• Bulletin of the Korean Chemical Society
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• 제20권6호
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• pp.689-695
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• 1999

Supercritical fluid extraction (SFE), ultrasonic extraction (USE), and accelerated solvent extraction (ASE) were compared with the well known Soxhlet extraction for the extraction of polychlorinated biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins(PCDDs) from the XAD-2 resin which was used to adsorb PCDDs in the atmosphere. XAD-2 resin spiked with five PCDDs was chosen as a sample. The optimum conditions for the extraction of PCDDs by SFE were turned out to be the use of CO2 modified with 10% toluene at 100 ℃ and 350 atm, with 5 min static extraction followed by 20 min dynamic extraction. SFE gave a good extraction rate with good reproducibility for PCDDs ranging from 68 to 98%. The ultrasonic extraction of PCDDs from XAD-2 was investigated and compared with other extractions. A probe type method was compared with a bath type. Two extraction solvents, toluene and acetone were compared with their mixture. The use of their mixture in probe type, with 9 minutes of extraction time, was found to be the optimum condition. The average recovery of the five PCDDs for USE was 82-93%. Accelerated solvent extraction (ASE) with a liquid solvent, a new technique for sample preparation, was performed under elevated temperatures and pressures. The effect of tem-perature on the efficiency of ASE was investigated. The extraction time for a 10 g sample was less than 15 min, when the organic solvent was n-hexaneacetone mixture (1 : 1, v/v). Using ASE, the average recoveries of five PCDDs ranged from 90 to 103%. SFE, USE, and ASE were faster and less laborious than Soxhlet extraction. The former three methods required less solvent than Soxhlet extraction. SFE required no concentration of the solvent extracts. SFE and ASE failed to perform simultaneous parallel extractions because of instrumental limitations.

• 한국조리학회지
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• 제14권3호
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• pp.210-222
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• 2008

This study showed that the brown stock, which is the base of demi-glace sauce, extracted by using a high pressure heating extractor is more advantageous than that extracted by the traditional extraction method for the mass production. We compared the former with the latter in terms of minerals and free amino acids. The results of this study are summarized as follows. When mineral contents were compared, the brown stock extracted by high.pressure heating extraction showed the tendency of increase in mineral contents in proportion to heating temperature and heating time, but, from extraction temperature of 140$^{\circ}C$, the contents of K, Mg, Na and P decreased with the increase of extraction time. In addition, mineral contents in the brown stock extracted by high-pressure heating extraction were generally lower than those in brown stock extracted by the traditional extraction method. This result was produced probably because materials were added repeatedly in the traditional method. Amino acids contents in brown stock according to the extraction methods were also examined. They increased with the increase in the number of extractions in the brown stock extracted by the traditional method, and those in the brown stock extracted using a high pressure heating extractor increased with the increase in heating temperature and extraction time. The results of this study are expected to be useful as a practical material for the mass production of brown stock products.

• Journal of Radiation Protection and Research
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• 제26권1호
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• pp.1-6
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• 2001

방사성 동위원소에 오염된 토양시료에 대하여 정확하고 신속한 U 등위원소 분석법을 개발하였고 IAEA 표준시료에 적용하여 분석법의 타당성을 검증하였다. TBP 용매추출법의 단점을 보완하기 위해서 토양시료를 질산 및 불산을 사용하여 메트릭스 성분으로부터 우라늄을 완벽하게 추출하였고 이온교환수지와 TRU Spec 수지를 이용하여 우라늄 등위원소를 악티나이드 원소로부터 순수분리하였다. 크로마토 그래피 추출법을 사용하여 토양시료에서 우라늄 등위원소 화학수율은 TBP 용매추출법의 경우보다 10% 정도 증가하였다. 크로마토 그래피 추출법을 사용한 IAEA 토양시료에 분석결과는 IAEA에서 보고된 수치와 일치하였다.

• 전자공학회논문지D
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• 제35D권7호
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• pp.48-55
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• 1998

We propose a new static current source model and parameter extraction method for AlGaAs/GaAs HBT. The proposed model has 9 parameters describing internal currents and are experessed with the physically meaningful parameters.The proposed parameter extraction method uses the measured dC IV curves and does not need the gummel plt data and any optimization process. the constructed model based on the proposed method predicts the measured data well.

