• Title/Summary/Keyword: extraction

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The Storage Property of Squid Viscera by Supercritical Carbon Dioxide Extraction

  • Lee, Min-Kyung;Yoo, Hong-Suk;Pack, Hyun-Duk;Chun, Byung-Soo
    • Journal of Marine Bioscience and Biotechnology
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    • v.2 no.1
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    • pp.55-59
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    • 2007
  • The oil and concentrated protein powder from squid viscera was extracted and recovered by a semi-batch supercritical carbon dioxide ($SCO_2$) extraction system and the degree of oxidation in the extracted oil was measured in order to compare with extracted oils using organic solvents. The degree of storage in treated squid viscera by $SCO_2$ extraction was measured in order to compare with untreated squid viscera. As results obtained, it was found that the auto-oxidation of the oils using $SCO_2$ extraction occurred very slowly compared to the oils by organic solvent extraction. And the treated squid viscera by $SCO_2$ extraction was reached the point of initial rottenness slowly than untreated squid viscera.

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Effects of Different Extraction Extraction Media and Reaction Mixtures on Photosystem II Activity of Spinach Chloroplasts (시금치 엽록체의 광계의 활성에 미치는 추출용매와 반응용액의 영향)

  • 권병규
    • Journal of Plant Biology
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    • v.19 no.4
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    • pp.95-99
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    • 1976
  • This work deals with different extraction media and reaction mixtures on photosystem II activity of Spinach chloroplasts. The photoreduction rate of ferricyanide and DPIP by intact chloroplasts which extracted with four kinds of extraction media; S-Tris-N pH 7.2, 8.0, S-Tricine-N pH 7.2, 8.0, was measured in five kinds of reaction mixtures; S-Tris-N pH 7.2, 8.0, S-Tricine-N pH 7.2, 8.0, 0.05 M-Tris pH 7.2. The extraction medium which shows the highest photoreduction rate was S-Tris-N at pH 7.2 and S-Tricine-N at pH 8.0. As to the reaciton mixture, S-Tricine-N pH 8.0 showed the highest rate. On the complex effects of extraction media and reaction mixtures, the highest photordeuction rate of Hill oxidant by intact chloroplasts was obtained by S-Tris-N pH 7.2 extraction medium and S-Tricine-N pH 8.0 reaction mixture. The second highest activity was obtained by S-Tricine-N pH 8.0 extraction medium and reaction mixture.

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Separation of Chromophoric Substance from Madder Plant under Different Extraction and Analytical Conditions (염료추출 및 분석 조건에 따른 꼭두서니의 색소성분 분리 거동)

  • ;S. Kay Obendorf
    • Journal of the Korean Society of Clothing and Textiles
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    • v.27 no.11
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    • pp.1350-1357
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    • 2003
  • This research was aimed to establish the standard extraction and analytical procedures for examining the chromophoric substance in madder root with the ultimate goal of identifying the dyes in badly faded textiles of archaeological origin. The separation temperature of gas chromatography, pH and other extraction conditions were tested. The results were as follows: The suitable separation temperature for the GC cappillary column was 50∼305$^{\circ}C$, and methanol was a good GC solvent for both standard alizarin and madder extraction. The best extraction of madder was achieved by 90 min soaking in room temperature followed by filtration and the actual heat extraction procedure. The best pH for extracting alizarin was pH 3 and above pH 5 alizarin was not detectible. Only alizarin and no purpurin was found in the extraction of the currently used madder plant.

Analysis of arsenic in contaminated soil SRM by two extraction methods: Ultrasonic extraction method and Microwave extraction method

  • Kim, Youn-Tae;Yoon, Hyeon;Shin, Mi-Young;Yoon, Cheol-Ho;Woo, Nam-Chil
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.227-230
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    • 2004
  • Two extraction techniques, Ultrasonic and Microwave extraction method, were tested for the determination of arsenic in contaminated soil SRM (Montana Soil). The extraction mixture was prepared by mixing 1 M ortho-phosphoric acid and 0.1 M ascorbic acid. This extractant was known to preserve arsenic species. The appropriate extraction time was 10 min to 20 min and the recovery rate was about 80%. A coupled system, SPE-HG-ICP-AES, was used for the determination of inorganic arsenic species. The detection limit was around 2 $\mu\textrm{g}$/1 and the linearity of calibration curve was better than $R^2$=0.99.

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A Study on the Analytical Methods Using Solid-phase Extraction for the Determination of Phenols in Water

  • Jeon, Chi-Wan;Lee, Jung-Hwa;Lee, Sang-Hak
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11a
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    • pp.135-138
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    • 2003
  • Based on solid phase extraction, gas chromatography and mass spectrometry procedure for determining phenol and its derivatives in natural water was presented. In solid phase extraction, three types of techniques using solid phase adsorption material were treated with acid and salt, and converted second portion of acetyl derivatives. Under the these condition, extraction efficiency and detection ability dependent on extraction methods were discussed. Obtained results using optimized solid phase extraction techniques showed more convenience, simplifier and lower cost than the conventional analytical methods with holding wide dynamic range and lower detection limits.

