• Title/Summary/Keyword: fiber surface treatment

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Effect of Dyeing Bath, Mordant and Chitosan Treatment on the Dyeing of Natural Cellulose Fiber Using African Marigold(Tagetes erecta L.) Petals Extract (African marigold(Tagetes erecta L.) 생화(生花) 추출물(抽出物) 염색(染色)에서 염욕(染浴)의 pH, 매염제(媒染劑,), Chitosan 처리(處理)가 섬유소섬유(纖維素纖維)의 염색성(染色性)에 미치는 영향(影響))

  • Kim, Kyung-Sun;Jeon, Dong-Won;Kim, Jong-Jun
    • Journal of Fashion Business
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    • v.11 no.1
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    • pp.136-148
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    • 2007
  • African marigold is a common plant easily available in many flower beds. It has been reported as a practical and prospective resource of dyes since the dyes can be extracted from their bodies as well as petals. In this research, cotton and ramie fabrics which are made from natural cellulose were dyed using the extract of the African Marigold which is a variety of marigold. Dyeing tests were carried out under different pH of the dye solution and mordants. Dyeability was evaluated by examining and measuring surface color, K/S value, and the changes in the maximum absorption wavelength. The probability of improving dyeability was investigated by pre-mordanting with pre-treated chitosan. For the dyeing with marigold extract, the color tone did not differ by pre-mordanting and non-mordanting. Reaction with post-mordanting was excellent, which was colored in various yellow series. The best dyeability was achieved in dye solution of pH 6.5-7.0 which is not conditioned. The largest K/S value and color difference were obtained in tin mordanting. The dye uptake was greatly increased in chitosan pre-treated mordanting compared with the post-mordanting without chitosan pre-treatment. Due to its high heat resistance, African Marigold extract is easy for dye extraction and dyeing, and its dyeability is excellent for natural cellulose fibers. Also, colorfastness was proved to be practically usable.

A Study on the Improvement on the Target Structure in a Magnetron Sputtering Apparatus (마그네트론 스퍼터링 장치의 타겟구조 개선에 관한 연구)

  • Bae, Chang-Hwan;Lee, Ju-Hee;Han, Chang-Suk
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.1
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    • pp.23-28
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    • 2010
  • The cylindrical magnetron sputtering has not been widely used, although this system is useful for only certain types of applications such as fiber coatings. This paper presents electrode configurations which improved the complicacy of the target assembly by using the positive voltage power supply. It is a modified type which has a target constructed with a large cylindrical part, a conical part and a small cylindrical part. When positive voltage was applied to an anode, a stable glow discharge was established and a high deposition rate was obtained. The substrate bias current was monitored to estimate the effect of ion bombardment. As a result, it was found that the substrate current was large. With cylindrical and conical cathode magnetron sputter deposition on the surface of the substrate to prevent re-sputtering, ion impact because it can increase the effectiveness with excellent ductility and adhesion of Ti film deposition can be obtained. We board at the front end of the ground resistance of $5\;k{\Omega}$ attached to the substrate potential can be controlled easily, and Ti film deposition with excellent adhesion can be obtained. Microstructure and morphology of Ti films deposited on pure Cu wires were investigated by scanning electron microscopy in relation to preparation conditions. High level ion bombardment was found to be effective in obtaining a good adhesion for Cu wire coatings.

Effects of Inorganic Coagulants on Sizing and Contamination in Newsprint Mill (무기 응결제가 신문용지의 사이즈도와 공정오염에 미치는 영향)

  • Lee, Tai Ju;Seo, Jin Ho;Lee, Kwang Seob;Jeong, Sung Hyun;Ryu, Jeong Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.3
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    • pp.40-46
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    • 2015
  • For some Korean newsprint mill, addition level of aluminum sulfate has been reduced because sulfur from aluminum sulfate has detrimental effect on the efficiency of anaerobic water treatment. At this moment, an unexpected decrease in sizing degree of TMP mixed newspaper was occurred. The phenomena means that hydrophobic substance usually originated from TMP cannot be fixed on the paper. This study focused on effect of alum and PAC on sizing of paper and contamination. Also, substitutability of PAC was discussed as a possible alternatives of aluminum sulfate under anaerobic condition of water treatment. Evaluation of sizing degree and pitch deposit potential were performed at the varied addition level of PAC and aluminum sulfate. Hydrophobic substance mainly derived from TMP could be fixed on the surface of fiber by PAC. Fines retention was not changed by replacing aluminum sulfate with PAC. Additionally, fixing of hydrophobic substance without excessive agglomeration can be enhanced by PAC with low molecular weight. Consequently, sizing degree of newspaper and contamination of recycling process of ONP can be controlled by low molecular weighted PAC.

