• Title/Summary/Keyword: delamination resistance

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The Dry Sliding Wear Properties of $SiC_w$ and $SiC_p$ Reinforced Bronze Matrix Composites (무윤활 미끄럼 마찰하에서 SiC 휘스커 및 입자강화 청동기지 복합재의 마모특성)

  • 이상로;허무영
    • Tribology and Lubricants
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    • v.9 no.2
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    • pp.49-55
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    • 1993
  • The dry sliding wear properties of the sintered Cu-10 wt%Sn bronze alloys reinforced with $SiC_w$ and $SiC_p$ were investigated by a pin-on-disc wear testing machine. The worn surfaces and the cross sections of the wear specimens and the wear debris were observed by SEM to study the effect of the variation of the ceramic phase contents in the composite and the wear condition on the wear behaviors. The wear of bronze matrix was dominated by the adhesive wear. The transition from mild to severe wear was found in the bronze matrix specimens at the applied load higher than 20N where the surface delamination caused the severe wear. The addition of $SiC_w$ and $SiC_p$ reinforcements in the romposites was proved to reduce the wear rate by the matrix strengthening at the applied load higher than 20N. SiC whiskers having a large length to diameter ratio which hold the deformed matrix were effective to hinder the crack propagation near the worn surface. Thus the maximum wear resistance was obtained in the composite reinforced by $SiC_w$ at the higher applied load.

Investigation of Wear Mechanisms of Tube Materials for Nuclear Steam Generators due to Stick-Slip Behavior under Fretting Conditions (프레팅 조건하에 있는 증기 발생기 세관재의 스틱-슬립 영역별 마멸 메커니즘 규명)

  • Lee Young-Ze;Jeong Sung-Hoon;Park Chi-Yong
    • Tribology and Lubricants
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    • v.21 no.1
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    • pp.33-38
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    • 2005
  • Fretting is the oscillatory motion with very small amplitudes, which usually occurs between two solid surfaces in contact. Fretting wear is the removal of material from contacting surfaces through fretting action. Fretting wear of steam generator tubes in nuclear power plant becomes a serious problem in recent years. The materials for the tubes usually are Inconel 690 (I-690) and Inconel 600 (I-600). In this paper, fretting wear tests for I-690 and I-600 were performed under various applied loads in water at room temperature. Results showed that the fretting wear loss of I-690 and I-600 tubes was largely influenced by stick-slip. The fretting wear mechanisms were the abrasive wear in slip regime and the delamination wear in stick regime. Also, I-690 had somewhat better wear resistance than I-600.

Thermal shock behaviors of TiN coatings on Inconel 617 and Silicon wafer substrates with finite element analysis method

  • Lee, Ki-Seuk;Jeon, Seol;Cho, Hyun;Lee, Heesoo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.2
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    • pp.67-73
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    • 2016
  • The degradation behaviors of TiN coating layers under thermo-mechanical stress were investigated in terms of comparison of finite element analysis (FEA) and experimental data. The coating specimen was designed to quarter cylinder model, and the pulsed laser ablation was assumed as heat flux condition. The FEA results showed that heat accumulation at the center of the laser-ablated spot occurred and principle stress was concentrated at the lower region of the coating layer. The microstructural observation revealed that surface melting and decrease of the coating thickness occurred in the TiN/Inconel 617 and the interfacial cracks formed in the TiN/Si. The delamination was caused by the mechanical stress from the center to the outside of the ablated spot as the FEA results expected. It was considered that the improvement of the thermal shock resistance was attributed to higher thermal conductivity of Si wafer than that of Inconel 617.

