• 제목/요약/키워드: dipping temperature

검색결과 160건 처리시간 0.027초

HTV 실리콘 고무에서 열화인자에 따른 저분자량 성분과 표면 발수성의 변화 (Effects of Ageing Factors on Low Molecular Weight Silicone Fluids Content Fluids Content and Surface Hydrophobicity in HTV Silicone Rubber)

  • 허창수;연복희;조한구
    • 한국전기전자재료학회논문지
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    • 제12권1호
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    • pp.1-10
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    • 1999
  • In this paper, we have investigated the effects of the environmental factors on Low Molecular Weight (LMW) silicone fluid contents existing in high temperature vulcanized (HTV) silicone rubber sample, using dipping method and contact angle, current measurement. Artificial treatments such as immersion in water, elevated temperature, UV irradiation and dry band arcing under salt-fog condition are selected as the environmental factors. This results will be helpful to investigate the degradation with time and to expect a life time, because the LMW silicone content, which is important to recovery the hydrophobicity of silicone rubber surface, show different results by each environmental factors.

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인산염 처리가 건마늘 플레이크의 품질에 미치는 영향 (Effects of Phosphate Complex Treatment on the Quality of Dried Garlic Flakes)

  • 김현구;조길석;신동화;김일환
    • 한국식품과학회지
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    • 제19권1호
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    • pp.75-80
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    • 1987
  • 마늘 플레이크 건조시 갈변을 방지하기위하여 축합 인산염의 농도 및 침지시간에 따라서 마늘 플레이크의 갈변현상을 조사하였다. 마늘 플레이크 건조중 갈변억제는 인산염 농도, 침지시간 및 환원당에 의해서 크게 좌우되며 갈변물질의 형성속도는 환원당 함량과 반비례의 관계가 있었다. 인산염 처리는 0.3%에서 3분간 침지함으로서 마늘 건조중 갈변을 억제할 수 있었으며 pyruvate 성분의 감소는 $0.2{\sim}0.3%$에서 3분 침지하는 것이 가장 적었다. 건조수율을 인산염을 처리하면 처리하지 않을 경우보다 $1.62{\sim}1.75%$의 수율이 떨어졌는데 이는 가용성 물질이 용출되어 수율이 감소되는 것으로 생각되었다.

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열압착법을 이용한 경.연성 인쇄회로기판 접합부의 접합 강도에 미치는 접합 조건의 영향 (Effects of Bonding Conditions on Joint Property between FPCB and RPCB using Thermo-Compression Bonding Method)

  • 이종근;고민관;이종범;노보인;윤정원;정승부
    • 마이크로전자및패키징학회지
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    • 제18권2호
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    • pp.63-67
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    • 2011
  • 본 연구에서는 interlayer로 Sn을 사용하여 경성 인쇄 회로 기판(Rigid printed circuit board, RPCB)과 연성 인쇄 회로 기판(Flexible printed circuit board, FPCB) 간의 열압착 접합(Thermo-compression bonding) 조건을 최적화하는 연구를 진행하였다. 접합에 앞서 FPCB를 다양한 온도와 시간조건 하에서 Sn이 용융된 솔더 배스 안에서 침지(Dipping) 공정을 수행하였고, 열압착법을 이용하여 FPCB와 RPCB의 접합을 수행하였다. FPCB/RPCB 접합부의 접합 강도를 $90^{\circ}$ 필 테스트(Peel test)를 이용하여 측정하였다. 그 결과 $270^{\circ}C$, 1s의 침지 조건에서 FPCB의 polyimide(PI)와 Cu 전극 계면에서 파단되고, 이때, 최대 박리 강도를 얻었다. FPCB와 RPCB의 열압착 접합시 주요 변수로는 압력, 온도, 시간이 있으며, 특히 온도의 증가에 따라 접합 강도가 크게 증가하였다. 접합부 계면 관찰 결과, 접합 온도와 시간이 증가함에 따라 접합 면적이 증가하였으며, 이로 인해 접합 강도가 증가하는 것으로 사료된다. 필 테스트 과정에서 나타나는 F-x(Forcedisplacement) 곡선을 토대로 산출한 파괴 에너지와 접합 강도는 $280^{\circ}C$, 10s의 접합 조건에서 가장 높게 나타났으며, 이 조건이 최적 접합 조건으로 도출되었다.