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Machine Learning Based Keyphrase Extraction: Comparing Decision Trees, Naïve Bayes, and Artificial Neural Networks

  • Sarkar, Kamal;Nasipuri, Mita;Ghose, Suranjan
    • Journal of Information Processing Systems
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    • v.8 no.4
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    • pp.693-712
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    • 2012
  • The paper presents three machine learning based keyphrase extraction methods that respectively use Decision Trees, Na$\ddot{i}$ve Bayes, and Artificial Neural Networks for keyphrase extraction. We consider keyphrases as being phrases that consist of one or more words and as representing the important concepts in a text document. The three machine learning based keyphrase extraction methods that we use for experimentation have been compared with a publicly available keyphrase extraction system called KEA. The experimental results show that the Neural Network based keyphrase extraction method outperforms two other keyphrase extraction methods that use the Decision Tree and Na$\ddot{i}$ve Bayes. The results also show that the Neural Network based method performs better than KEA.

Extraction characteristics of extraction resins containing HEH/EHP (HEH/EHP를 함유(含有)한 추출(抽出)수지의 추출특성(抽出特性))

  • Park, Kye-Sung;Kim, Joon-Soo
    • Resources Recycling
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    • v.15 no.4 s.72
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    • pp.13-18
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    • 2006
  • This study was to investigate the extraction characteristics of extraction resins containing HEH/EHP for Gadolinium solution. The experiments were carried out with the variation of equilibrium pH and initial concentration of Gd. The optimum extraction time was 90 mins on Gd extraction using resin. The extraction ratio(%) was increased by increasing equilibrium pH from pH 1.0 to 2.0. The experimentally measured amounts of Gd on resins at equilibrium agreed well with those predicted using Freundlich's isotherm.

Construction and Utilization of McCabe-Thiele Diagram for the Solvent Extraction (용매추출에서 McCabe-Thiele도의 작성 및 이용)

  • Lee, Man Seung
    • Resources Recycling
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    • v.27 no.4
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    • pp.65-69
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    • 2018
  • In solvent extraction, extraction isotherm represents the relation between the equilibrium concentration of metal in the aqueous and organic phase. McCabe-Thiele diagram on which extraction isotherm and operating line are constructed provides valuable information on the mass transfer operation. When the equilibrium constant of a solvent extraction reaction is known, the calculation method to obtain extraction isotherm was introduced. Kresmer equation by which the number of extraction stages can be calculated when the distribution coefficient is constant was introduced.

Optimization in Extraction Conditions of Carotenoids from Citrus unshiu Press Cake by Supercritical Carbon Dioxide (초임계 이산화탄소에 의한 감귤박으로부터 카로테노이드 추출 조건의 최적화)

  • Lim, Sang-Bin;Jwa, Mi-Kyung
    • Korean Journal of Food Science and Technology
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    • v.35 no.6
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    • pp.1104-1109
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    • 2003
  • Response surface methodology (RSM) was used to investigate the effects of the processing parameters on supercritical $CO_2\;(SC-CO_2)$. extraction of total carotenoids and ${\beta}$-cyptoxanthin from Citrus unshiu press cake. The parameters tested were $SC-CO_2$ pressure, dynamic extraction time, and concentration of ethanol added as the modifier to $CO_2$. Experimental data correlated well with the processing parameters (p<0.01), and there was a high statistically significant multiple regression relationship for the extraction of total carotenoids and ${\beta}-cyrptoxanthin$ ($R^2=0.9789$ and 0.9796, respectively). The optimal processing conditions were extraction pressure 33.4 and 37.3 MPa, extraction time 39.6 and 41.0 min, ethanol concentration 18.6 and 17.0% for total carotenoids and ${\beta}-cryptozanthin$, respectively. Maximum extraction yields predicted by RSM were 61.1 and 95.8% ppm, respectively. The extraction yield of total carotenoids increased asymptotically with the increase of the extraction pressure. It increased in proportion to extraction time and concentration of the cosolvent. The extraction yield of ${\beta}-cryptoxanthin$ increased with extraction pressure, extraction time, and concentration of the cosolvent. The extraction time and the concentration of the cosolvent, and the interaction between extraction time and the concentration of the cosolvent significantly affected the extraction yields of carotenoids from C. unshiu press cake.

Quantitative Extraction Analysis of Brominated Flame Retardant Substances Using Supercritical-Fluid Method for Environmental Assessment (초임계추출법을 이용한 브롬계 난연제 화합물 환경성 평가 추출효율 분석 연구)

  • Oh, Min-Kyung;Yoon, Sang-Hwa;Lee, Young-Kwan;Han, Jae-Sung;Won, Sung-Ho;Nam, Jae-Do
    • Polymer(Korea)
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    • v.32 no.1
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    • pp.13-18
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    • 2008
  • For the evaluation of brominated flame retardants included in polymeric electronic devices, we investigated the extraction methods and solvent systems for four different types of polymers of PC (polycarbonate), PP (polyropylene), PET (poly(ethylene terephthalate)) and PBT (poly(butylene terephthalate)) using different solvent systems of hexane/acetone, THF, toluene, and THF/toluene. In order to compare the extraction efficiency of different methods and solvent systems, the deca-BDE (decabromo diphenyl ether) flame retardant was included in PC, PP, PET and PBT systems and subsequently extracted by soxhlet, ultrasonic, accelerated solvent, microwave and supercritical fluid extraction methods. The amount of the extracted flame retardant was monitored to evaluate the extraction efficiency. The ultrasonic extraction method was found not to be acceptable as an extraction method for the polymer systems mainly due to a low salvation efficiency of the organic solvents. Soxhlet, accelerated solvent and microwave extraction methods exhibited over 80% of extraction efficiency for toluene. The supercritical fluid extraction method, which has been used as an extraction method for flame retardants in polymers, showed the extraction efficiencies of ca. 100% for PC and PP in the optimal extraction conditions of $60^{\circ}C$ and 120 bar.