• 제목/요약/키워드: extraction times

검색결과 1,278건 처리시간 0.029초

Removal of diesel hydrocarbons by microwave-enhanced soil vapor extraction (Focused on Loss and Kinetic constant for Diesel Hydrocarbons)

  • 김종운;박갑성
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2004년도 총회 및 춘계학술발표회
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    • pp.223-226
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    • 2004
  • In this paper, removal of diesel hydrocarbons (C$_{10}$-C$_{22}$) for dry and moist soil was investigated so that microwave-enhanced soil vapor extraction(SVE) reduced soil treatment time and raised remediation efficiency. Kinetic constants of diesel hydrocarbons with microwave energy were 7 times on dry soil and 1580 times on moist soil as much as those of SVE process without microwave energy. The diesel removals were 67.7~78.4% for $C_{10}$ and $C_{12}$, and 0~18.5% for $C_{14}$~C$_{22}$ for dry and moist soil with SVE process only. On the other hand, dry soil with microwave-enhanced SVE process showed 89.3~99.4% removal for $C_{10}$ and $C_{12}$ and 35.6~67.0% for hydrocarbons over $C_{14}$. All hydrocarbons(C$_{10}$~C$_{22}$) studied were significantly removed (93.6~99.8%) for moist soil with microwave-enhanced SVE process. Almost all diesel hydrocarbons were usually considered as semi-volatile compounds(SVOCs). Microwave-enhanced SVE process might have a great potential for remediation of soils contaminated with SVOCs.OCs.

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피리도스티그민 정제의 함량 측정을 위한 HPLC 분석법 (Quantitative Analysis of Pyridostigmine Bromide in Tablets by HPLC)

  • 피택산;조영;석대은;차승희;정윤수
    • Journal of Pharmaceutical Investigation
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    • 제21권3호
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    • pp.171-177
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    • 1991
  • A reverse-phase, ion-pair high performance liquid chromatographic (HPLC) method for the simultaneous quantative determination of pyridostigmine and its hydrolytic product, 3-hydroxy-N-methylpyridinium (HMP), is descrihed, The assay of pyridostigmine and HMP was linear in the range of amount from 24 to 60 mg/tablet and from 2.4 to 12.0 mg/tablet, respectively, with coefficient of variation (C.V.) of 0.05-0.12% (n=7) and 0.25-0.52% (n=5), respectively, and applicable conveniently even in the case of the mixture of pyridostigmine and HMP. Meanwhile, the conventional UV method gave inaccurate results for the aged pyridostigmine tablets. In the extraction of pyridostigmine from tablets prior to be assayed by HPLC, methanol was found to be more effective than ethanol or distilled water. Multiple extraction (four times) with methanol resulted in the full recovery of pyridostigmine, whereas ethanol gave 95% recovery even after four times extraction. Based on these results. the present method would be very useful for the accurate determination of pyridostigmine in the aged pyridostigmine tablets.

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효율적인 학습규칙의 신경망 기반 독립성분분석을 이용한 영상신호의 분리 및 특징추출 (Separations and Feature Extractions for Image Signals Using Independent Component Analysis Based on Neural Networks of Efficient Learning Rule)

  • 조용현
    • 한국지능시스템학회논문지
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    • 제13권2호
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    • pp.200-208
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    • 2003
  • 본 연구에서는 효율적인 학습규칙의 신경망 기반 독립성분분석기법을 이용한 영상신호의 분리와 특징추출을 제안하였다. 제안된 학습규칙은 할선법과 모멘트를 이용한 조합형 고정점 학습알고리즘이다. 여기서 할선법은 독립성분 상호간의 정보를 최소화하기 위한 목적함수의 최적화 과정에서 요구되는 1차 미분에 따른 계산을 간략화하기 위함이고, 모멘트는 최적화 과정에서 발생하는 발진을 억제하여 보다 빠른 학습을 위함이다. 제안된 기법을 $512\times512$의 픽셀을 가지는 10개의 영상을 대상으로 임의의 혼합행렬에 따라 발생되는 혼합영상의 분리에 적용한 결과, 뉴우턴법에 기초한 기존의 알고리즘과 할선법만에 기초한 알고리즘보다 각각 우수한 분리률과 빠른 분리속도가 있음을 확인하였다. 또한 $256\times256$ 픽셀의 10개 지문상과 $480\times225$ 픽셀의 지폐영상에서 선택된 각각 10,000개의 3가지 영상패치들을 대상으로 적용한 결과, 제안된 기법은 뉴우턴법이나 할선법의 알고리즘보다도 빠른 특징추출 속도가 있음을 확인하였다. 한편 추출된 $16\times16$ 펙셀의 160개 독립성분 기저벡터 각각은 영상 각각에 포함된 공간적인 주파수 특성과 방향성을 가지는 경계 특성이 잘 드러나는 국부적인 특징들임을 확인하였다.

