• Title/Summary/Keyword: drying agents

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Phytase Production by Rhizopus microsporus var. microsporus Biofilm: Characterization of Enzymatic Activity After Spray Drying in Presence of Carbohydrates and Nonconventional Adjuvants

  • Sato, Vanessa Sayuri;Jorge, Joao Atilio;Oliveira, Wanderley Pereira;Souza, Claudia Regina Fernandes;Guimaraes, Luis Henrique Souza
    • Journal of Microbiology and Biotechnology
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    • v.24 no.2
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    • pp.177-187
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    • 2014
  • Microbial phytases are enzymes with biotechnological interest for the feed industry. In this article, the effect of spray-drying conditions on the stability and activity of extracellular phytase produced by R. microsporus var. microsporus biofilm is described. The phytase was spray-dried in the presence of starch, corn meal (> $150{\mu}m$), soy bean meal (SB), corn meal (< $150{\mu}m$) (CM), and maltodextrin as drying adjuvants. The residual enzyme activity after drying ranged from 10.7% to 60.4%, with SB and CM standing out as stabilizing agents. Water concentration and residual enzyme activity were determined in obtained powders as a function of the drying condition. When exposed to different pH values, the SB and CM products were stable, with residual activity above 50% in the pH range from 4.5 to 8.5 for 60 min. The use of CM as drying adjuvant promoted the best retention of enzymatic activity compared with SB. Spray drying of the R. microsporus var. microsporus phytase using different drying adjuvants showed interesting results, being quite feasible with regards their biotechnological applications, especially for poultry diets.

Durable Water and Oil Repellent Finish of Wool Fabric(I) (양모직물의 내구성 발수 및 발유가공(I))

  • 나도춘;정순량;박병기;정경락
    • Textile Coloration and Finishing
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    • v.10 no.1
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    • pp.33-37
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    • 1998
  • It is rather important in the water and oil repellent finishing for wool fabric what kind of water-repellent agents will be used. In many cases, Fluorocarbon-based water-repellent agents(eg.Oleophobol-S), the surface tensions of which very low, were recom-mended on account of good water and oil repellencies. In repellent finishing, fabrics were padded in a bath which contained aqueous solution of water-repellent agents, and wetting agents, followed by drying and curing. The most suitable treating condition for excellent repellency was as follows Fabrics were padded at liquor pick-up ratio of 50%, with aqueous solution which contained $30g/\ell$ of water-repellent agents, and $40g/\ell$ of wetting agents. And the padded fabrics were dried at $110^\circ{C}$ for 1 minute, and cured at $160^\circ{C}$ for 2 minutes. For the fabrics, water and oil repellencies and durability to repeated dry-cleanings are observed.

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Preparation and Evaluation of Solid lipid Microspheres Containing Cyclosporine A (사이클로스포린을 함유한 고형 지질미립구의 제조와 평가)

  • 양수근;박준상;최영욱
    • YAKHAK HOEJI
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    • v.39 no.5
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    • pp.487-494
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    • 1995
  • Solid lipid microspheres (SLMs) were prepared using various lipids and solidifying agents, in order to enhance the gastrointestinal absorption of Cyclosporine A (Cs A) which is a practically water-insoluble drug with low systemic bioavailability. Egg lecithin and HCO-60 (polyoxyethylated 60 mol, hydrogenated castor oil) were used as lipids. Stearic acid and stearyl alcohol were used as solidifying agents. Emulsion concentrates containing Cs A were prepared by mixing the melted lipid and solidifying agent with water, employing bile salts as a cosurfactant. SLMs were obtained by dispersing the warm emulsion concentrate in cold distilled water under mechanical stirring, followed by freeze drying. Physical characteristics of each SLM were investigated by particle size analysis, optical microscopy and scanning electron microscopy. Mean particle size of SLMs was in the range of 30 to 40.mu.m. The SLMs were in good appearance with spherical shape before freeze drying, but were deformed partially after freeze drying. Drug loading efficiencies of SLMs were observed as high as 80 to 90% in average. The systemic bioavailability of Cs A from different SLM formula was investigated in rats following oral administration. Cs A in whole blood was extracted and assayed by HPLC. SLMs revealed the higher bioavailabilities than the standard formula based on the marketed product. SLMs might have several advantages over standard formula for enhanced gastrointestinal absorption, controlled release properties, high loading capacity of the water-insoluble drug, and feasibility of solid dosage forms with better stability in storage.

