• Title/Summary/Keyword: fiber surface treatment

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Interfacial Morphology of Glass Fiber/Polypropylene Composite (유리 섬유/폴리프로필렌 복합재료의 계면 형태구조)

  • 남주영;박수현;이광희;김준경
    • Polymer(Korea)
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    • v.27 no.4
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    • pp.299-306
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    • 2003
  • It is well known that the interaction and adhesion between the glass fiber (GF) and polymer matrix has a significant effect in determining the properties of fiber-reinforced materials. Therefore, it is one of important considerations to modify the surface of glass fiber with an appropriate sizing. We investigated the treatment method of glass fiber with coupling agent to improve the interaction of the interfacial region. The correlation between interfacial property and interphase microstructure was also examined in an attempt to realize a proper morphology at the glass fiber surfaces.

Electro-spun Antimicrobial Acrylic Fiber

  • Lee, Jae-Woong;Ren, Xue-Hong;Broughton, R.M.;Liang, Jie;Worley, S.D.;Huang, T.S.
    • Textile Coloration and Finishing
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    • v.19 no.2
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    • pp.44-49
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    • 2007
  • Antimicrobial fibers were prepared by an electro-spinning method. Polystyrene hydantoin(PSH) was employed as an antimicrobial precursor to produce an electro-spun antimicrobial acrylic fiber. Increasing the surface area of hydrophobic antimicrobial-fibers provides enhanced antimicrobial efficacy. The biocidal activity of electro-spun acrylic fibers could be rendered through chlorine bleach treatment, and the antimicrobial effectiveness against gram-Positive and gram-negative bacteria was investigated. In addition, scanning electron microscopy(SEM) demonstrated the feature of the electro-spun fibers.

Strength Property Improvement of OCC-based Paper by Chemical and Mechanical Treatments(I) (골판지 고지의 물리화학적 처리에 의한 강도 향상(제 1 보))

  • Lee, Jong-Hoon;Seo, Yung B.;Jeon, Yang
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.1
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    • pp.10-18
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    • 2000
  • To improve the physical properties of OCC (Old Corrugated Container) fibers, we used the mechanical pre-treatment on the fibers before refining . The mechanical action in the Hobart mixer induced high shear and compression on the fibers, which resulted in changes of fiber internal structure, and microcompressions on the surface of the fibers. We evaluated the amount of mechanical treatment on the fibers by fiber curl index for convenience. Four different refining techniques were applied to the pre-treated fibers (valley beater, Kady mill, PFI mill, and Impact refining) to find the best combination of the pre-treatment and the refining methods. Conclusions were summarized as followed. 1. Mechanical pre-treatment in Hobart mixer for more than 1 hour caused the increase of curl index of OCC fibers, and increased breaking length, burst index, and tear index the handsheets more than 10 % in this experiment. 2. Kady mill and PFI mill refining were effective in keeping fiber length from shortening Kady mill and Valley beater refining straightened out the fiber curls, and reduced the curl index. 3. Valley beating reduced fiber length very fast and generated fines more than other refining methods. 4. To increase breaking length and burst strength while keeping tear strength , combination of mechanical pre-treatment and Valley beating were most effective.

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The Study on the Effect of Plasma Pre-treatment on the Dyeing Properties and the Handle in the Environment Friendly Enzyme Finishing (친환경 효소가공에서 플라즈마 전처리가 염색성과 태에 미치는 영향)

  • Kim, Ji-Hyun
    • Journal of the Korea Fashion and Costume Design Association
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    • v.10 no.3
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    • pp.173-180
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    • 2008
  • Cotton, wool, cotton/wool blended (80:20) and tencel fabrics were treated with low temperature oxygen plasma, enzymes (cellulase or protease), or oxygen plasma-enzyme and they were examined for dyeing and handling properties for environment friendly finishing. The appropriate conditions for cellulase treatment were enzyme concentration of 3g/l, pH of 5, and $60^{\circ}C$ for one hour, and for protease treatment were enzyme concentration of 4g/l, pH of 8, and $60^{\circ}C$ for one hour. The equilibrium uptake of a direct dye on cotton changed with plasma treatment and plasma-cellulase treatment, and the rate of dyeing slightly decreased. When wool was dyed with acid dye, the equilibrium dye uptake did not change with plasma, protease treatment nor plasma-protease treatment, however, the rate of dyeing had increased with plasma-protease treatment. From these results, it is assumed that plasma attacks the surface of the fiber, and enzyme mainly affects the inner part of the fiber. Plasma treatment did not affect mechanical properties related to the handling of fabrics. The handling test showed increased extension at maxmum load(EM), tensile energy(WT) with decreased tensile resilience (RT), and the fabrics became softer but resilience decreased slightly with enzyme treatment. The bending recidity(B), hysteresis of bending moment(2HB), and hysteresis of shear force at five degrees(2HG5) decreased, however, shear stiffness(G) increased. I knew the plasma pre-treatment made fabrics softer with lower koshi(stiffness). The handling of plasma pre-treated fabrics was better than that of enzyme-treated fabrics. When we pre-treated fabrics, the handling test showed decreased coefficient of friction(MIU), geometrical roughness(SMD), while the surface of fabrics became smoother and numeri increased. Even though compression resilience(RC) increased, fukurami(bulky property) and compressive elasticity, decreased due to the linearity of compression-thickness curve(LC) and compression energy(WC).

