• Title/Summary/Keyword: fiber & film

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High-Sensitive Fiber-Optic pH Sensor Using Neutral Red Immobilized in Porous Sol-Gel Film (뉴트럴레드가 고정화된 다공성 졸-겔 필름을 이용한 고감도 광섬유 pH 센서의 특성)

  • Jeon, Da-Yeong;Yoo, Wook-Jae;Shin, Sang-Hun;Han, Ki-Tek;Park, Jang-Yeon;Park, Byung-Gi;Cho, Seung-Hyun;Lee, Bong-Soo
    • Journal of Sensor Science and Technology
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    • v.21 no.3
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    • pp.223-228
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    • 2012
  • In this study, a fiber-optic pH sensor based on a pH sol-gel film is fabricated. The sol-gel film is made by co-polymerizing tetramethoxysilane, trimethoxymethylsilane, ethanol and distilled water. As a pH indicator, a neutral red is immobilized in a thin porous film formed by the sol-gel process. The pH change in a sensing probe gives rise to a change in the color of the pH sol-gel film, and the absorbance of reflected light through the pH sol-gel film is also changed. By using a spectrometer, therefore, the spectra of reflected lights in the sensing probe with different pH values are measured. Also, the relationships between the pH values and the absorbance are analyzed on the basis of the color variations of the pH sol-gel films. In repeated experiments, the fiber-optic pH sensor shows that it has reversibility, a high reproducibility and a wide absorbance change in a pH range from pH 5 to 9. Also, we confirmed that the fabricated pH sol-gel film exhibits a fast response time, little or no pH indicator leaching and a dynamic range of 2.04 dB from pH 5 to 9. Based on the results of this study, a fiber-optic pH sensor can be developed for the pH monitoring in the harsh environments.

Manufacture of Short Fiber Prepreg using Electroflocking (Electroflocking을 이용한 단섬유 프리프레그 제조에 관한 연구)

  • Lim, S.H.;Lee, S.S.;Pak, M.;Kim, J.K.;Choe, C.R.;Kwon, S.J.
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.288-291
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    • 2002
  • The carbon fiber or glass fiber reinforced prepregs were manufactured using electrostatic flocking technology. The powder of high density polyethylene was used as a matrix. The base film of polyethylene was prepared using a fluidized bed of polyethylene powder under the high electric field. We obtained HDPE film with uniform thickness of minimum $80\mu\textrm{m}$. And the fibers were aligned on the molten HDPE film by the electroflocking process. The short fibers with 1mm were easily electrically charged and aligned under the high electric field. The carbon fibers with high conductivity were elasily electrically charged than the glass fibers with low conductivity. So lower electric field was needed for the carbon fibers.

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Development and Characterization of Active Alignment System of Optical Fiber and Film filter for Micro Optical Communication Module (초소형 광모듈 제작을 위한 광섬유와 박막형 필터의 능동형 정렬 및 평가 시스템)

  • 최두선;박한수;서영호;제태진;황경현
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.9
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    • pp.111-118
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    • 2004
  • The automatic assembly system of micro optical filter is a key technology in the development of optical modules with high functionality. In order to develop an automatic assembly system of optical fiber and filter, we have firstly developed the system and program capable of characterization of 30${\mu}m$-thick film filters as well as conventional optical filters. Moreover, we have carried out the characterization of optical filter using the developed system and program, and compared experimental results with by conventional handwork. The measurement of optical filters using the present system is faster, more precise and more reliable than those based on the conventional handwork.

Oxide Semiconductor Thin Film Transistor based Solution Charged Cellulose Paper Gate Dielectric using Microwave Irradiation