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Effect of moisture and drying time on the bond strength of the one-step self-etching adhesive system

  • Lee, Yoon;Park, Jeong-Won
    • Restorative Dentistry and Endodontics
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    • v.37 no.3
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    • pp.155-159
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    • 2012
  • Objectives: To investigate the effect of dentin moisture degree and air-drying time on dentin-bond strength of two different one-step self-etching adhesive systems. Materials and Methods: Twenty-four human third molars were used for microtensile bond strength testing of G-Bond and Clearfil $S^3$ Bond. The dentin surface was either blot-dried or air-dried before applying these adhesive agents. After application of the adhesive agent, three different air drying times were evaluated: 1, 5, and 10 sec. Composite resin was build up to 4 mm thickness and light cured for 40 sec with 2 separate layers. Then the tooth was sectioned and trimmed to measure the microtensile bond strength using a universal testing machine. The measured bond strengths were analyzed with three-way ANOVA and regression analysis was done (p = 0.05). Results: All three factors, materials, dentin wetness and air drying time, showed significant effect on the microtensile bond strength. Clearfil $S^3$ Bond, dry dentin surface and 10 sec air drying time showed higher bond strength. Conclusions: Within the limitation of this experiment, air drying time after the application of the one-step self-etching adhesive agent was the most significant factor affecting the bond strength, followed by the material difference and dentin moisture before applying the adhesive agent.

Analysis of Microorganisms and Water Transport Properties of the Cotton Fabrics through Dehydration and Drying Process during Washing (세탁의 탈수와 건조과정 중 면직물의 수분전달특성 및 미생물 분석)

  • 최해운;박명자;차옥선
    • The Research Journal of the Costume Culture
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    • v.10 no.5
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    • pp.578-589
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    • 2002
  • The purpose of this research was to analyze the residual water retention and to determine the number and species of microorganisms from the wet cotton fabrics in dehydration and drying process during washing. The drying rates of terrycloth and interlock knit under the rainy seasons were measured according to the dehydration and hanging methods, layers of fabric and pre-treatment agents. Microorganisms were isolated from the dried terrycloth by pure culture, and were identified by Biolog system. The results are as follow: The initial water retention of fabrics after dehydration decreased in the order of dripping>centrifuge>squeezing method, which affected the drying rate. The drying rates were faster by increasing surface area of fabrics. There was no significant difference in drying rate among the fabrics pre-treated with detergent, or fabric softener, or cationic surfactants such as Cetyltrimethylammonium bromide(CTAB) and Benzalkonium chloride(BC). Puedomonas aureginosa was found in the fabrics treated with a powder-type detergent. On the other side, there was no growth of microorganism in the fabrics treated with a liquid-type detergent (containing antibacterial agent), CTAB and BC.

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The Effect of Finishing Condition on the Antimicrobial Properties of Chrome-Tanned Leather for Apparel. (의류용 크롬유혁의 가공조건에 따른 항미생물효과)

  • 심미숙
    • Textile Coloration and Finishing
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    • v.9 no.6
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    • pp.74-78
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    • 1997
  • This study was performed to obtain the basic data of the effect of antimicrobic finishing on chrome-tanned leather for apparel. This study was to examine the effect of conditions of antimicrobic finishing on content of antimicrobic agents in the specimen by analysis and on the antimicrobic activity of specimens by means of shake flask test. The optimum conditions of antimicrobic finishing were found to be ; the concentration of Si-QAC-0.5%(o.w.f.), treating time-30minute, and drying method-air drying.

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Reduction of Pesticide Residues in the Production of Red Pepper Powder

  • Chun, Mi-Hwa;Lee, Mi-Gyung
    • Food Science and Biotechnology
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    • v.15 no.1
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    • pp.57-62
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    • 2006
  • Six organophosphorus, one organochlorine, and three synthetic pyrethroid pesticides were analyzed for their residues during washing and hot-air drying of red peppers conducted in the production of powder. The residue ratio in organophosphorus pesticides was 33% in chlorpyrifos, 31 % in diazinon, 50% in methidathion, 80% in EPN, 28% in fenitrothion, and 60% in profenofos. The ratio in pyrethroids was 109% in cypermethrin, 102% in deltamethrin, and 106% in fenvalerate. That in organochlorine was 56% in ${\alpha}$-endosulfan and 90% in ${\beta}$-endosulfan. The results were greatly different between organophosphorus and pyrethroid pesticides. UV irradiation along with hot-air drying brought about a remarkable reduction of the residues, up to 70% as compared with hot-air drying only. The removal effect was most remarkable in pyrethroids, which are hardly removed by hot-air drying. The color of the pepper was not changed during UV irradiation. The use of oxidizing agents such as hydrogen peroxide or chlorine dioxide during washing did not show a remarkable removal of residues. The residue ratio was not affected whether the pesticide is contaminated artificially or naturally.