전탕 시간에 따른 애엽의 성분패턴 비교연구 (The Comparative Study on Compositional Pattern Analysis of Decoction of Extracted Artemisia argyi by Different Extraction Time)

  • 윤준걸;김민선;한성민;황덕상;이진무;이창훈;장준복
    • 대한한방부인과학회지
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    • 제33권2호
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    • pp.1-12
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    • 2020
  • Objectives: This study was conducted to find out the optimal extraction time for Artemisia argyi. Methods: The compositional pattern was compared with HPLC (High Performance Liquid Chromatography) and GC (Gas-Chromatography) by decocting Artemisia argyi 10, 60, 120 minutes respectively. Results: With longer extraction time, the contents of reference compounds were extracted 1.1 times more when 3,4-dicaffeoylquinic acid was extracted for 60 minutes than when extracted for 10 minutes in HPLC test, but the contents were reduced when extracted for 120 minutes compared to 60 minutes extraction time. 3,4-di-O-caffeoylquinic acid, 3,5-di-O-caffeoylquinic acid, 4,5-di-O-caffeoylquinic acid, jaceosidin, and eupatilin showed the largest yield rate when extracted for 10 minutes, and it decreased as time passed. The contents of chlorogenic acid, 3,5-dicaffeoylquinic acid, 4,5-dicaffeoylquinic acid, jaceosidin, scoparone, and eupatilin were detected only in 10 minutes extraction but not in 60 or 120 minutes extraction according to GC test. Conclusions: The results show that extraction time could affect the physicochemical characteristic or composition of Artemisia argy extracted. Thus, short extraction time could be useful for decoction of Artemisia argyi.

열수추출 및 효소처리에 따른 감귤 과피 추출물의 기능성성분 수득에 대한 연구 (A Study on the Yield of Functional Components of Citrus Peel Extracts using Optimized Hot Water Extraction and Enzymatic Hydrolysis)

  • 노정은;윤성란;임애경;김혜정;허담;김대익
    • 한국식품조리과학회지
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    • 제28권1호
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    • pp.51-55
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    • 2012
  • This study was conducted to investigate the physicochemical properties of citrus peel extracts with different hot water extraction and enzymatic hydrolysis conditions. Enzymatic hydrolysis was also employed using Viscozyme L and results were compared with that of optimized hot water extract. Hot water extraction was performed under different parameters; the sample to solvent ratio(1:20, 1:15, 1:10), extraction time(2, 4 hrs), extraction temperature(85, $95^{\circ}C$) and enzymatic hydrolysis(0, 1%) and the subsequent extracts were used for determining their physicochemical properties, such as total yield, total phenolics, total flavonoids, and electron donating ability (EDA). With the increase in the sample to solvent ratio and extraction time, total yield, total phenolics, total flavonoids and EDA increased. But extraction temperature did not significantly affect the hot water extract. As hot water extract was hydrolyzed by the enzyme, total yield and active ingredients increased rapidly. In the result of total yield, total phenolics, total flavonoids and EDA, the activity of enzyme-treated extract was higher than those of enzyme-untreated extract. Based upon the overall hot water extraction efficiency, it was found that 20 times volume or 120 min at a time at $95^{\circ}C$ after enzyme treatment was optimal.