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The Effect of Acidic Liquid from Carbonized Rice Hull Treatments to Molded Fiber Packages on the Shelf Life of Egg (왕겨초액을 처리한 계란포장용 펄프몰드의 저장성 유지 효능 분석)

  • Min, Choon-Ki;Jo, Joong-Yeon;Shin, Joon-Sub;Lee, Se-Un;Jeon, Ki-Hong
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2011.10a
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    • pp.335-343
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    • 2011
  • We examined the effect of the acidic liquid from carbonized rice hull(ALCRH) treatments to molded fiber packages(MFP) on weight, Haugh unit, pH and microbial activity of egg to extend the shelf life in egg packaging. Higher concentration and surface spray treatment of the acidic liquid extended the shelf life of egg. ALCRH treatment to MFP improved the performance of the packaging for egg in terms of decreased weight loss and retarded microorganism growth of eggs during storage.

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A STUDY FOR THE BONDING STRENGTH OF COMPOSITE RESIN CORE TO GLASS FIBER POST (Glass Fiber Post와 Composite Resin Core의 전단결합강도)

  • Kim Tae-Hyoung;Shim June-Sung;Lee Keun-Woo
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.4
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    • pp.415-425
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    • 2005
  • Statement of problem : Fracture of composite resin core will be occulted by progress of crack. Bonding interface of different materials has large possibility of starting point of crack line. Therefore, the bond strength of glass fiber post to composite resin core is important for prevention of fracture. Purpose: This in vitro study tried to find out how to get the higher strength of glass fiber post to composite resin core through surveying the maximum load that fractures the post and cote complex. Materials and methods: 40 specimens made with glass fiber Posts(Style $post^{(R)}$, Metalor, Swiss) and composite resin core ($Z-100^{(R)}$, 3M, USA) were prepared and loaded to failure with push-out type shear-bond strength test in a universal test machine. The maximum fracture load and fracture mode were investigated in the specimens that were restored with four different surface treatments. With the data. ANOVA test was used to validate the significance between the test groups, and Bonferroni method was used to check if there is any significant statistical difference between each test group. Evely analysis was approved with 95% reliance. Results: On measuring the maximum fracture load of specimens, both the treatments of sandblasted and acid-etched one statistically showed the strength increase rather than the control group (p<0.005). The scanning electric microscope revealed that sand blasting made more micro-retention form not only on the resin matrix but on the glass fiber, and acid-etching contributed to increase in surface retention form, eliminated the inorganic particles in resin matrix. Specimen fracture modes investigation represented that sand blasted groups showed lower bonding failure than no-sand blasted groups. Conclusion: Referring to the values of maximum fracture load of specimens, the bonding strength was increased by sand blasting and acid-etching.

Fiber Surface Engineering to Improve Papermaking Raw Material Quality

  • Wang Eugene I-Chen;Perng Yuan Shing
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2006.06b
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    • pp.271-278
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    • 2006
  • We used polymers of alternating cationic and anionic nature to build up shells on fiber surfaces, strengthen the worn-out fibers and improve paper properties made from such fibers. OCC and ONP pulps were either dipped or salted out in the cationic polyallylamine, polyacrylamide and starch solutions. After centrifugal drying, these were followed by treatments in anionic polyacrylic acid, poly-acrylamide, and starch solutions, respectively. The shell-enhanced fibers were formed into handsheets and their physical properties evaluated. The results show that building multiple shells on worn-out fiber surfaces can strengthen the fibers and paper. The simpler and more practical impregnation-centrifuging treatment provided the desired effects, whereas salting out the polymers produced somewhat superior fibers. The latter process, were impractical, however. The first pair of polymeric shells imparted marked strength improvement, whereas later layers had diminishing efficacies. Overall, the methods can improve fiber quality, attaining paper strength requirements without resorting to expensive measures. Alternate cationic polymer and filler powders were also deposited on fiber surface based on the micriparticle system in an anticipation of stiffness gains. Platy minerals, such as montmorillonite, bentonite, sericite, clay and talc were added following cationic PAM. After dewatering of polymer-pigment shelled fiber of one to 3 pairs of layers, handsheets either calendered or uncalendered were evaluated. The results indicate that regardless of calendaring, stiffness of the handsheets did not improve appreciably while certain other strength properties showed gains. We also attempted the novel starch gel filler addition method wherein tapioca starch and filers (PCC, sericite or clay) were mixed at high solids content of 50% and cooked until gelatinized. The filled handsheets were dried under various conditions and then tested for their properties. Improvements in strengths of modified filled paper were observed.