저온도포열분해에 의해 제조된 Pb(Zr, Ti)O$_3$ 박막의 에피탁시와 결정화도에 미치는 전열처리 시간의 영향 (Effect of Prefiring Time on Epitaxy and crystallinity of Pb(Zr, Ti)O$_3$ Thin Films in Low Temperature Pyrolysis)

  • 황규석;이형민;김병훈
    • 한국세라믹학회지
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    • 제35권9호
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    • pp.969-973
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    • 1998
  • Pb(Zr, Ti)O3 (PZT) (Zr:Ti= 52: 48) thin films were prepared on MgO(100) substrates by dipping-py-rolysis process using metal naphthenates as starting materials. Thin films were fabricated by spin coating technique and the precursor films were prefired at 20$0^{\circ}C$ in air for 0.5, 1, 2, 3, and 24 h followed by final heat treatment at 75$0^{\circ}C$ for 30min. Film prefired for 24 h lost orientational properties and pole figure analysis showed the lost of the epitaxial relationship between the films and substrate while highly a/c-axis oriented thin films were obtained for the samples prefired for 1, 2, and 3h.

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Atmosphere Effects in Low Temperature Pyrolysis of Chemical Solution Derived Pb(Zr, Ti) O3 Films

  • Hwang, Kyu-Seog;Lee, Hyung-Min;Kim, Byung-Hoon
    • The Korean Journal of Ceramics
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    • 제4권3호
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    • pp.199-203
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    • 1998
  • $Pb(Zr, Ti)O_3$ (Pb:Zr:Ti=1:0.52:0.48) thin films were prepared on single crystal MgO(100) substrates by dipping-pyrolysis process using a solution of constituent metal naphthenates as starting materials. The solution was spin-coated onto substrate and the precursor films were pyrolyzed at $200^{\circ}C$ in air or at $200^{\circ}C$ in argon for 1, 2, 5 and 24h, followed by final heat treatment at $750^{\circ}C$. For all the films, highly (h00)/(00l)-oriented Pb$Pb(Zr, Ti)O_3$ thin films with smooth surfaces and crack-free were obtained, whereas thin film pyrolyzed in air for 24 h exhibited polycrystalline character. According to the pole-figure analysis, epitaxy of the product films was found to depend on pyrolysis atmosphere.

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Comparison of Electrodeposited Carbon Fibers Reinforce Epoxy Composites Using Monomeric and Polymeric Coupling Agents

  • Park, Joung-Man;Kim, Yeong-Min
    • Macromolecular Research
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    • 제8권4호
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    • pp.153-164
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    • 2000
  • By electrodeposition (ED) using a monomeric- and two polymeric coupling agents, the interfacial shear strength (IFSS) of carbon fiber/epoxy composites was investigated by fragmentation test. ED results were compared with the dipping and the untreated cases under dry and wet conditions. Multi-fiber composites (MFC) were used for the direct comparison for the untreated and the treated cases. Various treating conditions including time, concentration and temperature were evaluated, respectively. Under dry and wet conditions ED treatment exhibited much higher IFSS improvement compared to the dipping and the untreated cases. Monomeric- and polymeric coupling agents exhibited the comparative IFSS improvement. Adsorption mechanism between coupling agents and carbon fiber was analyzed in terms of the electrolyte molecular interactions during ED process based on to the chain mobility. The microfailure modes occurring from the fiber break, matrix and interlayer cracks were correlated to IFSS.