간접탄산염화를 위한 전기로제강슬래그 중 Ca, Fe 및 Si 성분의 초산수용액 침출 (Leaching of Ca, Fe and Si in Electric Arc Furnace Steel Slag by Aqueous Acetic acid Solution for Indirect Carbonation)

  • 윤기병
    • 자원리싸이클링
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    • 제26권1호
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    • pp.37-42
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    • 2017
  • 이산화탄소 저감을 위한 유효한 방법 중의 하나로 칼슘규산염 광물의 간접탄산염화 공정이 보고되고 있다. 이 공정은 염산, 질산 등의 산에 의하여 칼슘규산염으로부터 칼슘성분을 침출하는 단계와 이산화탄소에 의한 침출용액의 탄산염화 단계의 두 과정으로 구성된다. 침출용매로 초산수용액을 사용하는 경우에는 침출용액을 이산화탄소로 탄산염화 하는 과정에서 초산이 재생성 되어 침출단계로 순환되어 침출용매로 재사용될 수 있다. 제철 및 제강슬래그와 같은 산업부산물은 칼슘규산염을 많이 함유하고 있어 간접탄산염화공정의 원료로 사용될 수 있다. 본 연구에서는 초산수용액에 의한 국내 전기로제강슬래그의 침출효율을 조사하기 위하여, 초산수용액 농도, 침출온도 및 침출시간 등의 침출조건 변화에 따른 침출실험을 수행하였다.

추출조건이 홍삼엑기스의 지방과 유리지방당 조성에 미치는 영향 (Effect of the Extracting Condition on the Crude Fat and Free Fatty Acids of Red Ginseng Extract)

  • 성형순;윤석권
    • Journal of Ginseng Research
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    • 제9권2호
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    • pp.179-185
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    • 1985
  • The effect of temperature and ethanol concentration on lipids yield and free fatty acids were investigated during 1-5 times of 8 hours extraction. The crude lipids recovered was generally increased as the ethanol concentration increased while it was decreased at higher extraction temperature. Fatty acids composition in free fatty acids showed linoleum and plasmatic acids to be the major fatty acids, accounting 60% of 16 fatty acids identified. Fatty acids pattern was little affected by the changes in ethanol concentration while increase in temperature resulted significant changes in fatty acids composition.

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한글 인식에서 자소 추출에 관한 연구 (A Study on Algorithm of Phonemes Extraction in Korean Character Pattern Recognition)

  • 정영화;김은진;김정선
    • 한국통신학회:학술대회논문집
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    • 한국통신학회 1985년도 추계학술발표회 논문집
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    • pp.109-112
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    • 1985
  • This paper proposes a algorithm of phonemes extraction in korean character pattern recognition. The phonemes are classified into the patterns which are separable and connected with each other. The former is extracted by means of pattern matching in consideration of topological structure of ponemes and direction of stroke sequentially. The latter is extracted by means of index and window algorithm which are performed by a 3$\times$3 sequential local operation in the thinned character pattern.

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역추출과 PAR법에 의한 수질중 미량 수은의 비색정량에 관한 연구 (Colorimetric Determination of Trace Mercury(II) in Water by Back Extraction and PAR)

  • 정창웅
    • 한국환경보건학회지
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    • 제21권3호
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    • pp.96-101
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    • 1995
  • A selective and highly sensitive spectrophotometric measurements have been developed for the determination of trace mercury(II) with thiosulfate and PAR. Hg(II)-thiosulfate complex was extracted into high molecular alkylamine such as quaternary ammonium salt and back extracted into 1 M-HCl solution. The Hg(II)-PAR complex has maximum absorbance at 499 nm and obeys Beer's law in the range of 0.04~1.0 $\mu g/mL$ of mercury(II). The molar absorptivity and Sandell's sensitivity are $6.27\times 10^4 L.mole^{-1} cm^{-1}$ and $3.2\times 10^{-3}g/cm^2$ respectively.

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신경 회로망을 이용한 자궁 경부 세포진 영상의 영역 분할에 관한 연구 (A Study on Segmentation of Uterine Cervical Pap-Smears Images Using Neural Networks)

  • 김선아;김백섭
    • 대한의용생체공학회:의공학회지
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    • 제22권3호
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    • pp.231-239
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    • 2001
  • This paper proposes a region segmenting method for the Pap-smear image. The proposed method uses a pixel classifier based on neural network, which consists of four stages : preprocessing, feature extraction, region segmentation and postprocessing. In the preprocessing stage, brightness value is normalized by histogram stretching. In the feature extraction stage, total 36 features are extracted from $3{\times}3$ or $5{\times}5$ window. In the region segmentation stage, each pixel which is associated with 36 features, is classified into 3 groups : nucleus, cytoplasm and background. The backpropagation network is used for classification. In the postprocessing stage, the pixel, which have been rejected by the above classifier, are re-classified by the relaxation algorithm. It has been shown experimentally that the proposed method finds the nucleus region accurately and it can find the cytoplasm region too.

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