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EARLY CARIES DETECTION WITH DIGITAL IMAGING FIBER-OPTIC TRANS-ILLUMINATION (Digital Imaging Fiber-Optic Trans-Illumination을 이용한 초기우식의 탐지)

  • Lee, Jun-Seok;Kim, Jong-Soo;Yoo, Seung-Hoon
    • The Journal of Korea Assosiation for Disability and Oral Health
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    • v.3 no.2
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    • pp.87-90
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    • 2007
  • It's important that detect early caries of deciduous and permanent teeth to prevent dental caries and prevserve teeth, especially on proximal surface of deciduous teeth. The reason is that their prominent pulp horn lead to pulp treatment easily due to rapid caries progression. There are conventional exploring, visual inspection and radiographic exam for early caries detection. But, the standard method for diagnosing dental caries is subject and cavitation may be accelerated during exploring procedure. Caries can be diagnosed up to 40% mineral loss with radiograph. $DIFOTI^{(R)}$ (Digital Imaging Fiber-Optic TransIllumination) is diagnostic imaging system for early caries detection using fiber-optic illumination. It is possible that remineralize the tooth surface without tooth preparation and conserve the tooth structure by using $DIFOTI^{(R)}$.

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Application of Laser Surface Treatment Technique for Adhesive Bonding of Carbon Fiber Reinforced Composites (탄소복합재 접착공정을 위한 CFRP의 레이저 표면처리 기법의 적용)

  • Hwang, Mun-Young;Kang, Lae-Hyong;Huh, Mongyoung
    • Composites Research
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    • v.33 no.6
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    • pp.371-376
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    • 2020
  • The adhesive strength can be improved through surface treatment. The most common method is to improve physical bonding by varying the surface conditions. This study presents the effect of laser surface treatment on the adhesive strength of CFRP. The surface roughness was patterned using a 1064 nm laser. The effects of the number of laser shots and the direction and length of the pattern on the adhesion of the CFRP/CFRP single joint were investigated through tensile tests. Tests according to ASTM D5868 were performed, and the bonding mechanism was determined by analyzing the damaged surface after a fracture. The optimized number of the laser shots and the optimized depth of the roughness should be required to increase the bonding strength on the CFRP surface. When considering the shear stress in the tensile direction, the roughness pattern in the direction of 45° that increases the length of the fracture path in the adhesive layer resulted in an increase of the adhesive strength. The surface treatment of the bonding surface using a laser is a suitable method to acquire a mechanical bonding mechanism and improve the bonding strength of the CFRP bonding joint. The study on the optimized laser process parameters is required for utilizing the benefits of laser surface processing.

The Effect of Steam Treatment on Dyeing Properties of Wool Fibers (증기처리가 양모섬유의 염색성에 미치는 영향)

  • Lee, Mun Cheul;Bae, So Yeung;Wang, In Sook
    • Textile Coloration and Finishing
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    • v.9 no.2
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    • pp.10-16
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    • 1997
  • Merino wool top and fabric have been treated with steams such as superheated steam or high pressure steam. Moisture regain, water absorbency, water penetration, zeta potential, ESCA, SEM, and dyeing behavior were studied. Negative electric potential on the surface of wool fibers by steam treatment became higher than untreated. From the results of ESCA measurement, intensity of $O_{1s}$ was increased by steam treatment. Rate of dyeing and saturation dye exhaustion of wools increased by steam treatment, especially high pressure steam treatment. Moisture regain, water absorbency, water penetration, and surface appearances by SEM photographs of the steam-treated wools didn't change. There is no relationship between dyeing of the steam-treated wool and wettability to water. Therefore It seems likely that relaxation of adhesive filler in interscale of wool by steam treatment accelerate dye penetration into the fiber.

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