• Title/Summary/Keyword: dispersion method

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Microstructure and Mechanical Properties of Ni3Al Matrix Composites with Fine Aluminum Oxide by PM Method

  • Han, Chang-Suk;Choi, Dong-Nyeok
    • Korean Journal of Materials Research
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    • v.28 no.9
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    • pp.495-498
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    • 2018
  • Intermetallic compound matrix composites have been expected to be established as high temperature structural components. $Ni_3Al$ is a representative intermetallic alloy, which has excellent ductility even at room temperature by adding certain alloying elements. $Ni_3Al$ matrix composites with aluminum oxide particles, which are formed by the in-situ reaction between the alloy and aluminum borate whiskers, are fabricated by a powder metallurgical method. The addition of aluminum borate whiskers disperses the synthetic aluminum oxide particles during sintering and dramatically increases the strength of the composite. The uniform dispersion of reaction synthesized aluminum oxide particles and the uniform solution of boron in the matrix seem to play an important role in the improvement in strength. There is a dramatic increase in strength with the addition of the whisker, and the maximum value is obtained at a 10 vol% addition of whisker. The $Ni_3Al$ composite with 10 vol% aluminum oxide particles $0.3{\mu}m$ in size and with 0.1 wt% boron powder fabricated by the conventional powder metallurgical process does not have such high strength because of inhomogeneous distribution of aluminum oxide particles and of boron. The tensile strength of the $Ni_3Al$ with a 10 vol% aluminum borate whisker reaches more than twice the value, 930 MPa, of the parent alloy. No third phase is observed between the aluminum oxide and the matrix.

Preparation and Characterization of Surface Energy of BPDA-BAPP Polyimide

  • Kim, Kyung-Hoe;Kim, Yong-Gwon;Kwon, Young-Hwan
    • Macromolecular Research
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    • v.17 no.6
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    • pp.388-396
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    • 2009
  • The surface properties (water sorption and repellency, adhesion) are closely related to the surface tension of polymer solids. The critical surface tension (${\gamma}_c$) and surface tension (${\gamma}_s$) of a polymer solid were estimated by the contact angle method by our quantitative imaging system. BPDA (3,3',4,4'-biphenyl tetracarboxylic dianhydride)-BAPP (1,3-Bis(4-aminophenoxy) propane) polyimide was successfully synthesized. The ${\gamma}_c$ values were analyzed by a Zisman plot, a Young-$Dupr\acute{e}$-Good-Girifalco plot, and a log ($1+cos{\theta}$) vs log ${\gamma}_L$ plot. The ${\gamma}_s$ value of BPDA-BAPE polyimide was evaluated using the geometric mean equation and our multiple regression analysis. The calculated values of ${{\gamma}_s^d$ (a dispersion component), ${{\gamma}_s^p$ (a polar component), ${{\gamma}_s^h$ (a hydrogen bonding component), and ${\gamma}_s$ were 30.79, 9.32, 0.20, and 40.31 $mN{\cdot}m^{-1}$, respectively. The ${\gamma}_s$ of BPDA-BAPP polyimide containing both a methylene group and an ether group was larger than that of the polyimide containing only a methylene group.

Influence of Allylamine Plasma Treatment Time on the Mechanical Properties of VGCF/Epoxy

  • Khuyen, Nguyen Quang;Kim, Jin-Bong;Kim, Byung-Sun;Lee, Soo
    • Advanced Composite Materials
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    • v.18 no.3
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    • pp.221-232
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    • 2009
  • The allylamine plasma treatment is used to modify the surface properties of vapor grown carbon fibers (VGCF). It is to improve the interfacial bonding between the VGCF and epoxy matrix. The allylamine plasma process was performed by batch process in a vacuum chamber, using gas injection followed by plasma discharge for the durations of 20, 40 and 60 min. The interdependence of mechanical properties on the VGCF contents, treatment time and interfacial bonding between VGCF/ep was investigated. The interfacial bonding between VGCF and epoxy matrix was observed by scanning electron microscopy (SEM) micrographs of nanocomposites fracture surfaces. The changes in the mechanical properties of VGCF/ep, such as the tensile modulus and strength were discussed. The mechanical properties of allylamine plasma treated (AAPT) VGCF/ep were compared with those of raw VGCF/ep. The tensile strength and modulus of allyamine plasma treated VGCF40 (40 min treatment)/ep demonstrated a higher value than those of other samples. The mechanical properties were increased with the allyamine plasma treatment due to the improved adhesion at VGCF/ep interface. The modification of the carbon nanofibers surface was observed by transmission electron microscopy (TEM). SEM micrographs showed an excellent dispersion of VGCF in epoxy matrix by ultrasonic method.

