In the texture analysis, hardness was highest in the 7% grape-peel powder group, while the 5% groups showed the highest springness values. The 1% groups showed the highest cohesivness while the 7% groups were the chewiest. The 7% groups had the lowest stickiness values (p<0.05). It terms of sensory quality, the overall surface color, texture and taste were perceived as superior for the 3% grape-peel powder-added groups and lowest for the 7% group (p<0.001). The 3% treatment showed the best overall quality.

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Electrical and Mechanical Properties of Cu/Carbon Nano-Particle Hybrids Composites by Cathodic Electrophoresis (음극 전기영동법에 의해 제조된 구리/탄소 나노입자 하이브리드 복합재료의 전기적/기계적 특성 평가)

  • Lee, Wonoh;Lee, Sang-Bok;Choi, Oyoung;Yi, Jin-Woo;Byun, Joon-Hyung
    • Korean Journal of Metals and Materials
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    • v.48 no.12
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    • pp.1130-1135
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    • 2010
  • Cu/carbon nano-particle hybrids were fabricated through the cathodic electrophoretic deposition (EPD) process. CNT and CNF nano-particles were modified to give positive charges by polyethyleneimine (PEI) treatment before depositing them on the substrate. Since a Cu plate was used as an anode in the EPD process, Cu particles were also deposited along with the carbon nano-particles. Experimental observation showed the nano-hybrids constructed a novel formicary-like nano-structure which is strong and highly conductive. Utilizing the hybrids, carbon fiber composites were manufactured, and their electrical conductivity and interlaminar shear strength were measured. In addition, the deposition morphology and failure surface were examined by SEM observations. Results demonstrated that the electrical conductivities in the through-the-thickness direction and the interlaminar shear strength significantly increased by 350~2100% and 14%, respectively.

Study on the Hollow Fiber Nano-composite Membrane Preparation onto the Porous PVDF Membrane Surfaces using the Interfacial Polymerization (다공성 PVDF 막의 polyamide 계면중합법처리를 통한 나노 중공사 복합막 제조 연구)

  • Kang, Su Yeon;Cho, Eun Hye;Kim, Ihl hyung;Kim, Cheong Sik;Rhim, Ji Won
    • Membrane Journal
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    • v.24 no.2
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    • pp.107-112
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    • 2014
  • The composite membranes were prepared on the surface of hydrophobic porous poly (vinylidene fluoride) (PVDF) hollow fiber membranes through the interfacial polymerization. The preparation variables were the concentrations of piperazine (PIP), trimesoyl chloride (TMC) and the contents of polyethylene glyco l (PEG). The separation characterization of the resulting membranes were carried out for aqueous 100 ppm solution of NaCl, $CaSO_4$, and $MgCl_2$ and also mixed 300 ppm solution of NaCl and $CaSO_4$ in terms of the flux and rejection. Both the flux and rejection were the highest when the interfacial polymerization was conducted using TMC. When TMC concentration was 0.1 wt%, the flux and rejection were shown 48.3 LMH ($L/m^2{\cdot}hr$) and 59%, respectively. To improve the flux, the annealing post-treatment and the addition of PEG into piperazine were done. As expected, the overall flux was enhanced while the rejection was reduced.

Improvement of Mechanical Properties of Mg alloys through Control of Grain Size and Texture (결정립크기와 집합조직제어를 통한 마그네슘 합금의 기계적 성질 개선)

  • Kim, W.J.;Lee, J.B.;Kim, W.Y.;Jeong, H.G.;Park, J.D.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.57-58
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    • 2006
  • The effects of lowering ECAP temperature during ECAP process and Post-ECAP annealing on microstructure, texture and mechanical properties of the AZ31 alloys have been investigated in the present study. The as-extruded materials were ECAP processed to 2 passes at 553K prior to subsequent pressing up to 6 passes at 523K or 493K. When this method of lowering ECAP temperature during ECAP was used, the rods could be successfully deformed up to 6 passes without any surface cracking. Grain refinement during ECAP process at 553K might have helped the material to endure further straining at lower deformation temperatures probably by increasing the strain accommodation effect by grain boundary sliding, causing stress relaxation. Texture modification during ECAP has a great influence on the strength of Mg alloys because HCP metals have limited number of slip systems. As slip is most prone to take place on basal planes in Mg at room temperature, the rotation of high fraction of basal planes to the directions favorable for slip as in ECAP decreases the yield stress appreciably. The strength of AZ31 Mg alloys increases with decrease of grain size if the texture is constant though ECAP deformation history is different. A standard positive strength dependence on the grain size for Mg alloys with the similar texture (Fig. 1) supports that the softening of ECAPed Mg alloys (a negative slope) typically observed despite the significant grain refinement is due to the texture modification where the rotation of basal planes occurs towards the orientation for easier slip. It could be predicted that if the original fiber texture is restored after ECAP treatment yielding marked grain refinement, yield stress as high as 500 MPa will be obtained at the grain size of ${\sim}1{\mu}m$. Differential speed rolling (DSR) with a high speed ratio between the upper and lower rolls was applied to alter the microstructure and texture of the AZ31 sheets. Significant grain refinement took place during the rolling owing to introduction of large shear deformation. Grain size as small as $1.4{\mu}m$ could be obtained at 423K after DSR. There was a good correlation between the (0002) pole intensity and tensile elongation. This result indicates that tensile ductility improvement in the asymmetrically rolled AZ31 Mg alloys is closely related to the weakening of basal texture during DSR. Further basal texture weakening occurred during annealing after DSR. According to Hall-Petch relation shown in Fig. 1, the strength of the asymmetrically rolled AZ31 is lower than that of the symmetrically rolled one when compared at the same grain size. This result was attributed to weakening of fiber texture during DSR. The DSRed AZ31, however, shows higher strength than the ECAPed AZ31 where texture has been completely replaced by a new texture associated with high Schmid factors.

