• Maxillofacial Plastic and Reconstructive Surgery
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• v.18 no.1
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• pp.33-39
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• 1996

Human Dura mater treated by various processes was used to restore small periodontal defects, large bony defects for improvement of new bone formation, and soft tissue defects and replace the disc of TMJ, etc.. Tutoplast Dura is the solvent-preserved Human Dura mater and sterilized by gamma radiation. In our department, Tutoplast Dura was implanted in 32 patients, from 1994, 6 to 1995, 7. We implanted the Tutoplast Dura at 11 various cysts, 6 implantations, 4 fractures, 3 clefts, 2 TMJ disease, 2 maxillary sinusitis, etc.. We performed the retrospective study about the purpose of Tutoplast Dura implantation, postoperative complication and histologic examination of biopsy specimen at implant second surgery.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2001.11a
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• pp.31-32
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• 2001

Recently, many of the current development in surface modification engineering are focused on multilayered coatings. Multilayered coatings have the potential to improve the tribological and corrosion properties of tools and components. By using cathodic arc deposition, $WC-Ti_{1-x}Al_xN$ multilayers were deposited on steel substrates. Wear tests of four multiplayer coatings were performed using a ball-on-disc configuration with a linear sliding speed of 0.1m/s, 5N load. The tests were carried out at room temperature in airby employing AISI 52100 steel ball ($H_v=848N$) of 11mm in diameter. Electrochemical tests were performed using the potentiodynamic and electrochemical impedance spectroscopy (EIS) measurements. The surface morphology and topography of the wear scars of tribo-element and the corroded specimen have been determined by using scanning electron spectroscopy (SEM). Also, wear mechanism was determined by using SEM coupled with EDS. Results have showed an improved wear resistance and corrosion resistance of the $WC-Ti_{1-x}Al_xN$ coatings.

• Computers and Concrete
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• v.33 no.6
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• pp.659-670
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• 2024

The mechanical behaviour of layered concrete samples containing an internal crack was numerically studied by modelling the geo-mechanical specimens in the particle flow code in two dimensions (PFC2D). The numerical modelling software was calibrated with the experimental results of the Brazilian tensile strengths gained from the laboratory disc-type specimens. Then, the samples with the bedding layers and internal notch were numerically simulated with PFC2D under uniaxial compressive loading. In each specimen, the layers' thickness was 10 mm but the layer's inclination angle was changed to 0°, 30°, 60°, 90°, 120° and 150°. Of course, the layers'interfaces are considered to have very low strengths. The internal notch was kept at 3 cm in length however, its inclination angle was changed to 0°, 40°, 60° and 90°. Therefore, a total, of 24 numerical models were made to study the failure mechanism of the layered concrete samples. Considering these results, it has been concluded that the inclination angles of both internal crack and bedding layers affect the failure mechanism and uniaxial compressive strength of the concrete.

• The Journal of Korean Academy of Prosthodontics
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• v.47 no.1
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• pp.12-20
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• 2009

Statement of problem: When an implant is fixed, a fixture comes into contact with a tissue fluid. Adhesion of a tissue fluid to a surface of implant is various case by case. Purpose: The ultimate goal of this work is to analyze a correlation between a surface roughness and wettability of implant specimens. A measurement for wettability is performed considering 4 types of specimen implant with surface treatments different from each other to investigate the change of wettability with the elapse of time. Material and methods: Firstly, 20 specimens of titanium were prepared. The specimen were made of a commercial Titanium Grade IV with the diameter of 10 mm and the thickness of 1 mm. According to the method of surface treatment, the specimens were classified into 4 groups of 5 specimens per group. Group A: Machined Surface Group B: Anodized surface Group C: RBM (HA blasting) surface Group D: CMP (calcium methaphosphate) coating surface. Surface roughness of specimen was measured using SV-3000S4 (Mituyoto, Japan). The measurement was based on the standard of JIS1994. Sessile drop method was used to measure the wettability, which measures contact angle between implant disc and saline with the time interval of 5, 10, and 15 seconds. SPSS 11.0 was used to analyze the collected data. In order to analyze the difference of wettability and surface roughness according to implant surface treatment method. The statistical significance was tested with the confidence level of 95%. Pearson's correlation coefficient was used to evaluate the correlation of surface roughness and wettability. Results: The difference of surface roughness was statistically significant in the order of Group C ($1.69{\pm}0.26$), Group D ($1.58{\pm}0.16$), Group B ($0.78{\pm}0.14$) Group A ($0.18{\pm}0.05$). The wettability has also a statistically significant difference, which was in the order of group B ($17.70{\pm}2.66$), Group C ($27.86{\pm}4.52$), Group D ($66.28{\pm}3.70$) Group A ($70.52{\pm}8.00$). There was no difference in wettability with the passage of time. Conclusions: 1. The surface roughness was high in the order of RBM, CMP, Anodized, Machined group (P<.05). 2. The wettability was high in the order of Anodized, RBM, CMP, Machined group (P<.05). 3. There was no statistical significance in the correlation of surface roughness and wettability.