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Al-hot Dipping Followed by High-Temperature Corrosion of Carbon Steels in Air and Ar-0.2%SO2 Gas

  • Abro, Muhammad Ali;Jung, Seung Boo;Lee, Dong Bok
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2015년도 춘계학술대회 논문집
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    • pp.128-129
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    • 2015
  • Al-rich coatings were prepared on hot rolled low carbon steel by hot dipping method in molten Al-bath to investigate the corrosion resistance with the possible outcomes and defects of aluminized coatings in air and $Ar-0.2%SO_2$ mixed gases. Coating microstructure was composed of an inner Al-Fe intermetallic layer and outer Al-rich layer. Aluminum oxidized preferentially to the thin, outer, protective ${\alpha}-Al_2O_3$ layer, without forming the nonprotective iron/sulfur-oxide layer after heating at $800^{\circ}C$ for 20 h, in both the gases and provided the resistance against corrosion.

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Al-hot Dipping Followed by High-Temperature Corrosion of Carbon Steels in Air and Ar-0.2%SO2 Gas

  • 김민정;;박상환;지권용
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2015년도 춘계학술대회 논문집
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    • pp.122-122
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    • 2015
  • Al-rich coatings were prepared on hot rolled low carbon steel by hot dipping method in molten Al-bath to investigate the corrosion resistance with the possible outcomes and defects of aluminized coatings in air and $Ar-0.2%SO_2$ mixed gases. Coating microstructure was composed of an inner Al-Fe intermetallic layer and outer Al-rich layer. Aluminum oxidized preferentially to the thin, outer, protective ${\alpha}-Al_2O_3$ layer, without forming the nonprotective iron/sulfur-oxide layer after heating at $800^{\circ}C$ for 20h, in both the gases and provided the resistance against corrosion.

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광촉매를 이용한 셀룰로오스섬유의 기능화에 관한 연구 - 항균·소취성 및 자외선 차폐성을 중심으로 - (The Functional Properties of Cellulose Fabric Treated with TiO2 - Focusing on Antibacterial activity, Deodorization & UV cut ability -)

  • 권오경;문제기;손부헌;최영희
    • 한국의류산업학회지
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    • 제5권4호
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    • pp.395-398
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    • 2003
  • In this study, we measured the antibacterial activities, deodorization, UV cut ability, whiteness and SEM, according to the size($5{\mu}m$, $15{\mu}m$) of $TiO_2$, concentration(3%, 5%, 10%) and dipping temperature($50^{\circ}C$, $70^{\circ}C$) with using anatase type of $TiO_2$ photocatalyst. Photocatalyst is the substance which carries out functions, such as decomposition, removal, deodorization, antibacterial, etc. of a contaminant, in a place with light based on an oxidation-reduction reaction. The results of this study were as follow. Antibacterial activities are increased with increasing of the $TiO_2$'s concentration, and $TiO_2$ has high antibacterial activities for Staphylococcus aureus but it has low antibacterial activities for Klebsiella pneumoniae. The deodorization and UV cut ability is very good, therefore be able to get good effects with using only 3% of $TiO_2$. Every effects are increased by using small size of $TiO_2$ and high dipping temperature.

자망어구용 코팅발돌의 개발 (A Development of the Coated Lead Sinker for Gill-net)

  • 안영일
    • 수산해양교육연구
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    • 제22권4호
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    • pp.501-507
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    • 2010
  • The ceramic contained paint was made to replace the lead sinker for gill-net with coated lead sinker. The ceramic contained paints were coated in various conditions on the lead sinker with 19g of weight and the optimal coating condition was studied. The adaptability of the coated lead sinker was checked through the anti durability test and fishing operation with gill-net. The case of "Main material 70 wt% + Urethane thinner 30 wt% (Main material 700 $m{\ell}$ + Thinner 300 $m{\ell}$)" showed the best in the coating characteristics depending on the combination ratio of the ceramic paint contained. The coated lead sinker dried at $100^{\circ}C$ inside oven was superior to the drying in the room temperature in its surface glossiness and anti durability and faster drying time than the one dried in normal temperature. The quadruple layers of coating on lead sinker with 4 times of dipping and drying application showed the super anti durability in the coating characteristics depending on the frequency of dipping. When press is applied to the coated lead sinker, the coated layer is not detached from the sinker. In addition, the coated lead sinker was not damaged or peeled at the fishing operation about 2 months in various depths within 50m and by the materials at the bottom (sand, stone and gravel stone) and it was in good condition.