• 제목/요약/키워드: dipping time

검색결과 196건 처리시간 0.029초

조선왕조실록 밀랍지 시제품 제작 및 물리적 특성 분석 (Physical Property Analysis and Manufacture of Beeswax-Treated Paper of Annals of the Joseon Dynasty)

  • 윤경동;최경화;서진호;강영석;정소영
    • 보존과학연구
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    • 통권30호
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    • pp.149-155
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    • 2009
  • Annals of the Joseon Dynasty were composed of 1,229 volumes, and the 475 copies of total annals were wax-treated. Compared to non-wax treated copies, waxed volume of annals were seriously damaged such as crack, stick, discoloration to brown or black, and partially degradation. It is believed that the purpose of wax treatment for some volumes in the annals of the Joseon Dynasty is to prevent paper to deteriorate and to keep for the long time. But, beeswax could be deteriorated itself more rapidly. As a result, the waxed volume was much more damaged than non-waxed volume. Therefore, the investigation of decomposition and deterioration mechanism of beeswax-treated paper which might be used in waxed volume of the annals of the Joseon Dynasty must be done in order to prevent further decomposition and to restore the degraded wax-treated copies of the annals. For basis data of this purpose, physical properties of beeswax-treated paper be analyzed by coating methods. In result, sample products was manufactured reproducibility in lab scale. Specially, beeswax-treated method improved a orientation of papers. And the brushing method was stronger than the dipping method.

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Development of Long-Term Storage Technology for Chinese Cabbage - Physiological Characteristics of Postharvest Freshness in a Cooler with a Monitoring and Control Interface

  • Lim, Ki Taek;Kim, Jangho;Chung, Jong Hoon
    • Journal of Biosystems Engineering
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    • 제39권3호
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    • pp.194-204
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    • 2014
  • Purpose: The aim of this study was to develop long-term storage technology for Chinese cabbage in order to extend the period of availability of freshly harvested products. The scope of the paper deals with the use of a cooler with a remote monitoring and control interface in conjunction with use of packaging film. Methods: A cooler with a real time monitoring system was designed as a low-temperature storage facility to control temperature and relative humidity (RH). The effects of storage in high-density polyethylene (HDPE) plastic boxes, 3% chitosan dipping solution, polypropylene film (PEF) with perforations, and mesh packaging bags on physiological responses were investigated. The optimal storage temperature and humidity for 120 days were below $0.5^{\circ}C$ and 90%, respectively. Physiological and biochemical features of cabbage quality were also analyzed: weight loss, texture, and sugar salinity, chlorophyll, reducing sugar, and vitamin C contents. Results: The cooler with a remote monitoring and control interface could be operated by an HMI program. A $0.5^{\circ}C$ temperature and 90% humidity could be remotely controlled within the cooler for 120 days. Postharvest freshness of Chinese cabbages could be maintained up to 120 days depending on the packaging method and operation of the remote monitoring system. In particular, wrapping the cabbages in PEF with perforations resulted in a less than a 5% deterioration in quality. This study provides evidence for efficient performance of plastic films in minimizing post-harvest deterioration and maintaining overall quality of cabbages stored under precise low-temperature conditions with remote monitoring and a control interface. Conclusions: Packaging with a modified plastic film and storage in a precisely controlled cooler with a remote monitoring and control interface could slow down the physiological factors that cause adverse quality changes and thereby increase the shelf life of Chinese cabbage.

2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide를 이용한 고분자 습도센서의 감습 특성 및 신뢰성 (Humidity-Sensitive Characteristics and Reliabilities of Polymeric Humidity Sensors Using 2-Methacryloxyethyl dimethyl 2-hydroxyethyl ammonium brornide)

