• 제목/요약/키워드: drying strain

검색결과 131건 처리시간 0.028초

분무건조 및 대기 플라즈마 용사에 의한 지르코니아 열차폐 코팅재의 제조 및 평가 (Fabrication and Characterization of Zirconia Thermal Barrier Coatings by Spray Drying and Atmospheric Plasma Spraying)

  • 김철;허용석;김태우;이기성
    • 한국세라믹학회지
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    • 제50권5호
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    • pp.326-332
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    • 2013
  • In this study, we prepared yttria stabilized zirconia granules for thermal barrier coatings using a spray drying process. First, we characterized the properties of granules such as flow rate and packing density for utilizing the air plasma spray process. The flow rate and packing density data showed 0.732 g/sec and 2.14 $g/cm^3$, respectively, when we used larger and denser particles, which are better than hollow granules or smaller spherical granules. Second, we chose larger, spherical granules fabricated in alcohol solvent as starting powders and sprayed it on the bondcoat/nimonic alloy by an atmospheric plasma spray process varying the process parameters, the feeding rate, gun speed and spray distance. Finally, we evaluated representative thermal and mechanical characteristics. The thermal expansion coefficients of the coatings were $11{\sim}12.7{\times}10^{-6}/^{\circ}C$ and the indentation stress measured was 2.5 GPa at 0.15 of indentation strain.

Salmonella thphi Ty21a의 동결 건조와 안정성 (The lyophilization and stability of Salmonella typhi Ty21a)

  • 김세란;박동우;전홍렬;김희준;한성순;김기호;김홍진
    • 약학회지
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    • 제43권6호
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    • pp.793-797
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    • 1999
  • Salmonella typhi Ty21a is an attenuated strain of S. typhimurium and used for oral typhoid vaccine. In an attempt to increase the stability of Ty21a manufacturing typhoid vaccine, we studied about the stability of freeze-dried Th21a including additives at various temperature conditions. In order to investigate the freeze-drying rate of Ty21a according to various absorbance, we lyophilized Ty21a by using 8% sucrose as a stabilizer. The optimal freeze-drying rate of Ty21a was appeared when OD (optical density) value of the growth was between 2.5 and 3.0. To investigate the stability of Ty21a at various temperature, the viability was measured after storaging the freeze-dried Ty21a at the room temperature, cold and freezing condition for 1 week. The viability of Ty21a in cold and freezing storage condition was 5 times more stable than in room temperature. To search the most stable additives for the freeze-dried Ty21a, the viability of Ty21a including additives at the various storage condition was estimated. Mannitol and loctose were the most stable additives. Theses results suggest that the OD value of Ty21a growth, low temperature, mannitol and lactose are important factors for the optimal freeze-drying rate, the stable storage and the most stable additives, respectively.

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A Field Study to Investigate Moisture Loss from Early-Age Concrete Pavements

  • Jeong Jin-Hoon;Choi Koil
    • 콘크리트학회논문집
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    • 제16권5호
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    • pp.725-731
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    • 2004
  • A field test program was conducted for the newly placed concrete pavement of US Interstate Highway 10 between March 26th and 28th, 2003. The test section was located between Van Horn and Sierra Blanca in Hudspeth County approximately 130 km east of El Paso, Texas. The main objective of the test was collecting moisture-related data to validate the models of effective curing thickness, evaporation rate, and moisture-based maturity. Effect of moisture loss on drying shrinkage strain was studied using additional test instrumentation.

