• 한국염색가공학회지
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• 제35권2호
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• pp.67-81
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• 2023

This study aims to examine the possibility of using dried Dondropanax morbiferus extract as a functional dye. The leaves and branches of were extracted with distilled water and 30% ethanol, and the dyeability and functionality of silk fabrics were examined according to the color characteristics of the extract and dyeing conditions. As a result of analyzing the ultraviolet and visible light absorption spectrum of the extract, it was possible to confirm the peak of flavonoid belonging to polyphenol, and the peak of riboflavin expressing yellow color was confirmed. Adsorption equilibrium was observed at 4% dyeing concentration and 60 minutes of dyeing time, and as the temperature increased, dyeing amount increased without color change of Y-series. Aluminum mordanting also increased the yellow color. The color fastness of washing and UV irradiation was low, but the color fastness of rubbing was evaluated as relatively good. The silk fabric dyed with the distilled water extract of the leaves showed a 99.9% bacteriostatic reduction against Staphylococcus aureus and Klebsiella pneumoniae, showing excellent antibacterial properties.

• 한국염색가공학회:학술대회논문집
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• 한국염색가공학회 2008년도 제38차 학술발표대회
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• pp.117-119
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• 2008

This study was investigated for the dyeing properties of silk fabrics with Annatto Extract. The dye stuff was extracted by distilled water at 60$^{\circ}C$, 10minutes, 100:1 of bath ratio. The highest K/S value was showed at 25% dye concentration, 60minutes of dyed time at 50$^{\circ}C$ in the temperature. The post mordant conditions were better than that of pre mordant, especially post-Fe mordant showed highest K/S value. The laundering fastness was relatively good by Cu-mordant. Drying cleaning fastness appeared 4-5 grades.

• 한국의류학회지
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• 제36권4호
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• pp.412-421
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• 2012

The yerba mate that grows in the subtropical forests of South America is an evergreen tree within the Aquifoliaceae family. The yerba mate (Ilex paraguariensis) tea is habitually used as a drink in Argentina, Paraguay, Uruguay, and Southern Brazil. A wild mate tree needs about 25 years to fully grow to 15 a height of meters; however, they only grow to a height of 3-5 meters when cultivated. The leaves are 7-11 cm long and 3-5cm wide with a serrated margin. Yerba mate tea-based beverages are made from the leaves and stems of the mate tree. It is known that they contain a rich content of antioxidants and polyphenol, vitamins, amino acids, minerals and colorants. Dyeing properties of a mate plant in the silk, wool, linen and cotton fabrics were investigated. Constituents of colorant of mate tea are chlorophyll and carotinoid; in addition, it has more minerals such as (Fe, Ca, Mn, Mg, Na, K, Zn, and Cu) than green tea. Mate tea colorants showed good affinity to silk and wool fabrics. It was found that the optimum condition for dyeing was 30 minutes for dyeing time, 7 for pH of dyebath, and at a dyeing temperature of $80^{\circ}C$. The maximum absorbance wavelength (${\lambda}_{max}$) of silk and wool fabrics dyed with mate tea were at 420-440nm; however, that of linen and cotton fabrics were at 400nm. K/S values of fabrics dyed under optimum conditions were 1.979 for silk fabrics, 1.541 for wool fabrics, 0.551 for linens and 0.465 for cotton fabrics. Munsell hue values of dyed fabrics measured 3.1Y-6.4GY for silk, 1.4Y-8.3Y for wool, 5.5Y-3.7GY for linen, and 5.3Y-1.3GY for cotton. All dyed fabrics showed hues in-between greenish yellow and greenyellow. Colorfastness to rubbing, perspiration and dry-cleaning of dyed fabrics with mate tea were very good; however, the grades of colorfastness to washing of dyed linen and cotton fabrics were poor, and colorfastness to light were poor.

• 한국의류산업학회지
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• 제3권2호
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• pp.162-167
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• 2001

The dyeing powder drawn out from Cinnamoum cassia by water was concentrated. Using this powder, the silk fabrics were dyed and they measured with the K/S value, surface color, dye fastness and antimicrobial properties. The colorant of Cinnamoum cassia was proved flavonoids by FT-IR spectrum. The K/S values of silk by mordants concentration were much higher than those of high-concentration, the color yield of the silk fabrics were most efficient the premordanting method. The surface colors on the dyed fabric depended heavily upon mordants used or mordanting methods. For all cases, the value of the dyed fabric was generally dark except AI-mordant. The chroma produced clear for the unmordanting, the color difference was distinct when using the Fe-mordant. The color fastness was significantly improved when mordants were added. In the case of the light fastness, Cu-mordants improved more than 1-2 level. The Cu-mordant showed the greatest antimicrobial activity on the silk fabric.

• 한국의류산업학회지
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• 제8권4호
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• pp.476-480
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• 2006

For the purpose of application to new natural dyestuff, the dyeability of Rubus coreanus Miquel extract was analyzed. It was dyed in silk fabric according to various dye concentration, dyeing temperature, dyeing time, and dyeing repetition. And the effects of mordanting conditions were examined as color differences and color fastnesses. The maximum absorbance of Rubus coreanus Miquel extract was at 521 nm. The dyeaffinities were increased gradually as were increased dye concentration, dyeing temperature, dyeing time, and dyeing repetition. The dyeaffinity was increased at pre-mordanted condition, and color difference was increased distinctly at post mordanted condition. The hues of mordanted silk fabrics were RP, P, PB, BG where as non mordanted silk fabric was R. Lightfastness was the best at pre-Sn mordanted and the worst at Post-Al mordanted. Washing and perspiration fastnesses were improved on pre and post-Sn mordanted.