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Demonstration Study of Half-Saturated Bio-filter Wetland with Recirculation Pump for Road Stormwater (반포화 순환 여과식 인공습지에 의한 도로 강우유출수의 실증처리 연구)

  • Park, Kisoo;Kim, Youngchul
    • Journal of Wetlands Research
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    • v.19 no.3
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    • pp.259-270
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    • 2017
  • In this study, field-scale half-saturated bio-filter wetland equipped with recirculation system was operated with stormwater from the paved road, and its operational performance and functions of LID-BMP were analyzed and compared with other facilities. The reduction of TSS, COD, TN, and TP were 92%, 63%, 36%, and 75%, respectively. Comparison of the reduction efficiency were carried out with respect to ratio between surface and catchment areas(SA/CA). In addition, this LID-BMP facility can reduce about 70% of pollutant by treating only 18% of total rainfall runoff. The results show that LID used for this study gave similar efficiency although its ratio was smaller. In addition, comparison study was made between synthetic fiber as a filter media and organic media, which shows that there was not any significant difference between, TSS and TP reduction, but there were large difference in COD and TN removal due to the presence and absence of release of organic carbon. Meanwhile, wetland system in this study equipped with a first-flush capture gave a higher stability in terms of treatment performance.

Removal of Geosmin and 2-methylisoborneol in Drinking Water by Powdered Activated Carbon (분말 활성탄에 의한 먹는 물 내의 이취미 물질 제거)

  • Chae, A Na;Shin, Jae Won;Cho, Kang Woo;Lee, Byung Chan;Song, Kyung Guen
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.37 no.2
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    • pp.475-483
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    • 2017
  • Geosmin and 2-methylisoborneol (2-MIB) produced by cyanobacteria during algal blooming in surface water are the major taste-and-odor-causing compounds in drinking water and need to be removed. Activated carbon is often used in treatment plants for the mitigation of odor problem. However, there is a lack of information on the effect of pore size distribution and particle size of activated carbon for adsorption of both odor compounds. Therefore, we studied the effect of pore size distribution and particle size of activated carbon on the adsorption of geosmin and 2-MIB. When comparing the adsorption of geosmin and 2-MIB between activated carbon fiber (ACF), powdered activated carbon (PAC) and granular activated carbon (GAC), the order of removal efficiency was PAC > ACF > GAC. As a result of comparing PACs with various pore distribution characteristics, well-developed micropores on activated carbon were found to be favorable for adsorption of geosmin and 2-MIB. For particle size, smaller was more effective for adsorption of geosmin and 2-MIB.

Removal of Suspended Solids from Stormwater Runoff Using a Fabric Filter System (섬유필터를 사용한 강우유출수의 부유물질 제거 방법의 개발)

  • Koo, Young Min;Kim, Jaeyoung;Kim, Byung Ro;Seo, Dongil
    • Journal of Korean Society of Environmental Engineers
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    • v.37 no.3
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    • pp.165-174
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    • 2015
  • Non-point source pollution associated with suspended solids in stormwater has been known to often adversely affect surface water ecosystems. Various methods of treating stormwater in the basin area before the stormwater reaches the receiving body of water have been developed. However, these treatment methods tend to be costly to install and also to maintain. In this study, an economical way of removing TSS (total suspended solids) from stormwater runoff with a fabric filter system was developed. Polyester was chosen as a fabric-filter material, because it was found to be economical in cost and relatively resistant to various chemicals. An experimental device was developed and used to determine filtration rates through polyester fabric samples of a series of several pore-opening sizes ($20{\mu}m$ to $94{\mu}m$) under a series of water-heads (0.25 to 1 m). It was found that the filtration rate increased as the size of water head increased. It was also found that the smaller the pore size of the fiber filter was, the higher the TSS removal efficiency was. However, the TSS removal efficiency was not found to be much different among the filters with different sizes of pore opening due to the fact that most mass of TSS was associated with large particles.