A Study on Intrusion Alert Redustion Method for IDS Management (침입탐지 시스템 관리를 위한 침입경보 축약기법 적용에 관한 연구)

  • Kim, Seok-Hun;Jeong, Jin-Young;Song, Jung-Gil
    • Convergence Security Journal
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    • v.5 no.4
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    • pp.1-6
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    • 2005
  • Today the malicious approach and information threat against a network system increase and, the demage about this spread to persnal user from company. The product which provides only unit security function like an infiltration detection system and an infiltration interception system reached the limits about the composition infiltration which is being turn out dispersion anger and intelligence anger Necessity of integrated security civil official is raising its head using various security product about infiltration detection, confrontation and reverse tracking of hacker. Because of the quantity to be many analysis of the event which is transmitted from the various security product and infiltration alarm, analysis is difficult. So server is becoming the charge of their side. Consequently the dissertation will research the method to axis infiltration alarm data to solve like this problem.

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Study on the Evaluation of Uncertainty for the Efficiency of 0.75[kW] Class Three Phase Induction Motor (0.75[kW]급 삼상유도전동기 효율의 불확도 평가에 관한 연구)

  • Jun, Hee-Deuk;Park, Han-Seok;Kim, Dea-Kyong;Woo, Kyung-Il
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.64 no.4
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    • pp.653-659
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    • 2015
  • In the last few years, the regulations for efficiency grade of the three phase induction motor are internationally being discussed and upgraded for the protection of environment and energy saving. So the efficiency improvement and the reliable test result are essential to determine the premium grade three phase induction motor. While a study on developing the efficiency motor is active, there is little research about the guarantee for efficiency. So in this paper, the dispersion characteristic of the efficiency is studied using uncertainty theory for the three phase induction motor to improve the reliability of efficiency. The values such as input voltage, current, speed, torque were obtained by loss separation method to evaluate the uncertainty. From the result, it was known that the important loss factor could affect the uncertainty is the stray loss.

Sensing Properties of Hydrogen Gas for the MWCNT Thin Film Sprayed on the Glass Substrate Cured with Plasma and Nitrocellulose (플라즈마 및 니트로셀롤로우스로 처리된 유리기판을 사용한 MWCNT 스프레이 박막의 수소가스 검출특성)

  • Jang, Kyung-Uk
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.4
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    • pp.290-296
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    • 2011
  • Carbon nanotubes (CNTs) have excellent electrical, chemical stability, mechanical and thermal properties. In this paper, networks of Multi-walled carbon nanotube (MWCNT) materials were investigated as a resistive gas sensors for the $H_2$ gas detection. Sensor films were fabricated by the air spray method using the multi-walled CNTs dispersion solution on the glass substrates cured with plasma and nitrocellulose. Sensors were characterized by the resistance measurements in the self-fabricated oven in order to find the optimum detection properties for the hydrogen gas molecular. The sensitivity and the linearity of the MWVNT sensors using the glass substrate cured with plasma for the $H_2$ gas concentration of 0.06~0.6 ppm are 0.013~0.097%/sec and 0.131~0.959%FS, respectively. The MWCNT film was excellent in the response for the hydrogen gas moleculars and its reaction speed was very fast, which could be using as hydrogen gas sensor. The resistance of the fabricated sensors decreases when the sensors are exposed to $H_2$ gas.