• Journal of Korean Tunnelling and Underground Space Association
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• v.16 no.2
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• pp.237-248
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• 2014

Linear cutting test is known to be very effective to determine machine parameters (i.e. thrust force and torque) and to estimate penetration rate of TBM and other operation conditions. Although the linear cutting test has significant advantages, the test is expensive and time-consuming because it requires large size specimen and high load capacity of the testing machine. Therefore, a few empirical prediction models (e.g. CSM, NTNU and QTBM) alternatively adopt laboratory index tests to estimate design parameters of TBM. This study discusses the estimation method of TBM machine parameters and disc cutter consumption using punch penetration test and Cerchar abrasion test of which the researches are rare. The cutter forces and cutter consumption can be estimated by the empirical models derived from the relationship between laboratory test result with field data and linear cutting test data. In addition, the estimation process was programmed through which the design parameters of TBM (e.g. thrust, torque, penetration rate, and cutter consumption) are automatically estimated using laboratory test results.

• Applied Chemistry for Engineering
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• v.23 no.6
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• pp.534-538
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• 2012

$Na^+$-beta-alumina solid electrolyte was synthesized by solid state reaction using $Li_2O$ and MgO as a phase stabilizer, and the effect of stabilizers on the phase formation and sintering density was investigated. In order to determine the phase fraction according to the synthesizing temperature, the molar ratio of [$Na_2O$] : [$Al_2O_3$] was fixed at 1 : 5, and calcination was conducted at temperatures between $1200{\sim}1500^{\circ}C$ for 2 h. In the $Li_2O$-$Na_2O$-$Al_2O_3$ ternary system, ${\beta}^{{\prime}{\prime}}$-alumina phase fraction considerably increased by the secondary phase transition at $1500^{\circ}C$, whereas it maintained similarly in the MgO-$Na_2O$-$Al_2O_3$ system. Additionally, the disc-type specimens of $Na^+$-beta-alumina were sintered at the temperature between $1550{\sim}1650^{\circ}C$ for 30 min, and relative sintering densities, phase changes, and microstructures were analyzed. In case of $Li_2O$-stabilized $Na^+$-beta-alumina, ${\beta}^{{\prime}{\prime}}$-phase fraction and relative density of specimen sintered at $1600^{\circ}C$ were 94.7% and 98%, respectively. Relative density of MgO-stabilized $Na^+$-beta-alumina increased with a rise in sintering temperature.

• Restorative Dentistry and Endodontics
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• v.34 no.4
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• pp.364-370
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• 2009

The aim of this study was to evaluate the effect of fiber direction on the polymerization shrinkage of fiber-reinforced composite. The disc-shaped flowable composite specimens (d = 10 mm, h = 2 mm, Aeliteflo A2, Bisco, Inc., IL, USA) with or without glass fiber bundle (X-80821P Glass Fiber, Bisco, Inc., IL, USA) inside were prepared, and the longitudinal and transversal polymerization shrinkage of the specimens on radial plane were measured with strain gages (Linear S-series 350${\Omega}$, CAS, Seoul, Korea). In order to measure the free polymerization shrinkage of the flowable composite itself, the disc-shaped specimens (d = 7 mm, h = 1 mm) without fiber were prepared, and the axial shrinkage was measured with an LVDT (linear variable differential transformer) displacement sensor. The cross-section of the polymerized specimens was observed with a scanning electron microscope to examine the arrangement of the fiber bundle in composite. The mean polymerization shrinkage value of each specimen group was analyzed with ANOVA and Scheffe post-hoc test (${\alpha}$=0.05). The radial polymerization shrinkage of fiber-reinforced composite was decreased in the longitudinal direction of fiber, but increased in the transversal direction of fiber (p<0.05). We can conclude that the polymerization shrinkage of fiber-reinforced composite splint or restoratives is dependent on the direction of fiber.

