• Title/Summary/Keyword: diatomite powder

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Sintering of porous ceramic of diatomite according to molding pressure and PEG content

  • Lee, Ye-Na;Ahn, Seok-Hwan;Nam, Hoseok;Nam, Ki-Woo
    • Journal of Ceramic Processing Research
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    • v.19 no.6
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    • pp.467-471
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    • 2018
  • Diatomite powder, a naturally occurring porous raw material, was used to make ceramic materials with porosity and high strength. The sintering behavior of the diatomite powder at various sintering temperatures suggests that diatomite monoliths with a high porosity and strength can be prepared at $1100^{\circ}C$. The compressive strength of the sintered diatomite monoliths increased as the sintering temperature increased, and the molding pressure of 2 MPa and the binder of 18.6 wt.% were excellent. When the sintering temperature rises, the diatomite powder is melted, and its pores gradually disappear. SEM images show that strengthening begins with the formation of inter-particle bonds at a low sintering temperature.

Strength Characteristics of Mortar with Diatomite Powder as an Admixture (혼화재료로서 규조토 분말을 사용한 모르타르의 강도 특성)

  • Choi, Jaejin;Park, Hongtae;Kim, Jaewoo
    • Journal of the Society of Disaster Information
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    • v.11 no.3
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    • pp.329-336
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    • 2015
  • When diatomite powder was used as an admixture in mortar, its effects on the mortar strength was examined by experimental tests. For the tests, 4 kinds of commercially available diatomite powder were purchased ; one non-calcined product, one calcined product, and flux-calcined product two. The compressive and flexural strength of the mortar according to the increase of added amount of calcined diatomite powder increased at all test ages(7, 28, and 56 days). However, the use of non-calcined diatomite powder worsened the fluidity of mortar severely and that caused much more required water content. And flux-calcined product did not show useful effect on the mortar strength.

The Effects of Kaolin Addition on the Properties of Reticulated Porous Diatomite-kaolin Composites (고령토의 첨가가 3차원 망상 구조를 가지는 다공성 규조토-고령토 복합재의 기본 특성에 미치는 영향)

  • Lee, Chae-Young;Lee, Sujin;Ha, Jang-Hoon;Lee, Jongman;Song, In-Hyuck;Moon, Kyoung-Seok
    • Journal of Powder Materials
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    • v.27 no.4
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    • pp.325-332
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    • 2020
  • In this study, the effects of kaolin addition on the properties of reticulated porous diatomite-kaolin composites are investigated. A reticulated porous diatomite-kaolin composite is prepared using the replica template method. The microstructure and pore characteristics of the reticulated porous diatomite-kaolin composites are analyzed by controlling the PPI value (45, 60, and 80 PPI) of the polyurethane foam (which are used as the polymer template), the ball-milling time (8 and 24 h), and the amount of kaolin (0-50 wt. %). The average pore size decreases as the amount of kaolin increases in the reticulated porous diatomite-kaolin composite. As the amount of kaolin increases, it can be determined that the amount of inter-connected pore channels is reduced because the plate-shaped kaolin particles connect the gaps between irregular diatomite particles. Consequently, a higher kaolin percentage affects the overall mechanical properties by improving the pore channel connectivity. The effect of kaolin addition on the basic properties of the reticulated porous diatomite-kaolin composite is further discussed with characterization data such as pore size distribution, scanning electron microscopy images, and compressive strength.

The Effect of Processing Conditions on the Gradient Pore Structure of Diatomite by Centrifugal Molding (경사 기공 구조를 가지는 규조토의 제조에 원심 분리 성형 공정 변수들이 미치는 영향)

  • Ha, Jang-Hoon;Oh, Eun-Ji;Ahmad, Rizwan;Song, In-Hyuck
    • Journal of Powder Materials
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    • v.19 no.4
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    • pp.304-309
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    • 2012
  • The purpose of our study was to develop the fabrication method of porous diatomite ceramics with a porosity gradient by centrifugal molding. The processing variables of centrifugal molding were derived from Stoke's law of sedimentation, which were the radius of the particles, the acceleration due to centrifugal molding and the dynamic viscosity of the slurry. And these could be controlled by ball-milling conditions, centrifugal conditions, and the addition of methyl cellulose, respectively. The effects of processing conditions on the gradient pore structure of diatomite were investigated by particle size analysis, scanning electron microscope, and mercury porosimeter.

Characterization of the Silica Coated Diatomite Based Ceramic Filter for Water Treatment (실리카 분말이 코팅된 수처리용 규조토계 세라믹 필터의 특성평가)

  • Bae, Byung-Seo;Ha, Jang-Hoon;Song, In-Hyuck;Hahn, Yoo-Dong
    • Journal of Powder Materials
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    • v.21 no.1
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    • pp.21-27
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    • 2014
  • In this study, diatomite based materials were investigated as a support filter for silica particle coating. The silica sol for coating was synthesized by a st$\ddot{o}$ber process. The diatomite support was dry-pressed at 10 MPa and sintered at $1200^{\circ}C$ for 1 hour. The coating sol was prepared as a mixture of EtOH and silica sol. The diatomite support was coated by a dip-coating process. Silica coated diatomite filter was sintered at $1000{\sim}1200^{\circ}C$ for 1 hour. The largest pore size was decreased with increasing concentration ratio of coating sol. The gas and water permeability of silica coated diatomite decreased with increasing of concentration ratio of the coating sol.

