• 제목/요약/키워드: electron micrograph

검색결과 154건 처리시간 0.029초

Silicate계 La-아파타이트 산화물의 Bi 첨가에 따른 전기적 특성 (Electrical properties of Si-based La-apatite ceramics with addition of Bismuth)

  • 김대영;조서현;정광호;이태호;이성갑;김영곤;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2011년도 제42회 하계학술대회
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    • pp.1440-1441
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    • 2011
  • Apatite-lanthanum silicate has attracted considerable interest in recent years due to its high oxide ion conductivity, In this paper, Bi-doped samples $La_8Bi_2(SiO_4)_6O_3$ were prepared by conventional solid-state method and the influences of Bi-dopant content on calcining temperature were reported. The Samples were characterized by X-ray diffraction (XRD) and scanning electron micrograph (SEM) and impedance analysis.

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SOFC용 전극 제작 조건에 따른 전극 성능 및 구조 분석 (Effect of fabrication conditions on microstructure and performance of electrodes for SOFCs)

  • 나세윤;지영석;이윤호;조구영;차석원
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 춘계학술대회 논문집
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    • pp.307-310
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    • 2009
  • In order to develop SOFC cell performance, many kind of things were investigated. Electrode microstructure is the one of them therefore we focus on electrodes fabrication easily and efficiently. We can fabricate electrodes easily with Pt using DC magnetron sputtering and sintering. However sputtering is difficult to handle and to grow porous electrodes what we require. On the other hand sintering is much easier than sputtering to make porous and adhesive electrodes. So in this paper we deal with sintering and optimize to deposit electrodes conditions by analyzing electrode microstructure with sacnning electron microscopy(SEM) micrograph. Also, we compare electrochemical performance of cells fabricated by sputtering and sintering.

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인계화합물을 포함한 재활용 폴리우레탄폼의 난연성 (Fire Retardancy of Recycled Polyurethane Foam Containing Phosphorus Compounds)

  • 정영진
    • 한국응용과학기술학회지
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    • 제24권2호
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    • pp.182-189
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    • 2007
  • Used polyurethane was chemically degraded by treatments with flame retardants such as tris(3-chloropropyl) phosphate (TCPP), triethyl phosphate (TEP), and trimethyl phosphate (TMP). The structure of degraded products (DEP) was analyzed by FT-IR and P-NMR and it turned out to be phosphorus containing oligourethanes. Rigid polyurethane foam was produced by using the degraded products (DEP) as flame retardants. The flammability of recycled rigid polyurethane was investigated. The recycled polyurethane shows a reduced flammability over virgin polyurethane. In order to evaluate flame retardant properties of the recycled polyurethane foams with various amounts of DEP, the combustion parameters of the foam was measured by a cone calorimeter. Scanning electron micrograph of recycled PU shows the same uniform cell morphology as virgin PU.

Multiple-Bit Encodings of Bragg Photonic-structures by Using Consecutive Etch with Various Square Wave Currents

  • Lee, Bo-Yeon;Hwang, Minwoo;Cho, Hyun;Kim, Hee-Chol;Cho, Sungdong
    • 통합자연과학논문집
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    • 제4권3호
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    • pp.192-196
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    • 2011
  • New method to encode multiple photonic features of Bragg type reflector on silicon wafer has been investigated. Multiple bit encodes of distributed Bragg reflector features have been prepared by electrochemical etching of crystalline silicon by using various square wave current densities. Optical characterization of multi-encoding of distributed Bragg reflectors on porous silicon was achieved by Ocean optics 2000 spectrometer for the search of possible applications of multiple bit encoding of distributed Bragg reflectors such as multiplexed assays and chemical sensors. The morphology and cross-sectional structure of multi-encoded distributed Bragg reflectors was investigated by field emission scanning electron micrograph.

SHS화학로에 의한 SiC의 합성 (Synthesis of SiC by Self-Propagating High Temperature Synthesis Chemical Furnace)

  • 김도경;박성;조건;이형복
    • 한국세라믹학회지
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    • 제31권11호
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    • pp.1283-1292
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    • 1994
  • Ultra-fine $\beta$-SiC powders were fabricated by self-propagating high temperature synthesis process (SHS) using chemical furnace. The dependences of the C powders with different surface areas, the molar ratios of C/Si, the weight ratios of chemical fuel content, and pellet diameter-size on synthesis were investigated. Compositional and structural characterization of these powders was carried out by scanning electron micrograph and X-ray diffraction. The $\beta$-SiC powders which had C/Si mole ratio=1.05, 3 times chemical fuel contents, and pellet diameter=20 mm were optimum for synthesis efficiency. By optimizing process-variables, it is possible to fabricate $\beta$-SiC powders which have little secondary phases ($\alpha$-SiC).

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해양미생물로부터 면역증강물질 생산의 최적화

  • 최혜정;정명주;정영기
    • 한국생물공학회:학술대회논문집
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    • 한국생물공학회 2000년도 추계학술발표대회 및 bio-venture fair
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    • pp.309-312
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    • 2000
  • A halophilic bacterium was isolated from domestic marine. The bacterium was gram negative and motile. Transmission electron micrograph after cultivating for 6-, 20-, 72-, and 144 hrs showed that it was bacilli and contained intracellular granules, which were pleomorphic, larger in density by the time and considered to be PHB since they were positive on the sudan black B staining. The presence of sodium chloride was critical, because the isolated marine bacterium could not multiply and even produce any immunostimulant in the deficiency of sodium chloride. The strain produced an immunostimulant, which was investigated for the biological characteristics. The optimal conditions for the production of the immunostimulant were 1 % dextrose and 1 % yeast extract in artificial sea water for carbon and nitrogen sources, respectively. The initial pH and growth temperature for the production were 8.0 and $30^{\circ}C$ under the presence of oxigen, respectively.