  • Lee, Seong-Yeong;Jo, Gwang-Won;Jo, Won-Ju
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.207.1-207.1
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    • 2015
  • 차세대 디스플레이 소자로서 TAOS TFT (transparent amorphous oxide semiconductor Thin Film Transistor)가 주목 받고 있다. 또한, 최근에는 값 비싼 전자 제품을 저렴하고 간단히 처분 할 수 있는 시스템으로 대신 하는 연구가 진행되고 있다. 그중, cellulose-fiber에 전기적 시스템을 포함시키는 e-paper에 대한 관심이 활발하다. cellulose fiber는 가볍고 깨지지 않으며 휘는 성질을 가지고 있다. 가격도 저렴하고 가공이 용이하여 차세대 기판의 재료로서 주목받고 있다. 하지만, cellulose-fiber 위에는 고온의 열처리공정과 고품질 박막 성장이 어려워서 TFT 제작에 어려움을 겪고 있다. 이러한 문제를 해결하기 위해서 산화물 반도체를 이용하여 TFT를 제작한 사례가 보고되고 있다. 또한, 채널 물질 뿐만 아니라 cellulose fiber에도 다른 물질을 첨가하거나 증착하여 전기적 화학적 특성을 개선시킨 사례도 많이 보고되고 있다. 본 연구에서는 가장 저품질의 용지로 알려진 신문지와 A4용지를 gate dielectric을 이용하여서 a-IGZO TFT를 제작하였다. 하지만, cellulose fiber로 만들어진 TFT의 경우에는 고온의 열처리가 불가능 하다. 따라서 저온에서 높을 효율은 보이는 microwave energy를 이용하여 열처리를 진행하였다. 추가적으로 저품질의 종이의 특성을 개선시키기 위해서 high-k metal-oxide solution precursor를 첨가 하여 TFT의 특성을 개선시켰다. 결과적으로 cellulose fiber에 metal-oxide solution precursor을 첨가하는 공정과 micro wave를 조사하는 방법을 사용하여 100도 이하에서 cellulose fiber를 저렴하고 우수한 성능의 TFT를 제작에 성공하였다.

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A Study on the Proper Resin Film Thickness in RFI Process (RFI 공정시 적정 수지필름 두께에 관한 연구)

  • Yoon, S.H.;Lee, J.W.;Kim, J.S.;Kim, W.D.;Um, M.K.
    • Composites Research
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    • v.31 no.1
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    • pp.23-29
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    • 2018
  • The RFI process can be applied to very thick structures without limiting the resin viscosity. When the proper thickness of the resin film cannot be set, the resin film creates either the non-impregnated section or the excessive resin contents and this leads to the deterioration of mechanical properties. Therefore, this study proposed a method for setting the resin film thickness in the RFI process. The fiber compaction behavior test was proposed by setting the proper resin film thickness and the properties of composites were evaluated through short beam shear strength test, compression test and porosity measurement to verify the proposed method. The evaluation of physical properties of composites was conducted and an appropriate level of resin film thickness was found based on the results of fiber compaction behavior test.

Fabrication and Performance Evaluation of a Scintillating Film-based Gamma Imaging Detector to Measure Gamma-ray Distribution (감마선 분포 측정을 위한 섬광필름 기반의 감마 영상 검출기 제작 및 성능평가)

  • Shin, Sang Hun;Yoo, Wook Jae;Jang, Kyoung Won;Cho, Seunghyun;Lee, Bongsoo
    • Journal of Sensor Science and Technology
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    • v.24 no.3
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    • pp.202-207
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    • 2015
  • As a feasibility study on development of a gamma imaging probe, we developed a scintillating film-based gamma imaging detector that can obtain scintillation images with information of gamma-ray distribution. The scintillating film-based gamma imaging detector was composed of a sensing probe, an image intensifier, and a beam profiler. To detect and transmit scintillation image, the sensing probe was fabricated by coupling a scintillating film, a fiber-optic image conduit, and a fiber-optic taper, consecutively. First, the optical images of USAF 1951 resolution target were obtained and then, modulation transfer function values were calculated to test the image quality of the sensing probe. Second, we measured the scintillation images according to the activity of the 137Cs and the distance between the surface of 137Cs and the distal-end of sensing probe. Finally, the intensities of scintillating light as functions of the activity and the distance were evaluated from the region of interest in the scintillation image. From the results of this study, it is expected that a fiber-optic gamma imaging detector can be developed to detect gamma-rays emitted from radiopharmaceuticals during radioimmunoguided surgery.