Planarizaiton of Cu Interconnect using ECMP Process (전기화학 기계적 연마를 이용한 Cu 배선의 평탄화)

  • Jeong, Suk-Hoon;Seo, Heon-Deok;Park, Boum-Young;Park, Jae-Hong;Jeong, Hae-Do
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.3
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    • pp.213-217
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    • 2007
  • Copper has been used as an interconnect material in the fabrication of semiconductor devices, because of its higher electrical conductivity and superior electro-migration resistance. Chemical mechanical polishing(CMP) technique is required to planarize the overburden Cu film in an interconnect process. Various problems such as dishing, erosion, and delamination are caused by the high pressure and chemical effects in the Cu CMP process. But these problems have to be solved for the fabrication of the next generation semiconductor devices. Therefore, new process which is electro-chemical mechanical polishing(ECMP) or electro-chemical mechanical planarization was introduced to solve the technical difficulties and problems in CMP process. In the ECMP process, Cu ions are dissolved electrochemically by the applying an anodic potential energy on the Cu surface in an electrolyte. And then, Cu complex layer are mechanically removed by the mechanical effects between pad and abrasive. This paper focuses on the manufacturing of ECMP system and its process. ECMP equipment which has better performance and stability was manufactured for the planarization process.

The Exit Hole Burr Generation of CFRP with Ultrasonic Vibration (초음파 진동에 따른 CFRP의 출구 구멍 버 생성)

  • Won, Sung-Jae;Li, Ching-Ping;Park, Ki-Moon;Ko, Tae Jo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.1
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    • pp.134-140
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    • 2017
  • CFRP has many industrial applications due to its low weight and high strength properties. CFRP is a composite material composed of carbon fibers embedded in a polymer matrix; it provides excellent resistance to fatigue wear, corrosion, and breakage due to fatigue. It is increasingly demanded in aircraft, automotive, and medical industries due to its superior properties to aluminum alloys, which were once considered the most suitable for specific applications. The basic machining methods of CFRP are drilling and route milling. However, in the case of drilling, the delamination of each layer, uncut fiber, resin burning, spalling, and exit burrs are barriers to successful application. This paper investigates the occurrence of exit burrs when drilling holes with ultrasonic vibration. Depending on design parameters such as the point angle, the characteristics of hole drilling were identified and appropriate machining conditions were considered.

Design Optimization of Blast and Ballistic Impact Resistance Sandwich Panels Based on Kriging Approximate Models (크리깅 근사모델기반 복합충격 저항 샌드위치 패널 최적설계)

  • Jang, Sungwoo;Baik, Woon-Kyoung;Choi, Hae-Jin;Park, Soon Suk
    • Korean Journal of Computational Design and Engineering
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    • v.20 no.4
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    • pp.367-374
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    • 2015
  • Sandwich panels consisting of various materials have widely been applied for mitigating dynamic impacts such as ballistic and blast impacts. Especially, the selection of materials for different core set-ups can directly influence its performance. In this study, we design the sandwich panels for alleviating ballistic and blast impacts by controlling the stacking sequence of core materials and their thicknesses. FEM studies are performed to simulate the dynamic behavior of sandwich panels subjected to ballistic and blast impacts. Delamination between the core layers is also considered in the FEM studies for feasible design. Based on the FEM data, kriging models are generated for approximating design space and quickly predicting the FEM outputs. Finally, design optimizations are implemented to find the optimum stacking sequence of core materials and thicknesses with given impact situations.

A Study on the Removal of CFRP Machining Defects by Various Tool Geometries (공구 형상에 따른 CFRP의 가공결함 제거에 관한 연구)

  • Park, Ki Moon;Ko, Tae Jo;Yu, Zhen;Kumaran S, Thirumalai
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.4
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    • pp.16-23
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    • 2017
  • CFRP(Carbon Fiber Reinforced Plastics) has many industrial applications due to its low weight and high strength properties. Due to its superior properties, for example, excellent resistance to fatigue wear, corrosion, and breakage from fatigue, it has been widely applicable to aircraft, automotive, and medical industries and so on. The main machining for CFRP is drilling, and route milling. In case of drilling, the machining defects such as the delamination of each layer, uncut fiber, resin burning, spalling, and exit burrs are inevitable. The issue to remove such kind of defects is necessary to make CFRP parts successful. From this point of view, this paper investigates the removal effectiveness of machining defects existing at exit region with different type of tool geometries. Consequently, based on the experiments, the tool geometry is most impact factor to remove uncut fiber or resin.

