• Title/Summary/Keyword: extraction times

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Antioxidative Activity of Ethanol Extraction Fraction from the Korean Red Tail Ginseng (홍미삼 에탄올 추출분획의 항산화 활성)

  • Lee, Jong-Won;Do, Jae-Ho
    • Korean Journal of Food Science and Technology
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    • v.33 no.4
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    • pp.497-500
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    • 2001
  • The purpose of this study was to investigate the extraction method and antioxidative activities of phenolic compounds from Korean red tail ginseng. Antioxidative activities of red tail ginseng were evaluated with its ability to donate hydrogen to DPPH, and to inhibit the oxidation of linoleic acid and LDL induced by $H_2O_2$ and $FeCl_2$, respectivly by measuring the MDA formation. Total phenolic compounds expressed as % caffeic acid were 0.80%, 0.12%, 0.06%, 0.03%, 0.01% when red tail ginseng was consecutively extracted with 60% ethanol for 5 times, most of the phenolic compounds was recovered in the extract obtained after 3 times of extraction. The extraction efficacy of 60% ethanol was superior to that of water in extraction phenolic compounds, and the efficacy did not change after evaporating the extract followed by dissolving with water. 60% ethanol extract of red tail ginseng had weak ability to donate hydrogen to DPPH. MDA determination showed the antioxidative effect with inhibition ratio of 72.23% on linoleic acid oxidation by addition of red tail ginseng extract at the concentration of 1,500 ppm. 22.52% of LDL oxidation was inhibited by addition of 250 ppm.

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Quality Characteristics of Omija (Schizandra chinensis) Extracts with Various Water Types (물의 종류에 따른 오미자 추출액의 이화학적 품질특성)

  • Lee, Sung-Ho
    • The Korean Journal of Food And Nutrition
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    • v.26 no.4
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    • pp.706-712
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    • 2013
  • This is the basic study on the extraction characteristics of Omija (Schizandra chinensis) for juices of Korean traditional foods. Extraction is being performed as 25 times of the solvent ratio at room temperature and at $65^{\circ}C$ with deionized water, tap water and Cheong-song mineral water which have high contents of Ca and Mg. The overall good results of the extraction conditions are calculated from the values of L (Lightness), redness (a), yellowness (b), soluble solids content, acidity, pH levels and the DPPH radical scavenging activity by using the electron donating ability (EDA). The results are as follows: 12 hours of room temperature and 6 hours at $65^{\circ}C$ were good extraction times. The Cheong-song mineral water at $65^{\circ}C$ is available for rapid extractions when compared to deionized water and tap water. A longer extraction time shows lower values of acidity but increasing values of soluble solids content and DPPH radical scavenging activity when using the electron donating ability. The best sequences for the extractions are Cheong-song mineral water followed by tap water and distilled water after overall consideration.

Immune Activity of Lithospermum erythrorhizon Extracted by Extreme Low Temperature Extraction Process (극한 저온 추출 공정을 처리한 지치의 면역활성)

  • Seo, Yong Chang;Kim, Ji Seon;Kim, Young Ock;Kim, Jin Chul;Lee, Hyeon Yong
    • Korean Journal of Medicinal Crop Science
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    • v.21 no.2
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    • pp.105-111
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    • 2013
  • This study was performed to investigate the enhancement of immunomodulatory activities of Lithospermum erythrorhizon by extreme process. The extracts are WE100 (water extract for 24 hours at $100^{\circ}C$), WE80 (water extract for 24 hours at $80^{\circ}C$), EE (70% ethyl alcohol extract for 24 hours at $80^{\circ}C$) and EPE (extreme process for 30 minutes at $25^{\circ}C$, 500 MPa after 70% ethyl alcohol extracts for 3 hours at 40, 50, $60^{\circ}C$). Extraction yield was increased up to 5~10% by extreme process, compare to the normal extraction such as water solvent extraction, 70% ethyl alcohol solvent extraction. The cytotoxicity of the extracts was showed in the range of 12.68~15.89% at $1.0mg/m{\ell}$ for human lung cell (HEL299). The EPE40 was showed the lowest cytotoxicity 12.68%. The EPE60 extracted by extreme process increased the growth of human B and T cells up to $12.12{\times}10^4\;cells/m{\ell}$ and $14.88{\times}10^4\;cells/m{\ell}$, respectively and the EPE60 greatly increased the cytokine secretion of both IL-6 and TNF-${\alpha}$. The extracts by extreme process also exhibited higher levels of nitric oxide production from macrophages than the lipopolysaccaharides. It can be concluded that Lithospermum erythrorhizon has immune activities and The extreme process could increase higher immune activities possibly by immunomodulatory compounds.

