• Journal of the Korean Applied Science and Technology
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• v.26 no.4
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• pp.379-384
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• 2009

Epoxy resin based encapsulants are widely used in semiconductor packaging applications. Epoxy resin based encapsulants are often subject to crack or delamination during the reliability test due to the thermal stress caused by high modulus nature of epoxy resins. Epoxy functional siloxanes are often added into epoxy resin to reduce the modulus so that the thermal stress can be reduced. Epoxy functional siloxanes, additives for reduced modulus, were synthesized and added into the curable epoxy resins. The modulus and the coefficient of thermal expansion (CTE) were also measured to investigate the thermal stress and to see whether the epoxy functional siloxane adversely affects the CTE or not. As a result, around 26% to 72% of thermal stress reduction was observed with no adverse effect on CTE.

• Journal of the Korean Applied Science and Technology
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• v.33 no.4
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• pp.634-646
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• 2016

In this work, modified epoxy resins which were well melted in mild solvent were synthesized and solubility assessment was carried out for synthesized epoxy resins. Bisphenol-A type, phenol novolac type and ortho-cresol novolac type epoxy resins were used and fatty acid, dodecyl phenol (DP) and toluene diisocyanate (TDI) were added for synthesis of modified epoxy resins containing fatty acid (MEFA). Composition was epoxy resin/fatty acid = 1.0/0.5 and fatty acid/DP = 0.25/0.25 by equivalent weight and twelve MEFAs were synthesized according to epoxy resins. Viscosity and solubility were measured for twelve MEFAs. As a result, solubility of MEFA was excellent for mild solvent according to increasement of contents of benzene ring, glycidyl group and carbon number of alkyl group. And physical properties were measured for each coating of paints after preparing transparent paints of MEFA to melt well in mild solvent among twelve MEFAs. As a result, they showed an optimal performance on conditions of equivalent ratio of bisphenol-A type epoxy resin/fatty acid/DP/TDI; 1.0/0.25/0.25/0.5 and equivalent ratio of phenol novolac type epoxy resin/fatty acid/DP; 1.0/0.25/0.25 for drying time, adhesion, hardness, impact resistance and alkali resistance.

• 보존과학연구
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• s.17
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• pp.39-47
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• 1996

In this research, many effects were examined by testing of adhesive intensity and accelerated weathering with synthetic resins for the conservation treatment of cracks and damaged parts of Kyound Chun-Sa10-story Pagodas, the National Treasure No. 86.It was tested with two kinds of Epoxy resins, Acrylic, Silicone resin, and five kinds of Acetics vinyl resins, and then which was ensured a successful result with Epoxy resins. According to these consequences, they are determined to treat damaged parts with Epoxy resin.

• Journal of the Korean Applied Science and Technology
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• v.24 no.4
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• pp.399-409
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• 2007

Characteristics of polyaniline anti-corrosive coatings with various primer coating resins(epoxy resin, urethane resin, and others) and top coating resins(epoxy and acrylic urethane resins) were investigated through adhesion, acid resistance, alkaline resistance, water resistance, and anti-corrosion tests. As a result, the anti-corrosive properties of the prepared coatings using polyaniline varied with the types of primer and top coating resins. In this condition, the properties of adhesion, chemical resistance, and water resistance were found to be very satisfactory when using emeraldine base (EB) of polyaniline blended with single-packaged urethane and acrylic urethane resins as the primer coatings, and using acrylic urethane resin as the top coatings. Also, the anti-corrosive function of these anti-corrosive coatings was well preserved for 1000 hr in the salt spray experiment.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.67 no.10
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• pp.1322-1329
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• 2018

In this paper, the reliability test of three kinds of epoxy resin for GIS Spacer, which is a high voltage based heavy electric machine, AC electrical treeing experiments were performed. Three types of epoxy resins, Araldite B41, CT 5531 CI and B46, have slight viscosity differences. An non-uniform electric field, E = 1149.4 kV/mm, as the needle to plate electrode, a power source with a frequency of 1 kHz was applied to the tree electrode for accelerated deterioration. The treeing phenomena of the three kinds of epoxy resin all initiated, propagated, and destroyed by the branch tree. Epoxy Resin B46 was 145 times longer than B41 and 53 times longer than CT 5531CI. I think that the choice of epoxy resin is very important in choosing high voltage heavy electric machine insulation materials.