Wear Properties of Silicon Nitride Nano-Ceramics (나노 질화규소 세라믹스의 내마모 특성)

  • Kim, Jae-Hee;Kumar B, Venkata Manoj;Kim, Won-Sik;Hong, Seong-Hyeon
    • Journal of the Korean Ceramic Society
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    • v.46 no.5
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    • pp.505-509
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    • 2009
  • In this study, bulk nano-crystalline $Si_3N_4$ ceramics were fabricated by spark plasma sintering (SPS) and their mechanical properties, in particular wear, were investigated. A wide range of grain sizes, from 80 nm and 250 nm were obtained by varying sintering conditions ($1550^{\circ}C$-5 min to $1650^{\circ}C$-20 min). The elastic modulus of obtained ceramics was ${\sim}250$ GPa and hardness was in the range of $13{\sim}14$ GPa. The indentation fracture toughness increased from $2.58MPa{\cdot}m^{1/2}$ to $3.24MPa{\cdot}m^{1/2}$ with increasing sintering temperature possibly due to the elongated grains. Sliding wear tests revealed at least an order magnitude improvement in wear resistance with grain refinement. Microstructure analysis indicated that nano-$Si_3N_4$ specimens worn mainly through delamination and microcracking, while that of coarser specimens revealed severe wear with grain debonding and fracture.

Effect of ceramic powder addition on the insulating properties of polymer layer prepared by dip coating method

  • Kim, S.Y.;Lee, J.B.;Kwon, B.G.;Hong, G.W.
    • Progress in Superconductivity and Cryogenics
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    • v.16 no.1
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    • pp.14-18
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    • 2014
  • The mechanical, electrical and thermal characteristics of insulating materials may significantly affect the performance and reliability of electrical devices using superconductors. General method to provide insulating layer between coated conductors is wrapping coated conductor with Kapton tape. But uniform and compact wrapping without failure or delamination in whole coverage for long length conductor is not a simple task and need careful control. Coating of insulating layer directly on coated conductor is desirable for providing compact insulating layer rather than wrapping insulating layers around conductor. Ceramic added polymer has been widely used as an insulating material for electric machine because of its good electrical insulating properties as well as excellent heat resistance and fairy good mechanical properties. The insulating layer of coated conductor should have high breakdown voltage and possesses suitable mechanical strength and maintain adhesiveness at the cryogenic temperature where it is used and withstand stress from thermal cycling. The insulating and mechanical properties of polymer can be improved by adding functional filler. In this study, insulating layer has been made by adding ceramic particles such as $SiO_2$ to a polymer resin. The size, amount and morphology of added ceramic powder was controlled and their effect on dielectric property of the final composite was measured and discussed for optimum composite fabrication.

Electrochemical Evaluation of Si-Incorporated Diamond-Like Carbon (DLC) Coatings Deposited on STS 316L and Ti Alloy for Biomedical Applications

  • Kim, Jung-Gu;Lee, Kwang-Ryeol;Kim, Young-Sik;Hwang, Woon-Suk
    • Corrosion Science and Technology
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    • v.6 no.1
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    • pp.18-23
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    • 2007
  • DLC coatings have been deposited onto substrate of STS 316L and Ti alloy using r.f. PACVD (plasma-assisted chemical vapor deposition) with a mixture of $C_{6}H_{6}$ and $SiH_{4}$ as the process gases. Corrosion performance of DLC coatings was investigated by electrochemical techniques (potentiodynamic polarization test and electrochemical impedance spectroscopy) and surface analysis (scanning electron microscopy). The electrolyte used in this test was a 0.89% NaCl solution of pH 7.4 at temperature $37^{\circ}C$. The porosity and protective efficiency of DLC coatings were obtained using potentiodynamic polarization test. Moreover, the delamination area and volume fraction of water uptake of DLC coatings as a function of immersion time were calculated using electrochemical impedance spectroscopy. This study provides the reliable and quantitative data for assessment of the effect of substrate on corrosion performance of Si-DLC coatings. The results showed that Si-DLC coating on Ti alloy could improve corrosion resistance more than that on STS 316L in the simulated body fluid environment. This could be attributed to the formation of a dense and low-porosity coating, which impedes the penetration of water and ions.