  • 이칠원;공명선
    • 공업화학
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    • 제10권3호
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    • pp.461-466
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    • 1999
  • 암모늄염을 포함하는 고분자 습도센서를 2-methacryloxyethyl dimethyl 2-hydroxyethyl ammonium bromide (MDHAB)/MMA/DAEMA=6/3/1의 공중합체로부터 제조하였다. 감습막은 금/알루미나 전극에 침적법에 의하여 도포하였으며 $5^{\circ}C$, 40%RH, 70%RH, 그리고 90%RH에서 전형적인 임피던스는 각각 $298k{\Omega},\;11k{\Omega}$, 그리고 $2.3k{\Omega}$을 나타내어 감습특성은 저온에서 사용되는 습도 센서로서의 특성에 적합하였다. 온도 의존성 계수는 $5{\sim}20^{\circ}C$에서 $-0.80%RH/^{\circ}C$이었으며 히스테리시스는 ${\pm}2%RH$ 이내에 존재하였다. 응답 속도는 34%RH에서 88%RH로 변화할 때 38초였다. 신뢰성 시험으로서 온도 사이클, 습도 사이클, 고온 고습 저항성, 전기 인가, 장기 방치, 그리고 내수성을 측정하여 습도센서로서의 응용성을 평가하였다.

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Elevated Plus-Maze를 이용한 현삼의 항불안 효과 : GABA 신경계와의 관련성 연구 (Anxiolytic-like Effects of Scrophularia buergeriana Miquel Using the Elevated Plus-Maze in Mice : Involvement of GABAergic Nervous System)

  • 최윤희;정지욱
    • 동의생리병리학회지
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    • 제24권3호
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    • pp.476-483
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    • 2010
  • The present study was performed to investigate the putative anxiolytic-like effects of the aqueous extract of the roots of Scrophularia buergeriana (SB-W) using elevated plus-maze (EPM) and hole-board apparatus in mice. SB-W was orally administered at doses of 50, 100, 200 or 400 mg/kg to ICR mice, 1 h before the behavioral evaluation. Control group were administered with an equal volume of saline, and positive control group with buspirone (2 mg/kg, i.p.). The administration of SB-W significantly increased the percentage of time spent in open arms and entries into the open arms of the EPM compared with saline-treated control group (P < 0.05). Futhermore, those anxiolytic-like activities of SB-W were antagonized by flumazenil (a $GABA_A$ antagonist, 10 mg/kg), but not by WAY-100635 (a 5-$HT_{1A}$ antagonist, 0.3 mg/kg). Moreover, there were no changes in the locomotor activity and myorelaxant effects in any group compared with saline-treated control group. In the hole-board test, the administration of SB-W (200 and 400 mg/kg) significantly increased the number of head-dipping compared with saline-treated control group (P < 0.05). Therefore, these findings suggest that Scrophularia buergeriana promotes the anxiolytic-like activity mediated by GABAergic nervous system in mice.

화강암반내 단층지역에 위한 지하 방사성폐기물 처분장 인접지역에서의 열-수리-역학적 연성거동 비교 연구 (A comparison study on coupled thermal, hydraulic, and mechanical interactions associated with an underground radwaste repository within a faulted granitic rock mass)

  • 김진웅;배대석;강철형
    • 지질공학
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    • 제11권3호
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    • pp.255-267
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    • 2001
  • 지하 50m의 화강암반내 단층지역에 위치한 지하 방사성폐기물 처분장 인접지역에서의 열, 수리, 및 역학적 연성거동을 비교하고 분석하였다. 해석에는 2차원 해석코드인 UDEC을 사용하였다. 해석모델은 화강암반, 처분공내의 압축 벤토나이트로 둘러싸인 PWR 사용후 핵연료 처분용기, 및 처분동굴내에 채워진 혼합 벤토나이트를 포함한다. 수리-역학적, 열-역학적, 및 열-수리-역학적 연성거동을 비교 및 분석하였다. PWR 사용후 핵연료내의 방사성 물질로부터 나오는 시간의존 방사성 붕괴열이 처분장 및 인접지역에 미치는 영향을 분석하였다. 수리해석에는 steady state flow 알고리즘을 사용하였다.