On the Extending for the Plywood Glue by Bark Powder of Persimmon Tree and Chestnut Tree (감나무와 밤나무 수피(樹皮)를 이용(利用)한 합판(合板) 접착증량(接着增量)에 관(關)한 연구(硏究))

  • Suh, Jin-Suk;Doh, Geum-Hyun;Jo, Jae-Myeong
    • Journal of the Korean Wood Science and Technology
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    • v.16 no.3
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    • pp.17-21
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    • 1988
  • In order to investigate the extending effects on urea-formaldehyde resin- or phenol- formal- dehyde resin- glued keruing plywood, hot pressing temperatures were controlled to 110, 140, 170 and $200^{\circ}C$. As the extender, wheat flour, persimmon bark powder, chestnut bark powder, the equivalently- extended with the above three powders, and diatomite powder were respectively mixed with 5, 10, 15 and 20% ratios to the resin liquid, and also with these the no- extended was allowed. Based on the measured bonding strength, the conclusions were drawn: 1. In the urea- formaldehyde resin, extending effects on the bonding strength were in the order of wheat flour, the equivalently- extended with the wheat flour, persimmon- and chestnut bark powder, persimmon bark powder, chestnut bark powder. In the phenol- formaldehyde resin, the effects in the order of wheat flour, persimmon bark powder, diatomite powder, chestnut bark powder were resulted in. Specifically, superior bonding strength to the no-extended were given with the wheat flour and persimmon bark powder. 2. On the whole, the bonding strength decreased gradually, as the hot pressing temperature increased except for the diatomite powder extending.

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A Refining of Natural Diatomite and Synthesis of SiC Powder (규조토 정제 및 탄화규소 분말합성)

  • Pai, Chul-Hoon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.3
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    • pp.312-319
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    • 2017
  • For high value-added applications of natural blue diatomite, the physical refining process and synthesis of SiC from refined diatomite were investigated. Approximately 30 percent Fe ($Fe_2O_3$) in raw blue diatomite was removed by a particle sieve separation process; the Fe composition for 325 mesh down powder was approximately 2 percent. Although a wet and/or dry magnetic separation process had some influence on the separation and/or refining of Fe composition, the Fe composition in the non-magnetic by-product was approximately 2 percent. Water leaching separation was effective in removing the Fe composition; approximately 40 percent of the Fe in raw blue diatomite was removed. The synthesis of ${\beta}$-SiC by a carbothermal reduction of the $SiO_2$ in the refined diatomite using carbon (graphite, carbon black), the effects of an acid-treatment on removing the Fe, and the specific surface area for the synthesized powder were also investigated. The impurities were mostly eliminated and the specific surface area was increased to $52.5m^2/g$.

An Experimental Study on the Rheology Characteristics of Insulating Concrete (단열콘크리트의 레올로지 특성에 관한 실험적 연구)

  • Ryu, Dong-Woo;Ji, Suk-Won;Jeon, Hyun-Kyu
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.2
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    • pp.118-124
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    • 2016
  • The purpose of this study is to analyze the rheology characteristics of insulating concrete for each type of insulation performance improvement material and utilize the result as preliminary data for optimal flow designing and pumping analysis. As a result, when lightweight aggregate was mixed, the yield stress decreased significantly, and in case of type 2, the combination of micro form cell admixture (MFA) and calcined diatomite powder (DM) showed the most ideal flow characteristics. In case of type 3, the combination of micro form cell admixture (MFA), calcined diatomite powder (DM) and lightweight aggregate (L) showed the best flow characteristics.

Thermoelectric properties of SiC prepared by refined diatomite (정제 규조토로 합성한 탄화규소의 열전특성)

  • Pai, Chul-Hoon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.4
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    • pp.596-601
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    • 2020
  • Silicon carbide is considered a potentially useful material for high-temperature electronic devices because of its large band gap energy and p-type or n-type conduction that can be controlled by impurity doping. Accordingly, the thermoelectric properties of -SiC powder prepared by refined diatomite were investigated for high value-added applications of natural diatomite. -SiC powder was synthesized by a carbothermal reduction of the SiO2 in refined diatomite using carbon black. An acid-treatment process was then performed to eliminate the remaining impurities (Fe, Ca, etc.). n-Type semiconductors were fabricated by sintering the pressed powder at 2000℃ for 1~5h in an N2 atmosphere. The electrical conductivity increased with increasing sintering time, which might be due to an increase in carrier concentration and improvement in grain-to-grain connectivity. The carrier compensation effect caused by the remaining acceptor impurities (Al, etc.) in the obtained -SiC had a deleterious influence on the electrical conductivity. The absolute value of the Seebeck coefficient increased with increasing sintering time, which might be due to a decrease in the stacking fault density accompanied by grain or crystallite growth. On the other hand, the power factor, which reflects the thermoelectric conversion efficiency of the present work, was slightly lower than that of the porous SiC semiconductors fabricated by conventional high-purity -SiC powder, it can be stated that the thermoelectric properties could be improved further by precise control of an acid-treatment process.