• Korean Journal of Materials Research
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• v.23 no.4
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• pp.240-245
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• 2013

Electrochemical surface treatment is commonly used to form a thin, rough, and porous oxidation layer on the surface of titanium. The purpose of this study was to investigate the formation of nanotubular titanium oxide arrays during short anodization processing. The specimen used in this study was 99.9% pure cp-Ti (ASTM Grade II) in the form of a disc with diameter of 15 mm and a thickness of 1 mm. A DC power supplier was used with the anodizing apparatus, and the titanium specimen and the platinum plate ($3mm{\times}4mm{\times}0.1mm$) were connected to an anode and cathode, respectively. The progressive formation of $TiO_2$ nanotubes was observed with FE-SEM (Field Emission Scanning Electron Microscopy). Highly ordered $TiO_2$ nanotubes were formed at a potential of 20 V in a solution of 1M $H_3PO_4$ + 1.5 wt.% HF for 10 minutes, corresponding with steady state processing. The diameters and the closed ends of $TiO_2$ nanotubes measured at a value of 50 cumulative percent were 100 nm and 120 nm, respectively. The $TiO_2$ nanotubes had lengths of 500 nm. As the anodization processing reached 10 minutes, the frequency distribution for the diameters and the closed ends of the $TiO_2$ nanotubes was gradually reduced. Short anodization processing for $TiO_2$ nanotubes of within 10 minutes was established.

• Proceedings of the KACD Conference
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• 2008.05a
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• pp.235-245
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• 2008

The aim of this study was to develop a method for measuring the slumping resistance of resin composites and to relate it to the rheological characteristics. Five commercial hybrid composites (Z100. Z250. DenFil, Tetric Ceram. ClearFil) and a nanofill composite (Z350) were used to make disc-shaped specimens of 2 mm thickness. An aluminum mold with square shaped cutting surface was pressed onto the composite discs to make standardized imprints. The imprints were light-cured either immediately (non-slumped) or after waiting for 3 minutes at $25^{\circ}C$ (slumped). White stone replicas were made and then scanned for topography using a laser 3-D profilometer. Slumping resistance index (SRI) was defined as the ratio of the groove depth of the slumped specimen to that of the non-slumped specimen. The pre-cure viscoelasticity of each composite was evaluated by an oscillatory shear test and normal stress was measured by a squeeze test using a rheometer. Flow test was also performed using a flow tester. Correlation analysis was performed to investigate the relationship between the viscoelastic properties and the SRI. SRI varied between the six materials (Z100 < DenFil < Z250 < ClearFil < Tetric Ceram < Z350). The SRI was strongly correlated with the viscous (loss) shear modulus G' but not with the loss tangent. Also. slumping resistance was more closely related to the resistance to shear flow than to the normal stress. Slumping tendency could be quantified using the imprint method and SRI. The index may be applicable to evaluate the clinical handling characteristics of composites.

• Restorative Dentistry and Endodontics
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• v.33 no.3
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• pp.235-245
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• 2008

The aim of this study was to develop a method for measuring the slumping resistance of resin composites and to relate it to the rheological characteristics. Five commercial hybrid composites (Z100, Z250, DenFil, Tetric Ceram, ClearFil) and a nanofill composite (Z350) were used to make disc-shaped specimens of 2 mm thickness. An aluminum mold with square shaped cutting surface was pressed onto the composite discs to make standardized imprints. The imprints were light-cured either immediately (non-slumped) or after waiting for 3 minutes at $25{\circ}C$ (slumped). White stone replicas were made and then scanned for topography using a laser 3-D profilometer. Slumping resistance index (SRI) was defined as the ratio of the groove depth of the slumped specimen to that of the nonslumped specimen. The pre-cure viscoelasticity of each composite was evaluated by an oscillatory shear test and normal stress was measured by a squeeze test using a rheometer. Flow test was also performed using a flow tester. Correlation analysis was performed to investigate the relationship between the viscoelastic properties and the SRI. SRI varied between the six materials (Z100 < DenFil < Z250 < ClearFil < Tetric Ceram < Z350). The SRI was strongly correlated with the viscous (loss) shear modulus G' but not with the loss tangent. Also, slumping resistance was more closely related to the resistance to shear flow than to the normal stress. Slumping tendency could be quantified using the imprint method and SRI. The index may be applicable to evaluate the clinical handling characteristics of composites.