• 한국염색가공학회지
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• 제31권4호
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• pp.268-275
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• 2019

In this study, silk fabrics was dyed with sappan wood extracts fermented for 5 and 15 days, respectively, and then the dyeability, durability and the functionality of the dyed silk were investigated. Before dyeing, the silk was pretreated with chitosan-acetic acid solution or chitosan acetic acid and illite blend solution. Thereafter, UV-Visible transmittance, color, fastness, antimicrobial activity, and the FIR emissivity were analyzed. As a result, the K/S value was higher in the samples that were not pre-treated or fermented. Regardless of fermentation, the lightfastness was not significantly different. The color fastness to washing was slightly better when the samples were pretreated with chitosan-acetic acid and illite, and then dyed with extracts fermented 5 days. In addition, all samples showed high antimicrobial activity of 99.9%, regardless of the fermentation. Far-infrared emissivity was confirmed to be slightly increased by the illite and chitosan-acetic acid solution treatment compared to the untreated sample.

• 한국의류산업학회지
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• 제14권3호
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• pp.478-485
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• 2012

The dying properties of fabrics with Chaenomelis Fructus extract were studied through an investigation of the characteristic of Chaenomelis Fructus colorants, the effect of dyeing conditions (dye temperature, dyeing concentration, and times on dye uptakes), effect of mordant, effect of UV irradiation, and color change in addition, antimicrobial ability and deodorant ability were estimated. In the UV-Visible spectrum, the wavelength of maximum absorption of Chaenomelis Fructus extract was 280 nm and showed that tannin is the major pigment component. From the increase of absorbance by UV irradiation, it was assumed that catechol tannin color was developed through UV irradiation. An increased dyeing concentration resulted in a larger dye uptake. Dye uptake increased as the dyeing time and temperature increased. Chaenomelis Fructus extract showed relatively good affinity to silk than cotton. Mordant, Fe and Cu were effective to increase the dye uptake of cotton fabric in addition, the dye uptake of silk fabric mordanted with Fe and K improved. UV irradiation let the color of dyed fabrics develop regardless of the UV irradiation stage however, UV irradiation on the dyed fabric was more effective than on the extract for the color development. Dyed silk fabric showed very good antimicrobial abilities of 99.9% in addition, deodorant ability improved in the fabric dyed with Chaenomelis Fructus extract.

• 한국염색가공학회지
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• 제15권1호
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• pp.30-38
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• 2003

Research to dyeing properties of Ulmi cortex extract, silk and cotton fabrics were dyed and mordanted. Dyes were extracted from distilled water according to different pH values. The dyeability of Ulmi cortex extract were evaluated by conditions of dyeing temperature, dyeing time, dyeing pH, mordanting temperature, mordanting time, mordanting concentration and color fastness, etc. IR spectrum possessed absorption band of -OH at $3400cm^{-1},\;C-H\;at\; 2940cm^{ -1},\;aromatic\;C=C\;at\;1628cm^{-1},\;1518cm^{-1},\;C-O\;at\; 1107cm^{ -1},\;1043cm^{-1}$. And the $\labmda$max of extract appeared at 220nm and 280nm, so the substance of Ulmi cortex extract were catechin and tannin. Surface color of dyed fabrics were reddish yellow~yellow~greenish yellow. From the color fastness test, the fabrics dyed with PH 7 extract were excellent in irradiation and washing. Mordanting improved the color fastness and K/S value of dyed fabrics.

• 한국의류산업학회지
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• 제3권1호
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• pp.31-34
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• 2001

The color difference values of dyed fabrics with colorant in Eucommiae Cortex were as follows; One hour of dyeing depending on pH at $95^{\circ}C$ exhibited colors of dark brown, light brown, light beige and grey. The colors of wool, nylon and silk was darkest brown at pH 3 but light brown or yellow as pH increased. In all dyed fabrics the color was changed to darker brown as time prolonged, however; there was no further color change and value and chroma of wool declined. At pH 3, the increase in temperature turned colors of all dyed fabrics into dark brown from light yellow. As the result of repetitive dyeing, colors of all dyed fabrics gradually turned into darker brown. The methods of mordant resulted in color changes between light yellow and dark brown without various color changes.

• 한국의류학회지
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• 제37권3호
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• pp.413-423
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• 2013

Chlorophyll is an abundant pigment found in all green plants, algae, and cyanobacteria. This study uses methanol, acetone and water to extract spinach and mate powders in order to examine the possibility of dyeing animal fibers with chlorophyll without chemical alteration. It was shown that methanol extracts of spinach and mate powders can be effectively used to dye wool and silk fabrics if the extract is mixed with water by methanol:water 65:35 v/v. Compared to methanol extract, the acetone extract showed lower chlorophyll yield and lower dye uptake. Water was not an appropriate solvent for chlorophyll extraction and dyeing. Spinach powder showed a higher dye uptake than mate powder due to the higher chlorophyll content than mate powder. It is possible that the chlorophyll dyeing of wool and silk fabrics is due to the hydrogen bonding between the hydroxy amino acids in fiber and the carbonyl groups of chlorophyll. These carbonyl groups are on the heterocyclic ring and the methyl and ethyl side chains of chlorophyll.