Mechanical Properties of Carbon-Fiber Reinforced Polymer-Impregnated Cement Composites

  • Park, Seung-Bum;Yoon, Eui-Sik
    • KCI Concrete Journal
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    • 제11권3호
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    • pp.65-77
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    • 1999
  • A portland cement was reinforced by incorporating carbon fiber(CF), silica powder, and impregnating the pores with styrene monomers which were polymerized in situ. The effects of type, length, and volume loading of CF, mixing conditions, curing time and, curing conditions on mechanical behavior as well as freeze-thaw resistance and longer term stability of the carbon-fiber reinforced cement composites (CFRC) were investigated. The composite Paste exhibited a decrease in flow values linearly as the CF volume loadings increased. Tensile, compressive, and flexural strengths all generally increased as the CF loadings in the composite increased. Compressive strength decreased at CF loadings above approx. 3% in CFRC having no impregnated polymers due to the increase in porosity caused by the fibers. However, the polymer impregnation of CFRC improved all the strength values as compared with CFRC having no Polymer impregnation. Tensile stress-strain curves showed that polymer impregnation decreased the fracture energy of CFRC. Polymer impregnation clearly showed improvements in freeze-thaw resistance and drying shrinkage when compared with CFRC having no impregnated polymers.

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무작위 격자 모델을 이용한 파이버 보강 콘크리트의 건조수축 균열 거동 해석 (Simulation of Cracking Behavior Induced by Drying Shrinkage in Fiber Reinforced Concrete Using Irregular Lattice Model)

  • 김근휘;박종민;;임윤묵
    • 대한토목학회논문집
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    • 제30권4A호
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    • pp.353-359
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    • 2010
  • 시멘트계 기질을 사용하는 복합재료는 재료 양생 과정에서 발생하는 건조수축 균열에 취약하다. 본 연구에서는 파이버 보강 콘크리트의 건조수축에 의한 파괴 거동을 시뮬레이션 하고, 파이버의 조건이 균열 특성에 미치는 영향에 대해 분석한다. 수치 해석 모델은 무작위 격자 형태의 기하학적 구조를 공유하는 관로 요소와 rigid-body-spring 요소로 구성되는데, 각 요소가 담당하는 비역학적-역학적 거동의 커플링에 의해 건조수축이 표현된다. 파이버 보강을 모델링하기 위해 rigid-bodyspring network 내부의 semi-discrete 파이버 요소를 적용하였다. KS F 2424 자유 건조수축 실험을 해석하고 시간에 따른 건조수축 변형률 변화를 비교함으로써 재료의 건조수축 관련 계수들을 산정한다. 다음으로 여러 파이버 혼입률에 대해 KS F 2595 구속 건조수축 실험을 시뮬레이션 하고 균열 발생 일자를 선행 실험 결과와 비교하여 해석 모델의 타당성을 검증한다. 또한, 파이버의 길이와 표면 형태를 변화시켜 건조수축 균열 해석을 수행하고 최대 균열 폭을 측정하여 시뮬레이션에서 나타나는 균열 제어 효과를 판단한다.

도축 폐혈액 단백질을 이용한 Probiotics생산에서의 동결건조 조건 (Optimization of Freeze-drying Conditions for Probiotics Production with Animal Blood Proteins Added Medium.)

  • 현창기;신현길
    • 한국미생물·생명공학회지
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    • 제26권3호
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    • pp.200-205
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    • 1998
  • 본 연구는 도축 폐기물인 가축혈액의 이용을 위해 사료첨가제로서 혈분 성분이 함유된 유산균 probiotics의 생산을 목적으로 하여 수행되었다. 혈액으로부터 얻은 혈장을 질소원으로 이용한 BBPB 배지에, 시판 중인 미생물 사료첨가제로부터 분리된 probiotics용 Lactobacillus sp.를 배양하여 대조구인 MRS배지의 74%에 이르는 높은 생균수를 얻을 수 있었다. 얻어진 배양액의 동결 건조는 배양시간, 배양액의 pH보정, 배양액의 농축, 급속동결 등의 조건에 의해 균체의 생존율이 영향을 받았으며, 24시간 배양한 배양액을 pH 6.4로 보정한 뒤 10배로 농축하여 -5$0^{\circ}C$에서 3시간 동안 동결한 후 건조하는 조건으로 최적화되었다. BBPB 배지에 잔여하는 혈장 단백질 성분은 유산균의 동결건조 안정화 효과도 가지고 있는 것으로 나타났고 그 수준은 MRS와 유사하였다. 제제화를 위한 동결건조 안정제로는 Sucrose가 높은 효과를 나타내었고 10%첨가시 48.3%의 생존율로 $3.0{\times}^{10}$ CFU/g의 유산균 제제를 얻을 수 있었다. 본 연구에서의 동결건조조건을 이용하면 도축 폐혈액을 이용한 problotics의 산업적 생산이 가능할 것으로 사료된다.