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실험적 연구를 통한 모래입자 형상이 토질정수에 미치는 영향 (Experimental Study on Effects of Sand Particles Shape on Geotechnical Properties)

  • 신은철;김종인;이한진
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2006년도 춘계 학술발표회 논문집
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    • pp.896-905
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    • 2006
  • Several soil parameters such as particle characteristics, geological element, drainage and loading conditions are influenced on the shear strength of soil. The characteristics of soil particles are important factor to the shear strength of soil. However, this component is not well considered in the determination of soil strength in Korea. The particle shape of sand was analyzed by utilizing SEM(Scanning Electron Micrograph) and compared its results in terms of aspect ratio, angularity and roughness. Based on the determined soil parameters, the ultimate bearing capacity of sandy ground was estimated by using Terzaghi bearing capacity equation.

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2차원 광결정 슬랩 구조에서 광모드 특성 (Optical Mode Properties of the 2-D Photonic Crystal Slab)

  • 류한열;황정기;이용희
    • 한국광학회:학술대회논문집
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    • 한국광학회 2000년도 제11회 정기총회 및 00년 동계학술발표회 논문집
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    • pp.260-261
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    • 2000
  • 광결정(photonic crystal)은 빛의 파장 크기 정도의 격자 상수를 지닌 1차원, 2차원, 또는 3차원의 주기적인 구조이다. 광결정에는 광밴드갭(photonic bandgap)이라는 빛의 자발 방출이 억제된 진동수의 영역이 존재하는데, 이 영역을 이용하여 빛의 자발 방출을 조절하고 빛의 흐름을 제어할 수 있다. $^{[1]}$ 지난 10여년간 2차원, 3차원의 광결정 구조에 대한 연구가 많이 이루어져 왔는데, 최근에는 슬랩 도파관(slab waveguide)에 2차원 광결정을 만든 구조에 대한 연구가 활발하게 진행중이다. 이 구조는 평면 방향으로는 광밴드갭 효과로 광모드를 가둘 수 있고 수직 방향으로는 전반사를 이용하여 모드를 가둘 수 있어서 3차원적인 모드 confinement 효과를 얻을 수 있다. [그림 1]의 (a)에 air-bridge 형태의 2차원 광결정 슬랩(photonic crystal slab) 구조를 도식적으로 나타내었고, (b)에는 본 연구실에서 제작한 구조 표면의 scanning electron micrograph을 나타내었다. 현재 몇몇 연구 그룹에서 이와 같은 광결정 슬랩 구조를 이용한 반도체 레이저를 실현하는데 성공하였다.$^{[2,3]}$ (중략)

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속속이풀(Rorippa islandica Borb.)에서 분리한 순무 모자이크 바이러스 (Turnip Mosaic Virus Isolated from Rorippa islandica Borb)

  • 최준근;최국선;최장경;유병주;정태성
    • 한국식물병리학회지
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    • 제10권2호
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    • pp.136-139
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    • 1994
  • Turnip mosaic virus (TuMV) was isolated from Rorippa islandica showing mild mosaic symptom in growing field of Chinese cabbage and radish. Identification of the virus was based on host range, transmission by aphids, electron micrograph, serological reaction and hybridization detection. The virus systemically infected on Chenopodium quinoa, Nicotiana clevelandii, N. glutinosa, Brassica rapa, B. campestris subsp. pekinensis and Raphanus sativus, whereas showed local infection on C. amaranticolor, Gomphrena globosa and Tetragonia tetragonoides. The virus was transmitted by aphid (Myzus persicae). The virus particle was filamentous with 720$\times$12 nm in length, and reacted positively with an antiserum of TuMV in agar gel double duffusion test. In slot-blot hybridization using the digoxigenin(DIG)-labeled RNA probe, TuMV-RNA could be detected in sap of R. islandica infected with the virus. This is the first report of a natural infection of that virus on R. islandica.

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1%미만의 부피비를 가지는 알루미나 나노유체의 유효 열전도도 (Effective Thermal Conductivities of Al203 Nanoparticles Suspended in Water with Low Concentration less than 1 Vol. %)

  • 황교식;이병호;김준호;장석필
    • 한국항공운항학회지
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    • 제15권3호
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    • pp.1-5
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    • 2007
  • In this paper, effective thermal conductivities of water-based Al203-nanofluids with low concentration from 0.01 vol. % to 0.3 vol. % are experimentally obtained by transient hot wire method (THWM). The water-based Al203-nanofluids are manufactured by two-step method which is widely used. To examine suspension and dispersion characteristics of the water-based A1203-nanofluids, Zeta potential as well as transmission electron micrograph (TEM) is observed. We confirm the manufactured Al203-nanofluids have good suspension and dispersion. The effective thermal conductivities of the water-based Al203-nanofluids with low concentration are enhanced up to 1.64% compared with that of DI water at $21^{\circ}C$. In addition, experimental results are compared with theoretical results from Jang and Choi model.

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