Effects of Drying Agents on the Drying and Calcination in Synthesis of Mullite by Sol-Gel Process (졸-겔법에 의한 mullite합성시 건조 첨가제가 건조 및 소성에 미치는 영향)

  • Hahm, Yeong-Min;Hong, Young-Ho;Choi, Seung-Il
    • Applied Chemistry for Engineering
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    • v.4 no.3
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    • pp.497-504
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    • 1993
  • The effect of DCCA (Drying Control Chemical Additives) on the drying of gel was investigated in order to determine an optimum drying condition of mullite precursor through sol-gel process. Aluminium sec-butoxide was synthesized from aluminium foil and then mullite powders were synthesized from Tetra-ethyl-ortho-silicate (TEOS) and the aluminium sec-butoxide. N, N-dimethyl formamide (DMF), Glycerol, 1, 4-Dioxane, and Oxalic acid were used as DCCA. Mullite powders that were calcined at 200, 900, 1100, and $1250^{\circ}C$ for 2hr were analysed by XRD, TG-DTA, FT-IR, and SEM in order to investigate structural change and characteristics of calcined powders. The results of this work showed that the drying time of gel was reduced to about half in the presence of 0.1mol DMF compared with the absence of DCCA and also calcined powders were obtained without remarkable structural change despite of the addition of DCCA.

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Quality Characteristics of Spray Drying Microparticulated Calcium after Wet-grinding (습식분쇄하여 분무건조한 초미세 분말 칼슘의 품질특성)

  • Han, Min-Woo;Youn, Kwang-Sup
    • Korean Journal of Food Science and Technology
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    • v.41 no.6
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    • pp.657-661
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    • 2009
  • Liquid microparticulated seaweed calcium was manufactured via a wet grinding process. Thereafter, different forming agents such as cyclodextrin, gum arabic, and Na-caseinate were added to the liquid calcium, which was then spray-dried to investigate the quality of the powdered calcium treatments. The moisture contents of samples were approximately 2%. It was also determined that the different kinds of forming agents did not affect the spray drying efficiency. In addition, calcium solubility was the highest in a solution of pH 2. In buffer solution and vinegar, the powdered calcium made with gum arabic showed the highest solubility among the treatments. The calcium contents of all the powdered microparticulate seaweed calcium samples were about 28%, and calcium content was not affected by the forming agents. The spray-dried calcium powder made by spray drying with gum arabic had the highest water vapor uptake, whereas the seaweed calcium was stable in terms of water adsorption. The results of SEM observations indicated that a portion of the spray-dried calcium powders were in nano-scale after wet-grinding. Among the treatments, the use of saccharides as a forming agent resulted in the most uniform particle distribution after spray-drying.

Characterization of Lightweight Earthenware Tiles using Foaming Agents

  • Lee, Won-Jun;Cho, Woo-Suk;Hwang, Kwang-Taek;Kim, Jin-Ho;Hwang, Hae-Jin;Lee, Yong-Ouk
    • Journal of the Korean Ceramic Society
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    • v.52 no.6
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    • pp.473-478
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    • 2015
  • Green bodies of earthenware tile were prepared from a mixture of earthenware tile powder and SiC as forming agents by applying a conventional process. Granule powder for tile samples was prepared using the spray drying method with commercial earthenware raw material with a quantity of SiC of 0.3 wt%. The applied pressure was $250kg{\cdot}f/m^2$ and the firing temperature was $1050-1200^{\circ}C$. The effects of the SiC particle size and sintering temperature on the open porosity and total porosity were investigated and the correlative mechanism was also discussed. While total porosity was not significantly changed by decreasing the SiC particle size, the open porosity showed a gradual decrease, which represents an increase of the closed porosity. As the sintering temperature increased, coarsening was made among the pores due to excessive oxidation. The volume shrinkage and bending strength were demonstrated for the sintered tile samples. The sintered bulk density was also measured to determine the weight reduction value.