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콘크리트의 건조수축과 수리에너지의 상관관계 (A Relationship between Drying Shrinkage and Water Potential)

  • 한만엽
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1992년도 가을 학술발표회 논문집
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    • pp.58-61
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    • 1992
  • Water potential which controls miosture movement in concrete is a kind of stress which causes concrete shrinks or expands. Therefore, there is a straightforward relationship between the water potential and the shrinkage strain. Explicit equations which show the relationships between the two parameters were derived through rational process. Two micro mechanisms among three shrinkage mechanisms were considered in the theory. Thermocouple psychrometer were embedded in a concrete slab to measure the water potential and also to find a correlation with the shrinkage. The test results prove the validity of the theory, and show the way to utilize the delived equations.

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Development of a New Gut-targeted Oral Typhoid Vaccine Ty21a

  • Kim, Hong-Jin
    • 대한약학회:학술대회논문집
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    • 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2
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    • pp.153-154
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    • 2002
  • Salmonella typhi Ty21a is an attenuated strain of S. typhimurium and used for oral typhoid vaccine. In an attempt to increase the stability of Ty21a manufacturing typhoid vaccine, the stability of freeze-dried Ty21a including additives at various temperature conditions was studied. In order to investigate the freeze-drying rate of Ty21a according to various absorbance, Ty21a was lyophilized by using 8% sucrose as a stabilizer. (omitted)

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동물의 장에서 분리한 Enterococcus sp.의 특성 및 분말화

  • 박종진;변정수;조윤경;홍승서;이현수
    • 한국미생물·생명공학회지
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    • 제24권4호
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    • pp.393-398
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    • 1996
  • In order to develop a lactic acid bacterial powder which can be used as a probiotic for human and animal, a lactic acid bacteria which has high resistance against low pH and ox-gall, and shows a good growth inhibition against E. coli, was isolated from an animal intestine and characterized. The isolated strain was identified as Enterococcus faecium. It had more than 90% of survival at low pH for 2 hours and almost 100% of survival in the presence of 0.3% ox-gall. When co-cultured with E. coli in MRS broth, all of the E. coli cells were killed within 24 hours. The final powdered product of the isolated strain was manufactured after a freeze drying process using an industrial media, and then checked its stability. Its storage stability was 80% for 11 months at 18$\circ$C.

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횡구속 재료변화에 따른 고성능 콘크리트의 역학적 특성에 관한 실험적 연구 (An Experimental Study on the Mechanical Properties of High Performance Concrete with Material for Lateral Confinement)

  • 김은호;정덕우;홍상희;윤기원;한천구
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2002년도 봄 학술발표회 논문집
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    • pp.563-568
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    • 2002
  • This paper is a fundamental study on the mechanical properties of the high performance concrete confined with metal lath, glass and carbon fiber laterally. According to the results, it shows that the compressive strength increases by 9%, 8% and 6% in metal lath carbon fiber and glass fiber in case of W/B 30% respectively. In case of W/B 30% and 40%, flecxural strength shows largely in order of carbon fiber, metal lath, glass fiber. In strain-stress curve with the kinds of material for lateral confinement, while brittleness failure occurs in plain concrete just after maximum load, it is improved in some degree in confined concrete due to increase of the strain by increase of toughness. But, elastic modulus shows the similar tendency between confined concrete and plain concrete. Length change ratio by drying shrinkage shows little a bit in order of carbon fiber, glass fiber and metal lath due to confinement.

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