Chemical influences of the rhizomes of Atractylodes japonica, A. macrocephala, or A. chinensis on the extraction efficiencies of chemical compounds in the roots and rhizomes of Glycyrrhiza uralensis during hot-water extraction (열수추출 과정에서 삽주, 백출(큰꽃삽주), 북창출 배합이 감초 성분의 추출률에 미치는 영향)

  • Kim, Jung-Hoon
    • The Korea Journal of Herbology
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    • v.34 no.5
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    • pp.39-47
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    • 2019
  • Objectives : When herbal medicines are extracted together, they may interact with each other, leading to change of chemical characteristics. This study aimed to evaluate the influence of Atractylodes rhizomes (Atractylodes japonica, A. macrocephala, and A. chinensis) on the chemical features of the roots and rhizomes of Glycyrrhiza uralensis, which is are commonly combined with herbal medicines in many herbal formulae, when they are co-decocted. Methods : Liquiritin apioside, liquiritin, ononin, and glycyrrhizin levels of G. uralensis in hot-water extracts prepared by the combination of Atractylodes rhizomes with various weight ratios (G. uralensis : Atractylodes rhizomes = 10:0, 10:5, 10:10, and 10:20) and extraction times (60, 90, and 120 min) were quantified using a HPLC-diode array detector and compared by statistical analysis. Results : The concentrations of liquiritin apioside, liquiritin, ononin, and glycyrrhizin from G. uralensis roots and rhizomes mostly reduced when co-extracted with Atractylodes rhizomes, and the addition of A. chinensis most reduced their contents between Atractylodes combination groups. A. japonica and A. macrocephala rhizomes also showed differences of liquiritin and glycyrrhizin levels at 10 g and 20 g groups of Atractylodes rhizomes. Extraction times also affected the concentrations of liquiritin, ononin, and glycyrrhizin mostly during 60 and 90 min. Conclusions : Atractylodes rhizomes might alter the chemical characteristics of G. uralensis when these herbs are co-decocted. This study provides the understanding of the chemical interactions of herbal medicines during the extraction in hot water.

Single Drop Microextraction for Analysis of Mustard Gas(HD) (수포작용제(HD) 분석을 위한 단일방울 미세농축법 연구)

  • Park, Yang-Ki;Kim, Sung-Ki;Son, Byung-Hoon;Park, Myeong-Ju
    • Journal of the Korea Institute of Military Science and Technology
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    • v.11 no.2
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    • pp.95-100
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    • 2008
  • A fast, simple, inexpensive, and reproducible sample preparation for extraction and analysis of HD in water was studied using single-drop microextraction(SDME) and GC-MS. Operation parameters, such as extraction solvent, extraction time were optimized. The optimized conditions were $1\{mu}L$ trichloroethylene and 10 min extraction time. In these conditions, about 42 times higher enrichment factor(EF) was obtained. The detection limit of HD was $1\{mu}g/L$, and the precision expressed as relative standard deviation was about 9.0%.

Efficient Capacitance Extraction Method for 3D Interconnect Models (3차원 연결선 모형의 효율적인 커패시턴스 추출 방법)

  • 김정학;성윤모;김석윤
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.41 no.11
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    • pp.53-59
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    • 2004
  • This paper proposes an efficient method for computing the 3-dimensional capacitance of complex structures. The proposed method is based on applying numerical 2-dimensional capacitance extraction formula for 3-dimensional interconnect models. This method improves the extraction efficiency 952 times while compromising the accuracy within 1.8 percentage of maximal relative error, compared with the results of Fastcap program for various 3-D models. The proposed method can be used efficiently to extract electrical parameters of on/off-chip interconnects in VLSI systems.