• KSII Transactions on Internet and Information Systems (TIIS)
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• 제12권6호
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• pp.2470-2491
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• 2018

Web-scale open information extraction (Open IE) plays an important role in NLP tasks like acquiring common-sense knowledge, learning selectional preferences and automatic text understanding. A large number of Open IE approaches have been proposed in the last decade, and the majority of these approaches are based on supervised learning or dependency parsing. In this paper, we present a novel method for web scale open information extraction, which employs cosine distance based on Google word vector as the confidence score of the extraction. The proposed method is a purely unsupervised learning algorithm without requiring any hand-labeled training data or dependency parse features. We also present the mathematically rigorous proof for the new method with Bayes Inference and Artificial Neural Network theory. It turns out that the proposed algorithm is equivalent to Maximum Likelihood Estimation of the joint probability distribution over the elements of the candidate extraction. The proof itself also theoretically suggests a typical usage of word vector for other NLP tasks. Experiments show that the distance-based method leads to further improvements over the newly presented Open IE systems on three benchmark datasets, in terms of effectiveness and efficiency.

• 인터넷정보학회논문지
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• 제6권4호
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• pp.85-92
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• 2005

본 연구에서는 연속음성에서 개별 피치펄스와 TSIUVC를 추출하는 새로운 방법을 제안하고자 한다. TSIUVC 탐색과 추출은 FIR-STREAK 필터를 사용한 개별 피치펄스와 영교차율을 사용한다. 실험결과, 개별 피치펄스의 추출률은 남자음성에서 $96{\%}$, 여자음성에서 $85{\%}$를 얻을 수 있었다. 아울러, TSIUVC 추출률은 남자 음성의 경우 $88{\%}$에서 $94.9{\%}$, 여자 음성의 경우는 $84.8{\%}$에서 $94.9{\%}$의 결과를 얻었다. 제안한 방법은 음성분석, 음성합성, 새로운 Voiced/Silence/TSIUVC의 음성부호화 방식에 활용할 수 있을 것으로 기대된다.

• 약학회지
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• 제56권3호
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• pp.145-151
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• 2012

To develop fundamental data of herbal materials with heat treatment, we studied analytical and extraction methods of benzopyrene in black ginseng and validated by HPLC analysis. Benzopyrene was successfully separated in mobile phase of acetonitrile:water (80 : 20) and detection of excitation 294 nm, emission 404 nm. The calibration curve of benzopyrene was linear over the concentration range of 1.17~37.50 ng/ml with correlation coefficient of above 0.999. The limit of detection (LOD) and quantitation (LOQ) of benzopyrene was 0.25 and 0.75 ng/ml, respectively. Hexane extraction method was used as a new extraction method for benzopyren and the efficient of extraction was over 95%. In conclusion, analytical method and extraction method were suitable for the determination of benzopyrene in the black ginseng and could be applied to fundamental study and guideline of herbal materials with heat treatment.

• Natural Product Sciences
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• 제19권3호
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• pp.236-241
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• 2013

A high-performance liquid chromatography-diode array detector (HPLC-DAD) method was established for quantitative evaluation of nine constituents of Fraxinus rhynchophylla such as four coumarins, esculin (1), fraxin (2), esculetin (3), fraxetin (4), three lignans, syringaresinol 4,4'-O-${\beta}$-diglucoside (5), pinoresinol 4-O-${\beta}$-glucoside (6), pinoresinol (9), one secoiridoid, oleuropein (7), and one coumarinolignan, cleomiscosin C (8). The preferred chromatographic condition was obtained on Phenomenex Gemini-NX (3 ${\mu}m$, C18 110A, $150{\times}4.60$ mm) and the mobile phase was composed of water and acetonitrile using a gradient elution. The wavelength was set at 220 nm. Extraction condition of these constituents in F. rhynchophylla was also optimized through extraction time, extraction solvent and extraction method using established method. From this study, extraction at $70^{\circ}C$ with the mixture of ethanol and water for more than 12 h was suggested to be good extraction condition for these constituents. Quantitation of nine constituents in different F. rhynchophylla samples was also successfully accomplished with the newly established method.

• ETRI Journal
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• 제20권3호
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• pp.272-283
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• 1998

In this paper, we propose efficient content-based image retrieval methods using the automatic extraction of the low-level visual features as image content. Two new feature extraction methods are presented. The first one os an advanced color feature extraction derived from the modification of Stricker's method. The second one is a texture feature extraction using some DCT coefficients which represent some dominant directions and gray level variations of the image. In the experiment with an image database of 200 natural images, the proposed methods show higher performance than other methods. They can be combined into an efficient hierarchical retrieval method.

• 분석과학
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• 제8권4호
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• pp.1089-1094
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• 1995

Methods for the measurement of copper(II) complexing capacity (CuCC) of natural waters by using the back-extraction of bis(benzoyl-trifluoroacetonate)copper(II) and the extraction rate of dithizonato-copper(II) complex were described. Experimental results show that the CuCC of the Kiryu river water samples from urban area were consistently larger than those from up-stream, due to a ligand which originated from human activities.