• 제목/요약/키워드: dry aging

검색결과 161건 처리시간 0.032초

Effect of surface treatments on shear bond strength of resin composite bonded to CAD/CAM resin-ceramic hybrid materials

  • Gungor, Merve Bankoglu;Nemli, Secil Karakoca;Bal, Bilge Turhan;Unver, Senem;Dogan, Aylin
    • The Journal of Advanced Prosthodontics
    • /
    • 제8권4호
    • /
    • pp.259-266
    • /
    • 2016
  • PURPOSE. The purpose of this study was to assess the effect of surface treatments on shear bond strength of resin composite bonded to thermocycled and non-thermocycled CAD/CAM resin-ceramic hybrid materials. MATERIALS AND METHODS. 120 specimens ($10{\times}10{\times}2mm$) from each material were divided into 12 groups according to different surface treatments in combination with thermal aging procedures. Surface treatment methods were airborne-particle abrasion (abraded with 50 micron alumina particles), dry grinding (grinded with $125{\mu}m$ grain size bur), and hydrofluoric acid (9%) and silane application. According to the thermocycling procedure, the groups were assigned as non-thermocycled, thermocycled after packing composites, and thermocycled before packing composites. The average surface roughness of the non-thermocycled specimens were measured after surface treatments. After packing composites and thermocycling procedures, shear bond strength (SBS) of the specimens were tested. The results of surface roughness were statistically analyzed by 2-way Analysis of Variance (ANOVA), and SBS results were statistically analyzed by 3-way ANOVA. RESULTS. Surface roughness of GC were significantly lower than that of LU and VE (P<.05). The highest surface roughness was observed for dry grinding group, followed by airborne particle abraded group (P<.05). Comparing the materials within the same surface treatment method revealed that untreated surfaces generally showed lower SBS values. The values of untreated LU specimens showed significantly different SBS values compared to those of other surface treatment groups (P<.05). CONCLUSION. SBS was affected by surface treatments. Thermocycling did not have any effect on the SBS of the materials except acid and silane applied GC specimens, which were subjected to thermocycling before packing of the composite resin.

들깨 종자 활력 수준별 초저온 동결보존 후 발아율 및 Ascorbate Peroxidase 활성 변화 (Response of Germination Rate and Ascorbate Peroxidase Activity to Cryopreservation of Perilla (Perilla frutescens) Seeds with Variable Initial Viabilities)

  • 이영이;이명희;이정윤;이태윤;손은호;박홍재
    • 한국환경농학회지
    • /
    • 제36권4호
    • /
    • pp.256-262
    • /
    • 2017
  • 식물 종자를 비롯한 각종 유전자원을 액체질소에 저장하면 유전형질 특성의 손실 없이 장기간 보존할 수 있다. 본 연구에서 보존조건이 까다로워 단명 종자로 분류되는 들깨 종자를 초저온 동결저장 방법으로 보존할 수 있는지를 조사하였다. 수집한 들깨 품종별 종자의 초기 발아율은 40-95% 수준으로 다양하였는데, 수분함량을 3-8%로 조절한 종자를 액체질소에 처리하여도 발아율은 감소하지 않았다. 종자의 수분함량이 4-5%인 종자의 초저온 처리 후 발아율이 가장 높았으며, 초기 발아율이 낮은 품종에서는 초저온 처리에 의해 발아율이 증가하기도 했다. 인위 노화처리에 따라 종자의 발아율과 ascorbate peroxidase 활성은 감소하였으며, 품종별로 종자의 활력 저하 정도는 크게 달리 나타났다. 대조 처리 종자와 비교하였을 때, 초저온 처리과정에 발생할 수 있는 산화스트레스가 들깨 종자의 활력을 저해하지는 않을 것으로 추정되었다. 따라서 들깨 종자를 4-5% 수분함량으로 건조시켜 초저온 동결 저장하면 활력 손실 없이 장기간 보존할 수 있을 것으로 판단되며, 노화가 급속히 진행되는 품종의 경우에는 고활력 자원을 확보하거나 휴면타파 처리 후 초저온 동결 보존하는 것이 유리할 것으로 생각된다.

특정 개질아스팔트 혼합물의 노화, 균열 및 변형 특성 (Aging, Cracking and Deformation Characteristics of Selected Polymer-modified Asphalt Concretes)

  • 이학일;김현환;박남원;김광우
    • 한국도로학회논문집
    • /
    • 제10권2호
    • /
    • pp.205-219
    • /
    • 2008
  • Low-density polyethylene (LDPE)와 Styrene-butadiene-styrene (SBS)를 넣은 개질 아스팔트 혼합물은 바인더에 중량 비로 $3{\sim}6%$ 첨가하여 여러 가지 특성을 획기적으로 향상시킨 아스팔트 재료이다. 아스팔트 재료의 개질목적은 일반 혼합물의 균 열저항과 소성 변형과 같은 전형적인 약점을 향상시키기 위해서이다. 이 재료들은 많은 장점들을 가지고 있으며 플랜트 적용이 간편하고 현장적용성이 우수한 특정을 가지고 있다. 여러 해 동안의 경험을 통해 습식 개질 아스팔트와 건식 아스팔트 혼합물이 현장에서 실용화할 수 있게 발전되었다. 본 연구에서는 이를 종합적으로 평가하여 그 장단점을 일반 아스팔트 혼합물과 비교 평가하여 LDPE, SBS 개질 아스팔트 혼합물의 특성을 체계적으로 밝히는 것을 본 연구의 목적으로 한다.