Hydrogen Detection System Based on Pd Coated Single Mode Fiber Sensor (Pd이 코팅된 단일모드 광섬유 센서를 이용한 수소 검출 시스템)

  • Kim, Kwang-Taek;Park, Son-Oc;HwangBo, Seung;Mah, Jae-Pyung;Baik, Se-Jong;Im, Kie-Gon;Kim, Tae-Un;Kim, Hwe-Jong
    • Korean Journal of Optics and Photonics
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    • v.18 no.6
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    • pp.389-394
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    • 2007
  • The characteristics of the single mode fiber hydrogen sensor have been investigated theoretically and experimentally. Palladium is adopted as a material for the transducer and a thin Ni film is used for the adhesion between the fiber end and the Pd film. It is shown that sensitivity and response time strongly depend on the thickness of Pd film. The single mode fiber sensor coated with 5 nm thick Ni adhesion layer and 10 nm thick Pd transducer layer showed 0.6 dB change of reflectivity and $3{\sim}5$ sec of response time as it absorbed 4% hydrogen gas.

Study of transfer film in the sliding of nanoscale CuO-filled and fiber-reinforced polyphenylene sulfide (PPS) composites (CuO nanoparticle 및 fiber 로 구성된 PPS 복합재료의 sliding 조건하의 transfer film 에관한 연구)

  • Cho, Min-Haeng;Bahadur, Shyam;Park, Hye-Young;Kim, Yoon-Jun
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.967-972
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    • 2004
  • The role of transfer films formed during sliding of polymer composites against steel counterfaces was studied in terms of the tribological behaviors of composites. Four kinds of composites were included in this study: (1) unfilled PPS, (2) PPS+2%CuO, (3) PPS+2%CuO+5% carbon fiber (CF), and (4) PPS+2%CuO+15%Kevlar. The filler material CuO was in nanoscale particulate form and the reinforcing material was in the form of short fibers. The composites were prepared by compression molding at $310^{\circ}C$ and sliding tests were run in the pin-on-disk sliding configuration. The counterface was made of tool steel hardened to 55-60 HRC and finished to a surface roughness of 0.09-0.10 ${\mu}m$ Ra. Wear tests were run for 6 hrs at the sliding speed of 1 m/s and contact pressure of 0.65 MPa. Transfer films formed on the counterfaces during sliding were investigated using AFM and SEM. The results showed that as the transfer film became smooth and uniform, wear rate decreased. PPS+2%CuO+15%Kevlar composite showed the lowest steady state wear rate in this study and its transfer film showed the smoothest and the most uniform characteristics. The examination of worn surfaces of PPS+2%CuO composite using X-ray area scanning (dot mapping) showed back-transfer of steel counterface material to the polymer pin surface. This behavior is believed to strengthen the polymer pin surface during sliding thereby contributing to the decrease in wear rate.

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Tetrapyrazinoindoloporphyrazine Langmuir-Blodgett Films

  • Kim, Jong-Min;Jaung, Jae-Yun;Ahn, Hee-Joon
    • Macromolecular Research
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    • v.16 no.4
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    • pp.367-372
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    • 2008
  • We fabricated tetra(5-n-nonyl-8-tert-butyl-2,3-pyrazino[2,3-b]indolo)porphyrazinato copper(II) (Cu-Pc-$C_8$) Langmuir-Blodgett (LB) films. We further investigated the influence of arachidic acid (AA) as a transfer promoter, as well as the effect of dipping speed, on the deposition of the films on hydrophilic and hydrophobic substrates. In the case of pure Cu-Pc-$C_8$ LB deposition on a hydrophilic substrate, the transfer ratio was close to one for up-stroke depositions, but the previously deposited film was peeled off and re-spread onto water at down-stroke depositions. Whereas the stability of the Cu-Pc-$C_8$ LB films was not improved by AA addition on hydrophilic substrates, the deposition of Cu-Pc-$C_8$ was significantly improved by the presence of AA on a hydrophobic substrate. The AA-assisted deposition had transfer ratio of close to 1 and was essentially stable up to 10-layer depositions. Comparison of the UV-visible spectrum of a Cu-Pc-$C_8$/AA LB film with that of Cu-Pc-$C_8$/AA solution in dichloroethane revealed that the Soret and Q bands for the Cu-Pc-$C_8$/AA LB film were broadened and red-shifted due to the aggregation of phthalocyanines upon assembly in the LB film.