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생쥐 상악치조부에서의 파골세포의 당단백 합성 및 이동에 관한 전자현미경 자기방사법적 연구 (An Electron Microscopic Radioautographic Study of the Synthesis and Migration of the Glycoproteins in the Osteoclast of the Mice Maxillary Alveolar Bone)

  • 김명국
    • Applied Microscopy
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    • 제22권2호
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    • pp.118-126
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    • 1992
  • The pathway and time course of fucose-containing glycoprotein synthesis and intracellular translocation in osteoclasts of the mice maxillary alveolar bone were investigated by electron microscopic radioautography. Male Balb-C mice weighing 17gm were anesthetized with Nembutal and injected via the external jugular vein with 2.5 mCi of $L-[6-^{3}H]-fucose$ (specific activity 16.8 mCi/mmol) in 0.1 ml of sterile saline solution. At 5, 10, 20, 35 minutes and 8 hours after administration of the $^{3}H-fucose$, animals were killed by intracardiac perfusion of 30ml of 2% glutaraldehyde in a modified Tyroid solution, pH 7.4. The maxillae were then removed and further fixed in Karnovsky fixative for an additional 3-4 hours. After rinsing in 0.1M cacodylate buffer for 10 minutes, the maxillae were demineralized for 2 weeks at $4^{\circ}C$ in ethylene diamine tetra acetate containing 2% glutaraldehyde. The first interdental areas were mesiodistally sectioned into slices of 1mm thickness and postfixed in osmium tetroxide. Tissues were then dehydrated and embedded in Poly Bed. To prepare electron microscopic radioautography, the dipping method of Kopriwa (1973) was employed. Thin sections were coated with a crystalline monolayer of ILford $L_4$ photographic emulsion. After exposure for 4 months at $4^{\circ}C$, the sections were developed Kodak Microdol-X and Phenidon (for compact grains), fixed in 30% sodium thiosulfate, stained with uranyl acetate and lead citrate and examined in the electron microscope (JEOL 1200 EX). At 5, 10 and 20 minutes after injection, $^{3}H-fucose$ was concentrated in Golgi cisternae of the osteoblasts. By 35 minutes the labels were observed over small vesicles in the suprannclear area of osteoclasts. At 8 hours, numerous silver grains were located on the ruffled border and cell membrane of osteoclasts. These results indicate that fucose molecules are added in the Golgi apparatus and small vesicles appear to be responsible for translocation of the glycoproteins to the marginal portion of osteoblasts. The glycoproteins are distributed on the osteoclast cell surface and especially over the ruffled border.

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표면 촉매 화학 반응을 이용한 크기 조절이 가능한 홀 어레이 제작 (Fabrication of Size-Controlled Hole Array by Surface-Catalyzed Chemical Deposition)

  • 박형주;박정원;이대식;표현봉
    • 센서학회지
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    • 제27권1호
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    • pp.55-58
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    • 2018
  • Low-cost and large-scale fabrication method of nanohole array, which comprises nanoscale voids separated by a few tens to a few hundreds of nanometers, has opened up new possibilities in biomolecular sensing as well as novel frontier optical devices. One of the key aspects of the nanohole array research is how to control the hole size following each specific needs of the hole structure. Here, we report the extensive study on the fine control of the hole size within the range of 500-2500 nm via surface-catalyzed chemical deposition. The initial hole structures were prepared via conventional photo-lithography, and the hole size was decreased to a designed value through the surface-catalyzed chemical reduction of the gold ion on the predefined hole surfaces, by simple dipping of the hole array device into the aqueous solution of gold chloride and hydroxylamine. The final hole size was controlled by adjusting reaction time, and the optimal experimental condition was obtained by doing a series of characterization experiments. The characterization of size-controlled hole array was systematically examined on the image results of optical microscopy, field emission scanning electron microscopy(FESEM), atomic-force microscopy(AFM), and total internal reflection microscopy.