  • PDF

Rotating Wheel Dip Test에 의한 에폭시 절연재료의 내트래킹성과 열화 특성 (Tracking Resistance and Aging Characteristics of Epoxy Insulating Materials by the Rotating Wheel Dip Test)

  • 조한구
    • 한국전기전자재료학회논문지
    • /
    • 제21권6호
    • /
    • pp.530-537
    • /
    • 2008
  • This paper describes the results of a study on the tracking performance of outdoor insulating materials based on the rotating wheel dip test(RWDT). And, the influence of surface degradation was evaluated through such as measurement of the flashover voltage after and before tracking test, also aspects of surface degradation using scanning electron microscopy. The time to tracking breakdown of treated filled specimen is longer than untreated filled specimen. And, after the RWDT, the surface of specimen by adding untreated filler appeared heavy erosion. It was found that the addition to surface treated filler, the better tracking resistance. In the RWDT, the breakdown specimen is not affected by the dry flashover voltage, despite the fact that the surface degradation of tracking test has different state on each specimen. This suggests that wet flashover voltage play an important role in evaluating of tracking and erosion on the surface degradation in tracking test. And, the flashover voltage of specimen under wet conditions are greatly affected by the salt concentration and degree of degradation by the RWDT Because of hydrophobicity and degree of degradation by the RWDT, the flashover voltage of treated filled specimen is higher than that of untreated filled specimen. Different types of specimen may have different hydrophobicity and their surface state under contaminated conditions may not be the same.

한지의 밀랍 및 탈랍처리 기법과 열화거동 평가 (Evaluation of the Beeswax Applying and Dewaxing Technique of Hanji, and Their Ageing Behaviors)

  • 강광호;이금자;김형진
    • 펄프종이기술
    • /
    • 제42권3호
    • /
    • pp.58-66
    • /
    • 2010
  • The Annals of beeswax applied-Joseon Dynasty have some serious damages such as cracks, brown, red or black spots, and discolorations by chemical and biological degradation, but others without any beeswax application have still been keeping good quality during over several hundred years. It would be convinced that the beeswax applied in the Annals resulted in these deteriorations. Therefore, in order to focus on the aging mechanism and conservation techniques for the beeswax-applied Annals of Joseon Dynasty, the beeswax applying and dewaxing techniques of Hanji were tried by auto bar coater with a hot plate, and by heat-pressure sensitive extracting treatments. The ageing behaviors of beeswaxed Hanji and dewaxed Hanji were investigated by measuring the changes of physical, optical, morphological, and chemical properties, through accelerated ageing treatment in dry oven at $150^{\circ}C$ during 48 hours. Consequently, the ageing actions of beeswaxed Hanji were even faster than that of Hanji. The optimum dewaxed amounts from beeswaxed Hanji was also obtained in pressure of $40\;kg_f$ under heating conditions.

Functionalized Raspberry-Like Microparticles obtained by Assembly of Nanoparticles during Electrospraying

  • Cho, Eun Chul;Hwang, Yoon Kyun;Jeong, Unyong
    • Bulletin of the Korean Chemical Society
    • /
    • 제35권6호
    • /
    • pp.1784-1788
    • /
    • 2014
  • The present study suggests a novel method to produce raspberry-like microparticles containing diverse functional materials inside. The raspberry-like microparticles were produced from a random assembly of uniformly-sized poly(methyl methacrylate) (PMMA) nanoparticles via electrospraying. The solution containing the PMMA nanoparticles were supplied through the inner nozzle and compressed air was emitted through the outer nozzle. The air supply helped fast evaporation of acetone, so it enabled copious amount of microparticles as dry powder. The microparticles were highly porous both on the surface and interiors, hence various materials with a function of UV-blocking ($TiO_2$ nanoparticles and methoxyphenyl triazine) or anti-aging (ethyl(4-(2,3-dihydro-1H-indene-5-carboxyamido) benzoate)) were loaded in large amount (17 wt % versus PMMA). The surface and interior structures of the microparticles were dependent on the characteristics of functional materials. The results clearly suggest that the process to prepare the raspberry-like microparticles can be an excellent approach to generate functional microstructures.