• Transactions on Electrical and Electronic Materials
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• v.11 no.2
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• pp.89-91
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• 2010

Partial discharge (PD) resistances were investigated for three types of samples: original epoxy resins, epoxy micro composites with and without the silane processing, and mixture composites with micro and nano particles. The PD was applied to these materials using rod, gap, and plane electrodes. The partial discharge resistance found in the micro composites was better than that found in the original epoxy resin. Moreover, the mixture composites of $SiO_2$ nano and micro particles had much larger resistances than the original epoxy resin or microcomposites. It can be regarded that this excellent property was due to the fact that the nano particles have a dense structure between the micro particles.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.29 no.9
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• pp.565-570
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• 2016

In this work, the complex permittivity of epoxy resins is measured. Epoxy resins, epoxy with micro size fillers and epoxy with micro+nano alumina composites have been evaluated for dielectric properties according to frequency variation. The dielectric spectroscopy measurement and analyses are carried out in the frequency range of $10^{-2}Hz$ to 1MHz and constant to room temperature. The results of dielectric loss suggest that significant improvement in the electrical performance can be expected by using samples containing nano and micro fillers mixture when compared to materials containing only microfillers. As the result, we verified the specific characteristics of dielectric permittivity and dielectric loss namely, relative permittivity become low with improving dispersibility of nano+micro mixture composites and become rise with agglomerate of nano particles.

• Proceedings of the Korea Concrete Institute Conference
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• 1997.10a
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• pp.659-664
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• 1997

RC structures can deteriorate for many defective factors. In the repair and retrofit works of concrete, epoxy resins are widely used as repair materials. The object of this study is to investigate the material properties and durabilities of epoxy resins which are commonly used in repairing concrete. The material properties such as line-expansion modulus, viscosity, microstructure and physical parameter as well as the durabilities such as gravity change, tensile strength, elongation change were carried out.

• Journal of Conservation Science
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• v.21
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• pp.41-48
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• 2007

The resistance for atmospheric corrosion of the conventional 5 epoxy resins (Araldite rapid, Araldite AW 106, Araldite SV 427, Devcon, and CDK), those were used to restoration of the iron relics, were investigated in this study. Temperature, UV light, and water were chosen for the factors of the atmospheric corrosion. The drastic voluminous changes of the epoxy resins were found at the temperature range between $40^{\circ}C$ and $70^{\circ}C$ After UV exposure, the colors of the epoxy resins were severely changed. In case of the indoor exposure the chroma value(${\Delta}E$) of the resins were less than 2, which showed a little changes of the colors. The result of the water contact angle test was Araldite rapid>AW 106>Devcon>SV 427>CDK. Although the contact angles of the resins were reduced by UV exposure, SV 427 was stable comparatively.

• Carbon letters
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• v.11 no.2
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• pp.102-106
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• 2010

In this work, the effect of aminized multi-walled carbon nanotubes (NH-MWNTs) on the mechanical interfacial properties of epoxy nanocomposites was investigated by means of fracture toughness, critical stress intensity factor ($K_{IC}$), and impact strength testing, and their morphology was examined by scanning electron microscope (SEM). It was found that the incorporation of amine groups onto MWNTs was confirmed by the FT-IR and Raman spectra. The mechanical interfacial properties of the epoxy nanocomposites were remarkably improved with increasing the NH-MWNT content. It was probably attributed to the strong physical interaction between amine groups of NH-MWNTs and epoxide groups of epoxy resins. The SEM micrographs showed that NH-MWNTs were uniformly embed and bonded with epoxy resins, resulted in the prevention of the deformation and crack propagation in the NH-MWNTs/epoxy nanocomposites.