Analysis on Physical Changes of Pectinase-Treated Brown Rice (Oryza sativa) (Pectinase 처리 전후의 현미의 물리적 변화 분석)

  • Pih, Kyung-Tae;Kim, Keun-Cheol
    • Journal of Life Science
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    • v.23 no.4
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    • pp.554-559
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    • 2013
  • Brown rice (Oryza sativa) is rich in nutrients, including dietary fiber, vitamins, minerals, and other unmeasured constituents, as well as carbohydrates. Brown rice is an applicable staple for chronic diseases, such as diabetes and hyperlipidemia, but it is not commonly used in dietary management due to several reasons. In this study, we investigated the possibility of using digestive enzymes to process brown rice. When the weight of the brown rice was measured after packing in the same volume of water, it was increased in pectinase-treated brown rice compared to control or collagenase-treated brown rice. Using SEM analysis, we observed huge scratches and nanopores on the surface of the brown rice after the pectinase treatment, but the nutritional components were preserved. We also analyzed the water adsorption rate and performed a starch reaction assay to examine the physical changes after the pectinase treatment. The pectinase-treated brown rice showed a higher water adsorption rate and a faster starch reaction than the nontreated brown rice. These results suggest that digestive enzymes like pectinase can aid the nutritional preservation of brown rice and improve its taste.

Effect of Sodium Lignosulfonate Treatment on the Dispersion of CaCO3 in CaCo3/Polypropylene Composite (Sodium Lignosulfonate 표면처리가 탄산칼슘/폴리프로필렌 복합체에서 탄산칼슘의 분산에 미치는 영향)

  • Song, Junyoung;Kwark, Young-Je;Jeong, Youngjin
    • Polymer(Korea)
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    • v.39 no.3
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    • pp.382-387
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    • 2015
  • The dispersion of calcium carbonate ($CaCO_3$) in polypropylene (PP) and the effect of $CaCO_3$ size on the crystallinity of PP were studied. Polymer composite usually suffers from the brittleness when reinforced with inorganic fillers. The problem is generally related to the size and dispersion of fillers. First, the dispersion was studied for the nanosize $CaCO_3$ with 15~40 nm average diameter. To enhance the dispersibility in PP, the surface of the $CaCO_3$ was treated with sodium lignosulfonate (SLS). $CaCO_3$/PP composites were prepared via melt compounding. The $CaCO_3$ coated with more than 3 wt% SLS was uniformly distributed within the PP matrix, while the uncoated $CaCO_3$ formed aggregated structures in the PP. Even with 30 wt%, the SLS-$CaCO_3$ was well dispersed in the PP matrix. Also, the transition enthalpy of $CaCO_3$/PP increased and the full-width of half maximum of the crystallization peak decreased regardless of SLS coating and size of $CaCO_3$. However, the crystallinity of PP was more influenced by nano $CaCO_3$. These results imply that the nano $CaCO_3$ coated with SLS may reduce the brittleness of polymer composites.

A Study on the Treatment of Heavy Metal in Wastewater by Redox Reaction of Cu-Zn Metal Alloy and Adsorption reaction of Al-Silicate (Cu-Zn 금속합금의 산화 환원반응과 Al-Silicate의 흡착반응을 이용한 폐수 중 중금속처리에 관한 연구)

  • Lee, Soo-Jeong;Kim, Jong Hwa;Song, Ju Yeong
    • Journal of the Korean Applied Science and Technology
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    • v.33 no.3
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    • pp.441-448
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    • 2016
  • Heavy metal removal study is conducted from synthetic waste water by reduction and oxidation(redox) reaction of Cu-Zn metal alloy and adsorption reaction of aluminium silicate. Heavy metal whose ionization tendency is smaller than zinc are reducted in an aqueous solution, and the concentration of ionized zinc is reduced by adsorption reaction. The average diameter of metal alloy micro fiber is about $200{\mu}m$, and the surface area is wide enough to get equilibrium in a single cycle treatment. A single cycle treatment of redox reaction of Cu-Zn metal alloy, could remove 100.0 % of Cr(III), 98.0 % of Hg, 92.0 % of Sn and 91.4 % of Cu respectively. An ionization tendency of chromium is very close to zinc, but removal efficiency of chromium by redox reaction is significant. This result shows that trivalent chromium ion is expected to generate hydroxide precipitation with $OH^-$ ion generated by redox reaction. Zinc ion generated by redox reaction is readily removed by adsorption reaction of aluminium silicate in a single cycle treatment. Other heavy metal components which are not perfectly removed by redox reaction also showed very high removal efficiency of 98.0 % or more by adsorption reaction. Aluminium ion is not increased by adsorption reaction of aluminium silicate. That means heavy metal ion removal mechanism by adsorption reaction is turned out to be not an ion exchange reaction, but an adsorption reaction.