팔만대장경판의 세포벽 열화 (Cell Wall Deterioration of the Tripitaka Koreana Wooden Plates)

  • 박소윤;강애경;박상진
    • Journal of the Korean Wood Science and Technology
    • /
    • 제24권2호
    • /
    • pp.55-60
    • /
    • 1996
  • Tripitaka Koreana were made during Coryo Dynasty from 1236 to 1251 A.D. Buddhist scriptures were engraved on 81.340 wooden plates. Some plates were varnished with Rhus lacquer, but most of them were uncoated. Macroscopically, most of the plates appeared intact due to the storage in a well-ventilated wooden house. Because, they were irregularly used for printings with ink, it can be assumed that they were repeatedly exposed to ink-water and drying processes. The present were made to examine the changes of wood cell structures occurred during long-term aging deterioration processes in these dry archaeological wooden plates. Light, scanning and transmission electron microscopes were employed for this study. Wedge-shaped cracks and delamilations were found from the lumen side toward the compound middle lamellae and they progressed toward primary or secondary walls. A large amount of hypae in vessels and the degradation of vessel-ray pit walls by the fungal hyphae were observed. When compared to the recent wood, the birefringence of wood fibers was considerably lower or completly disappeared, suggesting the degradation of crystalline cellulose in these wood samples. The degradation of the cell wall could be also revealed the calculation of crystallinity with X-ray diffraction and the size of crystalline region was estimated.

  • PDF

Evaluation and Prediction of Corrosion Resistance of Epoxy Systems and Epoxy/Polyurethane Systems in Seawater Environment

  • Lee, Chul-Hwan;Shin, Chil-Seok;Baek, Kwang-Ki
    • Corrosion Science and Technology
    • /
    • 제5권1호
    • /
    • pp.33-38
    • /
    • 2006
  • Current coating practice requires the thickness of anti-corrosion organic coatings to be over $250{\mu}m$ for immersion parts of ships and offshore structures and the corrosion resistance of these coatings has been evaluated by destructive and qualitative analysis. Recently, Electrochemical Impedance Spectroscopy(EIS) method has been employed, as an alternative, to evaluate corrosion resistance of organic coatings. This method is characterized as being nondestructive, reproducible, and quantitative in evaluating aging of organic coatings. In this study, EIS method was adopted to quantitatively and effectively select the coating systems having optimized protective performance. Evaluations of several epoxy and epoxy/polyurethane coating systems typically used for ships and offshore structures were carried out in wet($50^{\circ}C$, $90^{\circ}C$) and dry(room temp.) environments to accelerate the degradation of the organic coatings. These results were compared with the conventional scribed(scratched) test results. The plausible prediction model for determining the remaining life-time of coating systems was also proposed based on variations of impedance data, FT-IR and $T_g$ measurements results.

GS1을 활용한 빅데이터 분석 플랫폼 기반의 스마트 소화기구 모니터링 시스템 (Smart Fire Fighting Appliances Monitoring System using GS1 based on Big Data Analytics Platform)

  • 박흠
    • 디지털산업정보학회논문지
    • /
    • 제14권4호
    • /
    • pp.57-68
    • /
    • 2018
  • This paper presents a smart firefighting appliances monitoring system based on big data analytics platform using GS1 for Smart City. Typical firefighting appliances are fire hydrant, fire extinguisher, fire alarm, sprinkler, fire engine, etc. for the fire of classes A/B/C/D/E. Among them, the dry chemical fire extinguisher have been widely supplied and 6 millions ones were replaced for the aging ones over 10 years in the past year. However, only 5% of them have been collected for recycling of chemical materials included the heavy metals of environment pollution. Therefore, we considered the trace of firefighting appliances from production to disposal for the public open service. In the paper, we suggest 1) a smart firefighting appliances system using GS1, 2) a big data analytics platform and 3) a public open service and visualization with the analyzed information, for fire extinguishers from production to disposal. It can give the information and the visualized diagrams with the analyzed data through the public open service and the free Apps.

Development of manufacturing method for the honey coating semi-dried mulberry fruit using hot air dryer

  • Kim, Hyun-bok;Kwon, O-Chul;Ju, Wan-Taek;Kim, Yong-Soon;Sung, Gyoo Byung;Hong, Seong-jin;Kim, Dooho
    • International Journal of Industrial Entomology and Biomaterials
    • /
    • 제37권2호
    • /
    • pp.63-68
    • /
    • 2018
  • Semi-dried mulberry fruit can be distributed at room temperature and maintained its chewy texture and shape. It can be used for its own itself or food materials. We develop the honey coating semi-dried mulberry fruit manufacturing method through hot air dryer. After extracting the moisture from the thawing process, honey was coated and dried. Drying time for semidried mulberry fruit was shortened by manufacturing on the day of work without going through aging process. The first the mulberry fruit juice was separated from the frozen mulberry fruit at room temperature of the laboratory or in the dryer of $60{\sim}90^{\circ}C$, then the first dried by a hot air drier at $60^{\circ}C$ for 3 to 4 h. Next, it is coated with honey, which is equivalent to 20% weight of the first dried mulberry fruit, and then the second dried at a temperature of $38^{\circ}C$ for 20 ~ 30 h. The honey coating semi-dried mulberry fruit by above method was shiny on the surface and retained its shape. The moisture content was about 15% and it was confirmed that it could be stored at room temperature.