Security Method of Multimedia Data Characteristics on Video Conference System (영상회의 시스템에서 멀티미디어 데이터 특성에 따른 보안 방법)

  • Han, Kun-Hee
    • Journal of the Korea Society of Computer and Information
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    • v.10 no.4 s.36
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    • pp.143-148
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    • 2005
  • Video conference system it is various at internet and uses the reading is become accomplished. Research of like this portion synchronization of audio, the compression technique and multimedia data, supports the video conference the research of the Mbone of the IP multicast for being active. being become accomplished the multimedia service which is various an video from internet, the line speed of communication becomes high-speed anger and to follow leads is become accomplished. The video conference from opening elder brother dispersion internet network environment the problem against the image which is an image conference data and a voice security is serious and it raises its head. To sleep it presents the security method which from the video conference it follows in quality of multimedia data from the dissertation which it sees and it does.

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Percolation threshold and piezoresistive response of multi-wall carbon nanotube/cement composites

  • Nam, I.W.;Souri, H.;Lee, H.K.
    • Smart Structures and Systems
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    • v.18 no.2
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    • pp.217-231
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    • 2016
  • The present work aims to develop piezoresistive sensors of excellent piezoresistive response attributable to change in nanoscale structures of multi-wall carbon nanotube (MWNT) embedded in cement. MWNT was distributed in a cement matrix by means of polymer wrapping method in tandem with the ultrasonication process. DC conductivity of the prepared samples exhibited the electrical percolation behavior and therefore the dispersion method adopted in this study was deemed effective. The integrity of piezoresistive response of the sensors was assessed in terms of stability, the maximum electrical resistance change rate, and sensitivity. A composite sensor with MWNT 0.2 wt.% showed the lowest stability and sensitivity, while the maximum electrical resistance change rate exhibited by this sample was the highest (96 %) among others and even higher than those found in the literature. This observation was presumably attributed by the percolation threshold and the tunneling effect. As a result of the MWNT content (0.2 wt.%) of the sensor being near the percolation threshold (0.25 wt.%), MWNTs were close to each other to trigger tunneling in response of external loading. The sensor with MWNT 0.2 wt.% was able to maintain the repeatable sensing capability while sustaining a vehicular loading on road, demonstrating the feasibility in traffic flow sensing application.

Stability Studies of Biodegradable Polymersomes Prepared by Emulsion Solvent Evaporation Method

  • Lee Yu-Han;Chang Jae-Byum;Kim Hong-Kee;Park Tae-Gwan
    • Macromolecular Research
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    • v.14 no.3
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    • pp.359-364
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    • 2006
  • Di-block copolymers composed of two biocompatible polymers, poly(ethylene glycol) and poly(D,L-lactide), were synthesized by ring-opening polymerization for preparing polymer vesicles (polymersomes). Emulsion solvent evaporation method was used to fabricate the polymersomes. Scanning electron microscope (SEM) images confirmed that polymersomes have a hollow structure inside. Confocal laser microscope and optical microscope were also used to verify the hollow structure of polymersomes. Polymersomes having various sizes from several hundred nanometers to a few micrometers were fabricated. The size of the polymersomes could be readily controlled by altering the relative hydrodynamic volume fraction ratio between hydrophilic and hydrophobic blocks in the copolymer structure, and by varying the fabrication methods. They showed greatly enhanced stability with increased molecular weight of PEG. They maintained their physical and chemical structural integrities after repeated cycles of centrifugation/re-dispersion, and even after treatment with surfactants.

Optimum Design of High Speed Transmission SMF Link Using DCF (분산보상 광섬유를 이용한 초고속 단일모드 광섬유 전송링크의 최적 설계 연구)

  • 김용범
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.25 no.9B
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    • pp.1518-1526
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    • 2000
  • This paper proposes an optical transmission link design method based on an optimum compensation scheme using dispersion compensating fiber (DCF), so that high-speed long-distance optical transmission would be possible over the conventional standard single mode fiber (SMF) link. The proposed design method provides the maximized transmission distances according to the signal speeds, where the amplifier spacing and repeater spacing are optimized wit respect to self-phase modulation(SPM) due to fiber nonlinearity and amplified spontaneous emission (ASE) noises caused by optical amplifies. It is also shown that there exists an optimum input signal power range balancing the effects of ASE noise and SPM for the given amplifier spacing and repeater spacing.

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