A Study on Paper of Old Monk by Yun Duseo (윤두서필 노승도의 바탕 종이 고찰)

  • Cheon, Juhyun;Park, Miseon;Kim, Yein
    • Conservation Science in Museum
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    • v.16
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    • pp.82-95
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    • 2015
  • Old Monk by Yun Duseo is realized to use silver paper which is made of rarity material. This sudy investigates reason why silver, that is easily discoloration in environmental condition, is susceptible in present. The method was the surface treatment materials and the base fiber through direct observation, optical instruments and XRF analysis. Based on these results, reproducing experiment was conducted to research materials in paper of Old Monk and the surface treatment technique. The results, the paper was treated 'Dochim' with a mineral having polygonal crystals for improving smoothness and density. XRF analysis result showed high calcium content, therefore, the paper was not used silver, it guess pulverized shells of abalone or other types of shellfish. Accordingly, the research was narrowed down to shells with shiny, reflective surfaces which at the same time contain high amounts of calcium. A new experiment was conducted using unprocessed abalone shells. Through the reproducing experiment, shellfish has high possibility as used mineral in paper. Notwithstanding, this experiment was unable to precisely reproduce the smoothness and shine of the original paper. Further research may therefore be needed.

An Experimental Studies on the alleviation effects of Daebangpoongtang(大防風湯) in LPS-induced arthritis (대방풍탕(大防風湯)의 LPS유발(誘發) 관절염(關節炎) 완화효과(緩和效果)에 관한 실험적(實驗的) 연구(硏究))

  • Jeon, Won-June;Shin, Gil-Jo;Lee, Won-Chul
    • The Journal of Dong Guk Oriental Medicine
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    • v.9
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    • pp.35-49
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    • 2000
  • Purpose: This study is to investigate the alleviation effects of Daebangpoongtang in LPS induced arthritis in mice knee joint. Methods : Daebangpoongtang was chosen to treat the arthritis caused by injecting $300{\mu}g/kg$ LPS to mice knee joint. The control group had no treatment, while the LPS group was injected $300{\mu}g/kg$ LPS to mice knee joint and the DBP group was oral administrated of Daebangpoongtang. After injection of $300{\mu}g/kg$ LPS to mice knee joint, the alteration of synovial lining cell, vessel, fibrosis, distribution of collagen fiber, fibroblast, mast cell, infiltration of inflammation component cell and distribution of ICAM and VCAM was observed by light microscope(BX50). Results : In the DBP extract treatment group, the distribution of vessel, the enlargement of synovial lining cell layer, the synovial lining cells with filopodia, the fibrosis, the distribution of fibroblast in synovial membrane, the distribution of TCAM and VCAM on the knee joint was less than that of LPS group. Infiltrated lymphocyte into the apical surface had not observed in the DBP extract treatment group. The distribution of mast cell was as same as control group(no treatment group) and it showed granulated type. Conclusion: According to the above results, it might be considered that the administration of Daebangpoongtang has a curative effect on synovial membrane injury in arthritis by inhibiting increase of vessel, cell adhesion molecule(ICAM and VCAM) in LPS induced arthritis.

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Effect of Winter Mulching on Growth and Fiber Yield of Ramie Plant (동계피복이 모시풀의 생육 및 섬유수량에 미치는 영향)

  • 권병선;김상곤;정동희;임준택
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.38 no.3
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    • pp.208-212
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    • 1993
  • Since ramie suckers distribute soil surface layer within 10cm depth, some of them are dead from low soil temperature in winter. An experiment was conducted to investigate the effects of various mulching methods on safe overwintering of sucker at three or four years old, fully-grown ramie plots. The sprouting dates of ramie was March 28 in transparent vinyl mulching(TPEF), April 1 in transparent vinyl mulching over cover of straw, manure or rice hull at the amount of 500kg /10a (CM), and April 6 in black vinyl mulching(BDEF). These treatments showed earlier sprouting date from 9 to 18 days than the conventional mulching with 1000 kg straw /10a the sprouting date of which was April 15. TPEF treatment showed the earliest but ununiform sprouting. In contrast, sprouts in CM treatment was uniform but emerged somewhat later compared with the treatment of TPEF. The number of stems per unit area increased 50 percent more in TPEF, and 35 to 39 percent more in CM than the treatment of conventional mulching.

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Crystallization of the NiZn ferrite nanofibers fabricated by electrospinning method (전기방사법을 이용해 제조된 NiZn ferrite 나노 섬유의 결정화)

  • Na, Kyeong-Han;Yoo, Sun-Ho;Song, Tae-Hyub;Kim, Sung-Wook;Choi, Won-Youl
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.6
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    • pp.226-231
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    • 2020
  • Polyvinyl pyrrolidone nanofibers including nickel, zinc, and iron precursors were fabricated via the electrospinning method. To convert as-spun nanofibers to Ni0.5Zn0.5Fe2O4 oxide nanof ibers which is capable of shielding an electromagnetic wave, heat treatment conditions were optimized. To obtain the heat treatment condition that can exclude amorphous carbon black and secondary crystal phase, samples were taken at each temperature while the calcination process and analyzed. According to the X-ray diffraction (XRD) analysis, the Ni0.5Zn0.5Fe2O4 crystal phase started to appear from 300℃, but it was confirmed through energy dispersive spectroscopy (EDS) analysis that heat treatment of 500℃ or more was required to remove most of the carbon black. When the calcination temperature exceeds 650℃, crystal nuclei starts to grow and the fiber surface condition becomes rough, so it was confirmed that the heat treatment conditions should be selectively determined according to the application field.