포스포늄 염을 가진 고분자 습도센서의 감습 특성 및 신뢰성 (Humidity-Sensitive Characteristics and Reliabilities of Polymeric Humidity Sensor Containing Phosphonium Salts)

  • 김오영;공명선
    • 공업화학
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    • 제9권4호
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    • pp.554-560
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    • 1998
  • 포스포늄 염을 포함하는 감습성 전해질 고분자 결로센서를 vinylbenzyl triphenyl phosphonium chloride(VTPC)/styrene=3/7의 공중합체로부터 제조하였다. 감습막은 금/알루미나 전극에 침적법에 의하여 도포하였으며 $25^{\circ}C$의 70%RH, 80%RH, 90%RH, 그리고 95% RH에서 임피던스는 $11M{\Omega}$, $980k{\Omega}$, $50k{\Omega}$, 그리고 $11k{\Omega}$를 각각 보여 주어 감습 특성은 결로 센서로서의 특성에 매우 적합하였으며 $15{\sim}35^{\circ}C$에서 온도 의존성 계수는 $-0.25%RH/^{\circ}C$이었으며 히스테리시스는 ${\pm}2%RH$ 이내에 존재하였다. 응답 속도는 70%RH에서 98%RH로 변화할 때 45초이었다. 신뢰성 시험으로서 온도 사이클, 습도 사이클, 고온 고습 저항성, 전기 인가, 장기 방치, 그리고 내수성을 측정하여 결로 센서로서의 적합성을 평가하였다.

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온주(溫州)밀감 sac의 저장중(貯藏中) 변화(變化) (Changes of Satsuma Mandarin Sacs during Storage)

  • 최영배;강동섭;강영주
    • 한국식품영양과학회지
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    • 제16권3호
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    • pp.21-25
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    • 1987
  • 온주(溫州)밀감 sac을 통조림 저장하기 위한 기초자료를 얻기 위하여 sac을 염소수에 침지하여 예비살균하고 밀봉전 살균온도가 저장중 sca에 미치는 영향을 검토하였다. sac의 당도, 산도 및 pH는 처리조건에 따라 큰 변화가 없었으나 염소처리에 의하여 sac의 파괴율은 저장초기에 증가하였으나 저장기간이 길어짐에 따라 평준화 되었다. 총 카로테노이드는 변화가 크지 않았으며, 총 비타민 C는 저장 3개월과 4개월 사이에 감소가 컸다. 환원형 비타민 C는 저장초기에, 산화형 비타민 C는 저장후기에 주로 감소하였다. 또한 비타민 C의 감소는 염소처리보다 살균온도 및 저장온도에 의해 더 큰 영향을 받은 것으로 보였다.

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새로운 N-Methacryloyl-N'-ethyl-N'-propyl Piperazinium Bromide 단량체를 사용한 습도센서 및 그들의 특성 조사 (Resistive Humidity Sensor Using New N-Methacryloyl-N'-ethyl-N'-propyl Piperazinium Bromide Monomer and Their Properties)

  • 이인호;박찬교;공명선
    • 폴리머
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    • 제33권4호
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    • pp.326-332
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    • 2009
  • 새로운 감습성 단량체인 N-methacryloyl-N'-ethyl-N'-propyl piperazinium bromide(MANEPPB)를 N-methacryloyl-N'-ethyl piperazine(MANEP)와 1-bromopropane의 4차염화 반응에 의하여 합성하였다. MANEPPB/MMA/AA=60/35/5, 70/25/5, 80/15/5, 90/5/5 및 95/0/5 조성의 전해질 공중합체를 감습막으로 사용하기 위하여 제조하였다. 상기 감습액에 아지리딘 가교제인 trimethylolpropane tris(2-methyl-1-aziridinopropionate)(TTAP)를 혼합하여 금 전극 위에 침적법에 의하여 도포하고 가교반응을 진행하여 습도센서를 제조 하였다. 상대습도에 대한 습도센서의 저항을 측정하였을 때, $20{\sim}90%RH$ 상대습도 영역에서 $10^3$의 저항 값이 변화하였으며, 이것은 상용 습도센서로서 대기의 습도를 측정하는데 요구되는 특성을 보여주었다. 그 밖에 온도 의존성, 주파수 의존성, 히스테리시스, 응답 및 회복 속도 그리고 내수성을 측정하여 습도센서로서 특성을 평가하였다.