Effect of Extracting Conditions on Some Factors Affecting the Sugar Composition of Red Ginseng Extract (추출조건이 홍삼엑기스의 당과 유리당의 조성에 미치는 영향)

  • 성형순;김나미
    • Journal of Ginseng Research
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    • v.9 no.1
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    • pp.104-111
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    • 1985
  • The quality of concentrated red ginseng extract, which was prepared from Korean red ginseng tails, was studied with respect to the changes in the ethanol concentration in the range of 0-90% and temperature of 70-10$0^{\circ}C$ during 1-5 times of extraction. Each extraction time was taken 8 hours at given temperature. The ratio of free sugars to total sugar changed significantly with the number of extraction and ethanol concentrations. An increase in reducing sugar and free sugars and a decrease in extracted soluble starch were fond as ethanol concentration increased. Extraction temperature was found little effect on extractability of sugars and their ratios. Analysis of free sugars in red ginseng extract identified 6 frdd sugars such as rhamnose, xylose, fructose, glucose, sucrose and maltose, including sucrose to be major.

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A Study on Free-formaldehyde in the Resin Finished cotton Fabric (III) -Extraction of Free-formaldehyde in the Urea-formaldehyde Resin-finished cotton fabric- (수지가공포의 유리 Formaldehyde에 관한 연구(III) -Urea Formaldehyde 수지가공포중의 유리 Formaldehyde 추출-)

  • Cho Soon Chae;Rhie Jeon Sook;Rhee Jong Mun;Shin Sang Jin
    • Journal of the Korean Society of Clothing and Textiles
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    • v.5 no.1
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    • pp.23-26
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    • 1981
  • In this paper, the extraction mechanism of free formaldehyde in the urea formaldehyde resin finished cotton fabric is discussed. An empirical equation for formaldehyde release has been formulated. $$F=3.7\times10^{-3}\;H\;T^{2.2326}+440$$ in which, F: the amount of free formaldehyde extracted ($\mu$g/g) H: extraction time (min) T: extraction temperature ($^{\circ}C$)

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Solvent Extraction of Zinc from Strong Hydrochloric Acid Solution with Alamine336

  • Lee, Man-Seung;Nam, Sang-Ho
    • Bulletin of the Korean Chemical Society
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    • v.30 no.7
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    • pp.1526-1530
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    • 2009
  • Solvent extraction reaction of Zn(II) by Alamine336 from strong HCl solution up to 10 M was identified by analyzing the data reported in the literature. The equilibrium constant of this reaction was estimated by considering the complex formation between zinc and chloride ion. The necessary thermodynamic parameters, such as equilibrium constant for the formation of complexes and the interaction parameters, were evaluated from the thermodynamic data reported in the literature. The following solvent extraction reaction and the equilibrium constant was obtained by considering the activity coefficients of solutes present in the aqueous phase with Bromley equation. $Zn^{2+}\;2Cl^{-}\;+\;R_3NHCl_{org}\;=\;ZnCl_3R_3NH_{org},\;K_{ex}\;=\;6.33\;{\times}\;10^2$ There was a good agreement between measured and calculated distribution coefficients of Zn(II).

Effect of Extraction on Chemical Composition of Rcd Ginseng Extract (추출 회수에 따른 홍삼 extract의 성분 조성에 관한 연구)

  • 최강주;김만욱;성현순;홍순근
    • Journal of Ginseng Research
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    • v.4 no.1
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    • pp.88-95
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    • 1980
  • Red ginseng was extracted with water and analyzed for yield, saponin, pectin and other chemical composition. It was found that: (1) The total solid content in extract after 6 times of extraction was 46.8%,: including 13.6% of centrifugal residue; (2) 83.7% of total extractable solids and 86% total saponin was extracted after the initial three runs of extraction. (3) No significant changes were observed in HPLC pattern of extracted saponins over a range of extractions; (4) The ratio of centrifugal residue to total solids increased as the number of extractions increased; (5) The ratios of fat, protein, reducing sugar and pectin contents decreased with repeating extraction while those of crude fiber, total sugar and 35% alcohol insoluble residue increased when they were compared with total solids.

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